等温处理时间对触变挤压锡青铜轴套的组织和性能的影响

doi:10.11901/1005.3093.2021.280

材料研究学报

2022, Vol. 36

Issue (9): 641-648 DOI: 10.11901/1005.3093.2021.280

研究论文

本期目录 | 过刊浏览

等温处理时间对触变挤压锡青铜轴套的组织和性能的影响

肖寒(

), 周瑀杭, 陈磊, 张雄超, 崔鋆昕, 熊迟

昆明理工大学材料科学与工程学院昆明 650093

Effect of Isothermal Time on Microstructure and Properties of Thixo-extruded Tin Bronze Bushing

XIAO Han(

), ZHOU Yuhang, CHEN Lei, ZHANG Xiongchao, CUI Yunxin, XIONG Chi

Faculty of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, China

引用本文:

肖寒, 周瑀杭, 陈磊, 张雄超, 崔鋆昕, 熊迟. 等温处理时间对触变挤压锡青铜轴套的组织和性能的影响[J]. 材料研究学报, 2022, 36(9): 641-648.
Han XIAO, Yuhang ZHOU, Lei CHEN, Xiongchao ZHANG, Yunxin CUI, Chi XIONG. Effect of Isothermal Time on Microstructure and Properties of Thixo-extruded Tin Bronze Bushing[J]. Chinese Journal of Materials Research, 2022, 36(9): 641-648.

全文: PDF(20170 KB) HTML

摘要:

采用冷轧-等温处理SIMA法(CRITSIMA 法)制备半固态锡青铜坯料并将其挤压成锡青铜轴套,研究了等温处理时间对其微观组织和力学性能的影响。结果表明：随着等温处理时间的延长锡青铜轴套的平均晶粒尺寸随之增大,晶粒的粗化速率为296 μm³/s,形状因子先增大后减小,布氏硬度和延伸率先提高后降低,抗拉强度逐渐降低。在910℃等温15 min的锡青铜轴套其综合性能最高,形状因子为0.74,平均晶粒尺寸为63.56 μm,抗拉强度为368 MPa,延伸率为4.5%,布氏硬度为126 HBW。

关键词 ：金属材料, 铜合金, 等温处理, 触变挤压, 微观组织, 力学性能

Abstract：

Semi-solid tin bronze blanks was prepared by cold rolling-isothermal treatment SIMA method (CRITSIMA method), and then tin bronze bushing parts were extruded. The effect of isothermal treatment time on the microstructure and mechanical properties of thixotropic tin bronze bushing parts is investigated. The results show that with the increase of isothermal treatment time, the average grain size gradually increased, the coarsening rate of solid grain is 296 μm³/s, the shape factor first increased and then decreased, the Brinell hardness first increased and then decreased, the tensile strength gradually decreased, and the elongation first increased and then decreased. The microstructure and comprehensive properties of the tin bronze bushing are the best when kept at 910℃ for 15 min. The shape factor is 0.74, the average grain size is 63.56 μm, the tensile strength is 368 MPa, the elongation is 4.5%, and the Brinell hardness is 126 HBW.

Key words： metal materials copper alloy isothermal treatment thixotropic extrusion microstructure mechanical properties

收稿日期: 2021-04-29

ZTFLH:

TG146.1⁺1

基金资助:国家自然科学基金(51965028);云南省基础研究计划项目(202001AT070031);昆明理工大学分析测试基金(2019T20100165)

作者简介: 肖寒,男,1981年生,博士

	服务

	把本文推荐给朋友
	加入引用管理器
	E-mail Alert
	RSS
	作者相关文章
	肖寒
	周瑀杭
	陈磊
	张雄超
	崔鋆昕
	熊迟
44.8K

链接本文:

https://www.cjmr.org/CN/10.11901/1005.3093.2021.280 或 https://www.cjmr.org/CN/Y2022/V36/I9/641

图1 触变成形模具的示意图

图2 拉伸试样的尺寸和取样位置

图3 等温时间不同的锡青铜的金相组织

图4 等温时间不同的锡青铜的晶粒尺寸和形状因子

图5 锡青铜的平均晶粒尺寸D3与等温时间关系的散点图和线性拟合

图6 在触变挤压锡青铜不同位置取样的金相组织

图7 触变挤压锡青铜的XRD谱

图8 触变挤压锡青铜的面扫描图

表1 触变挤压锡青铜中Cu、Sn和P 元素的含量

图9 等温时间不同的锡青铜的布氏硬度

图10 等温时间不同的锡青铜试样的拉伸性能

图11 等温时间不同的锡青铜拉伸断口的形貌

1	Spencer D B, Mehrabian R, Flemings M C. Rheological behavior of Sn-15 pct Pb in the crystallization range [J]. Metallurgical Transactions B, 1972, 3(7): 1925
2	Flemings M C. Behavior of metal alloys in the semisolid state [J]. Metallurgical Transactions B, 1991, 22(3): 269 doi: 10.1007/BF02651227
3	Chu C L, Wu X Q, Qiu S C, et al. Microstructure and Gd-rich phase evolution of as-cast AZ31-xGd magnesium alloys during semi-solid isothermal heat treatment [J]. J. Cent. South. Univ., 2021, 28(01): 1 doi: 10.1007/s11771-020-4504-x
4	Zhang H T, Fan L L, Zhou M Y, et al. Effects of semi-solid treatment by electro-magnetic induction on micro-structure evolution and mechanical properties of the Mg-2.4Y-4Nd-0.5Zr-1Ni alloys [J]. Mater. Res. Express., 2020, 7(5): 6506
5	Jiang J F, Wang Y, Qu J J, et al. Microstructure evolution of AM60 magnesium alloy semisolid slurry prepared by new SIMA [J]. J. Alloy. Compd., 2010, 497: 62 doi: 10.1016/j.jallcom.2010.02.099
6	Guan R G, Zhao Z Y. Simulation and experimental research on continuous extending rheo-extrusion process for producing 6201 alloy tube [J]. Chin. J. Mater. Res., 2011, 25(1): 25
6	管仁国, 赵占勇. 6201合金管材连续流变扩展挤压成形过程的数值模拟和实验研究 [J]. 材料研究学报, 2011, 25(1): 25
7	Gu G C, Pesci R, Langlois L, et al. Microstructure investigation and flow behavior during thixoextrusion of M2 steel grade [J]. J. Mater. Process. Tech., 2015, 216: 178 doi: 10.1016/j.jmatprotec.2014.09.009
8	Meng Y, Sugiyama S, Soltanpour M, et al. Effects of predeformation and semi-solid processing on microstructure and mechanical properties of Cr-V-Mo steel [J]. J. Mater. Process. Tech., 2013, 213(3): 426 doi: 10.1016/j.jmatprotec.2012.09.021
9	Chen Y N, Wei J F, Zhao Y Q, et al. Microstructure evolution and grain growth behavior of Ti14 alloy during semi-solid isothermal process [J]. T. Nonferr. Metal. Soc., 2011, 21(5): 1018 doi: 10.1016/S1003-6326(11)60815-7
10	Cao M, Wang Z, Zhang Q. Microstructure-dependent mechanical properties of semi-solid copper alloys [J]. J. Alloy. Compd., 2017, 715: 413 doi: 10.1016/j.jallcom.2017.03.360
11	Cao M, Zhang Q, Huang K, et al. Microstructural evolution and deformation behavior of copper alloy during rheoforging process [J]. J. Mater. Sci. Technol., 2020, 42: 17 doi: 10.1016/j.jmst.2019.09.036
12	Wang J, Xiao H, Wu L B, et al. Study of rolling-remelting SIMA process for preparing the semi-solid billet of ZCuSn10 alloy [J]. Acta. Metall. Sin., 2014, 50(5): 567 doi: 10.3724/SP.J.1037.2013.00654
12	王佳, 肖寒, 吴龙彪等. 轧制-重熔SIMA 法制备ZCuSn10 合金半固态坯料 [J]. 金属学报, 2014, 50(5): 567 doi: 10.3724/SP.J.1037.2013.00654
13	Jiang J F, Wang Y, Liu J, et al. Microstructure and mechanical properties of AZ61 magnesium alloy parts achieved by thixo-extruding semisolid billets prepared by new SIMA [J]. T. Nonferr. Metal. Soc., 2013, 23(03): 576 doi: 10.1016/S1003-6326(13)62502-9
14	Cao M, Zhang Q, Zhang Y S. Effects of plastic energy on thixotropic microstructure of C5191 alloys during SIMA process [J]. J. Alloy. Compd., 2017, 721: 220 doi: 10.1016/j.jallcom.2017.05.245
15	Sankara Rao L, Jha A K, Ojha S N. Microstructure and Tribological Characteristics of Strain-Induced Melt Activation (SIMA)-Processed Al-10Cu-Fe alloy [J]. Int. J. Metalcast., 2018, 12(3): 523 doi: 10.1007/s40962-017-0187-y
16	Chen G, Zhou T, Wang B, et al. Microstructure evolution and segregation behavior of thixoformed Al-Cu-Mg-Mn alloy [J]. T. Nonferr. Metal. Soc., 2016, 26(01): 39 doi: 10.1016/S1003-6326(16)64086-4
17	Li Y K, Li L, Geng B Y, et al. Microstructure characteristics and strengthening mechanism of semisolid CuSn10P1 alloys [J]. Mater. Charact., 2021, 172: 110898 doi: 10.1016/j.matchar.2021.110898
18	Jiang J F, Wang Y, Xiao G F, et al. Comparison of microstructural evolution of 7075 aluminum alloy fabricated by SIMA and RAP [J]. J. Mater. Process. Tech., 2016, 238: 361 doi: 10.1016/j.jmatprotec.2016.06.020
19	Lifshitz I M, Slyozov V V. The kinetics of precipitation from supersaturated solid solutions [J]. J. Phys. Chem. Solids., 1961, 19(1): 35 doi: 10.1016/0022-3697(61)90054-3
20	Chen G, Zhang S, Zhang H M, et al. Controlling liquid segregation of semi-solid AZ80 magnesium alloy by back pressure thixoextruding [J]. J. Mater. Process. Tech., 2018, 259: 88 doi: 10.1016/j.jmatprotec.2018.04.023
21	Vieira E A, Ferrante M. Prediction of rheological behaviour and segregation susceptibility of semi-solid aluminium-silicon alloys by a simple back extrusion test [J]. Acta. Mater., 2005, 53: 5379 doi: 10.1016/j.actamat.2005.08.014

[1]	潘新元, 蒋津, 任云飞, 刘莉, 李景辉, 张明亚. 热挤压钛/钢复合管的微观组织和性能[J]. 材料研究学报, 2023, 37(9): 713-720.
[2]	毛建军, 富童, 潘虎成, 滕常青, 张伟, 谢东升, 吴璐. AlNbMoZrB系难熔高熵合金的Kr离子辐照损伤行为[J]. 材料研究学报, 2023, 37(9): 641-648.
[3]	宋莉芳, 闫佳豪, 张佃康, 薛程, 夏慧芸, 牛艳辉. 碱金属掺杂MIL125的CO₂ 吸附性能[J]. 材料研究学报, 2023, 37(9): 649-654.
[4]	赵政翔, 廖露海, 徐芳泓, 张威, 李静媛. 超级奥氏体不锈钢24Cr-22Ni-7Mo-0.4N的热变形行为及其组织演变[J]. 材料研究学报, 2023, 37(9): 655-667.
[5]	邵鸿媚, 崔勇, 徐文迪, 张伟, 申晓毅, 翟玉春. 空心球形AlOOH的无模板水热制备和吸附性能[J]. 材料研究学报, 2023, 37(9): 675-684.
[6]	幸定琴, 涂坚, 罗森, 周志明. C含量对VCoNi中熵合金微观组织和性能的影响[J]. 材料研究学报, 2023, 37(9): 685-696.
[7]	欧阳康昕, 周达, 杨宇帆, 张磊. 含LPSO相Mg-Y-Er-Ni合金的组织和拉伸性能[J]. 材料研究学报, 2023, 37(9): 697-705.
[8]	徐利君, 郑策, 冯小辉, 黄秋燕, 李应举, 杨院生. 定向再结晶对热轧态Cu71Al18Mn11合金的组织和超弹性性能的影响[J]. 材料研究学报, 2023, 37(8): 571-580.
[9]	熊诗琪, 刘恩泽, 谭政, 宁礼奎, 佟健, 郑志, 李海英. 固溶处理对一种低偏析高温合金组织的影响[J]. 材料研究学报, 2023, 37(8): 603-613.
[10]	刘继浩, 迟宏宵, 武会宾, 马党参, 周健, 徐辉霞. 喷射成形M3高速钢热处理过程中组织的演变和硬度偏低问题[J]. 材料研究学报, 2023, 37(8): 625-632.
[11]	陈晶晶, 占慧敏, 吴昊, 朱乔粼, 周丹, 李柯. 纳米晶CoNiCrFeMn高熵合金的拉伸力学性能[J]. 材料研究学报, 2023, 37(8): 614-624.
[12]	由宝栋, 朱明伟, 杨鹏举, 何杰. 合金相分离制备多孔金属材料的研究进展[J]. 材料研究学报, 2023, 37(8): 561-570.
[13]	任富彦, 欧阳二明. g-C₃N₄ 改性Bi₂O₃ 对盐酸四环素的光催化降解[J]. 材料研究学报, 2023, 37(8): 633-640.
[14]	王昊, 崔君军, 赵明久. 镍基高温合金GH3536带箔材的再结晶与晶粒长大行为[J]. 材料研究学报, 2023, 37(7): 535-542.
[15]	刘明珠, 樊娆, 张萧宇, 马泽元, 梁城洋, 曹颖, 耿仕通, 李玲. SnO₂ 作散射层的光阳极膜厚对量子点染料敏化太阳能电池光电性能的影响[J]. 材料研究学报, 2023, 37(7): 554-560.

Viewed

Full text

Abstract

Cited

Shared

Discussed