自供能<strong>Ag/SnSe</strong>纳米管红外探测器的制备和性能研究

doi:10.11901/1005.3093.2021.375

材料研究学报

2022, Vol. 36

Issue (8): 591-596 DOI: 10.11901/1005.3093.2021.375

研究论文

本期目录 | 过刊浏览

自供能Ag/SnSe纳米管红外探测器的制备和性能研究

方向明¹, 任帅², 容萍², 刘烁², 高世勇²(

)

^1.太原学院材料与化学工程系太原 030032
^2.哈尔滨工业大学材料科学与工程学院哈尔滨 150001

Fabrication and Infrared Detection Performance of Ag-modified SnSe Nanotubes

FANG Xiangming¹, REN Shuai², RONG Ping², LIU Shuo², GAO Shiyong²(

)

^1.Department of Materials and Chemical Engineering, Taiyuan University, Taiyuan 030032, China
^2.School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China

引用本文:

方向明, 任帅, 容萍, 刘烁, 高世勇. 自供能Ag/SnSe纳米管红外探测器的制备和性能研究[J]. 材料研究学报, 2022, 36(8): 591-596.
Xiangming FANG, Shuai REN, Ping RONG, Shuo LIU, Shiyong GAO. Fabrication and Infrared Detection Performance of Ag-modified SnSe Nanotubes[J]. Chinese Journal of Materials Research, 2022, 36(8): 591-596.

全文: PDF(1505 KB) HTML

摘要:

采用光沉积法在SnSe纳米管表面沉积Ag纳米粒子,在室温下制备了Ag修饰的SnSe纳米管(Ag/SnSe),通过SEM、EDS、TEM和XRD等手段表征其表面形貌、元素组成和晶体结构。随后,将Ag/SnSe纳米管旋涂在FTO导电面作为工作电极并以Pt电极为对电极组装了Ag/SnSe纳米管红外探测器,使用830 nm的光作为红外模拟光源研究了红外探测性能。结果表明,Ag/SnSe纳米管的平均直径约为100~200 nm,Ag纳米颗粒负载在SnSe纳米管表面。与SnSe纳米管红外探测器相比,Ag修饰的SnSe纳米管红外探测器的最大光电流密度提高到120 nA/cm²,上升时间和下降时间分别缩短到0.109和0.086 s。同时,Ag修饰的SnSe纳米管红外探测器的稳定性较高,可循环使用。

关键词 ：无机非金属材料, SnSe纳米管, 光沉积法, Ag纳米粒子, 红外探测器

Abstract：

Ag-modified SnSe nanotubes (Ag/SnSe NTs) were fabricated by light irradiation assissted deposition process, therewith Ag nanoparticles were deposited on the surface of SnSe NTs at room temperature. The morphology, chemical composition and crystal structure of the prepared Ag/SnSe NTs were characterized by SEM, EDS, TEM and XRD. The results show that the average diameter of SnSe NTs covered with Ag nanoparticles is approximately 100~200 nm. In addition, the infrared detector based on Ag/SnSe NTs (IRPD) was assembled with Ag/SnSe NTs spin-coated on the conductive surface of FTO as the working electrode and the Pt electrode as the counter electrode. Afterwards, the infrared detection performance of Ag/SnSe NTs IRPD was further investigated by adopting infrared light of 830 nm as the simulated light source. Compared with the SnSe NTs IRPD, the maximum photocurrent density of Ag/SnSe NTs IRPD achieves 120 nA/cm², simultaneously the rise time and decay time are declined to 0.109 s and 0.086 s, respectively, demonstrating the characteristics of good stability and repeatability.

Key words： inorganic non-metallic materials SnSe nanotubes light deposition method Ag nanoparticles infrared detector

收稿日期: 2021-06-24

ZTFLH:

TN36

基金资助:国家重点研发计划(2019YFA0705201);黑龙江省自然科学基金(LH2020E033)

作者简介: 方向明,男,1982年生,副教授

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https://www.cjmr.org/CN/10.11901/1005.3093.2021.375 或 https://www.cjmr.org/CN/Y2022/V36/I8/591

图1 SnSe纳米管和Ag/SnSe纳米管的SEM照片

图2 Ag/SnSe纳米管的EDS能谱

图3 Ag/SnSe纳米管的TEM和高分辨TEM照片

图4 Ag/SnSe纳米管的XRD谱

图5 SnSe纳米管和Ag/SnSe纳米管红外探测器在开/关红外光照射下的电流密度曲线

图6 SnSe纳米管和Ag/SnSe纳米管红外探测器单个周期的光电响应特征曲线

图7 Ag/SnSe纳米管红外探测器的原理

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