Hot Isostatic Pressing of GH4099 Alloy Powders and Preparation of Thin-walled Cylinders

doi:10.11901/1005.3093.2023.514

Chinese Journal of Materials Research

2024, Vol. 38

Issue (9): 669-679 DOI: 10.11901/1005.3093.2023.514

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Hot Isostatic Pressing of GH4099 Alloy Powders and Preparation of Thin-walled Cylinders

YIN Yifeng¹^,², LU Zhengguan¹, XU Lei¹, WU Jie¹(

)

1 Shi -changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2 School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110116, China

Cite this article:

YIN Yifeng, LU Zhengguan, XU Lei, WU Jie. Hot Isostatic Pressing of GH4099 Alloy Powders and Preparation of Thin-walled Cylinders. Chinese Journal of Materials Research, 2024, 38(9): 669-679.

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Abstract

Two pre-powders of GH4099 alloy were prepared via techniques of plasma rotating electrode process (PREP) and electrode induction melting gas atomization (EIGA) respectively. Then, the powders were subjected to hot isostatic pressing (HIP) to prepare bulk GH4099 alloy (PM GH4099 alloy), and the effect of HIP temperature on the microstructure and tensile properties of PM GH4099 alloy was investigated. The results show that in comparison with EIGA process, the GH4099 powder prepared by PREP process has better powder sphericity with thinner surface oxide scale, which is more suitable for hot isostatic pressing preparation of workpiece of PM GH4099 alloys. With the increasing HIP temperature within the range of 1165^oC~1230^oC, the porosity and prior particle boundaries (PPBs) of the acquired PM GH4099 alloy decreases significantly, therewith, the corresponding tensile properties at 900^oC were improved. Finally, with the help of finite element modeling (FEM) to assist the envelope design and make, and finally thin-walled cylinders of PM GH4099 were successfully fabricated with the PREP powder via HIP at 1230^oC/150 MPa/4 h. The FEM predicted dimensional shrinkages are consistent with that of the actual made thin-walled cylinders of PM GH4099, and the deviation between the corresponding key dimensions is less than 5%.

Key words: metallic materials GH4099 alloy powder metallurgy hot isostatic pressing near-net shape manufacturing

Received: 19 October 2023

ZTFLH:

TG132.32

Fund: CAS Project for Young Scientists in Basic Research(YSBR-025);National Science and Technology Major Project of China(J2019-VⅡ-0005-0145)

Corresponding Authors: WU Jie, Tel: (024)83978843, E-mail: jwu10s@imr.ac.cn

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https://www.cjmr.org/EN/10.11901/1005.3093.2023.514 OR https://www.cjmr.org/EN/Y2024/V38/I9/669

Table 1 Chemical compositions of GH4099 pre-alloyed powders (mass fraction, %)

Fig.1 Morphologies of GH4099 pre-alloyed powders (a) PREP, (b) EIGA

Fig.2 Particle size distribution of GH4099 pre-alloyed powders

Fig.3 XPS patterns of GH4099 pre-alloyed powders (a) EIGA, (b) PREP

Fig.4 DSC curves of GH4099 pre-alloyed powders during the heating stage

Table 2 HIP conditions for GH4099 alloy powders

Fig.5 SEM images of GH4099 alloys (a, b) HIP1, (c) HIP2, (d) HIP3

Fig.6 Carbide at the PPBs in GH4099 alloys under HIP3. (a) TEM images, (b) Electron diffraction pattern and (c) EDS spectrum of particle 1 in (a)

Fig.7 Micro-CT images of GH4099 alloys (a) HIP1, (b) HIP3, and (c) column comparison chart

Fig.8 Tensile properties at room and elevated temperature of as-HIPed GH4099 alloys (a, b) room temperature and (c, d) 900^oC

Fig.9 Tensile fracture surface of GH4099 alloys at 900^oC (a) HIP1, (b) HIP2, (c) HIP3

Fig.10 Predicted size of thin-walled cylinder before (a) and after (b) shrinkage by FEM

Fig.11 Physical model diagram of thin-walled cylinder (a) and relative positional relationship between simulated and measured values of thin-walled cylinder cross-section (b)

Table 3 Comparison of the measured and simulated dimensions of thin-walled cylinder at some positions

1	Zhang H B. Hot deformation behavior and microstructure evolution of GH99 superalloy [D]. Harbin: Harbin Institute of Technology, 2015
	张弘斌. GH99高温合金高温变形行为及组织演化规律研究 [D]. 哈尔滨: 哈尔滨工业大学, 2015
2	Li F, Lu Q, Yu Y D. Forming process and microstructure and properties of selective laser melted GH4099 superalloy [J]. T. Mater. Heat Treat., 2021, 42(9): 98 doi: 10.13289/j.issn.1009-6264.2021-0132
	李范, 卢强, 佘亚东. 激光选区熔化GH4099高温合金成形工及组织性能 [J]. 材料热处理学报, 2021, 42(9): 98
3	Lü H, Yang Z B, Wang X, et al. Microstructures and tensile properties of GH4099 alloy Fabricated by laser additive manufacturing after heat treatment [J]. Chin. J. Lasers., 2018, 45(10): 77
	吕豪, 杨志斌, 王鑫等. 激光增材制造GH4099合金热处理后的显微组织及拉伸性能 [J]. 中国激光, 2018, 45(10): 77
4	Hu Y L, Lin X, Li Y L, et al. Effect of heat treatment on the microstructural evolution and mechanical properties of GH4099 additive-manufactured by directed energy deposition [J]. J. Alloys. Compd., 2019, 800: 163
5	Tan C L, Weng F, Sui S, et al. Progress and perspectives in laser additive manufacturing of key aeroengine materials [J]. Int. J. Mach. Tools. Manuf., 2021, 170: 103804
6	Thomas M, Baxter G J, Todd I. Normalised model-based processing diagrams for additive layer manufacture of engineering alloys [J]. Acta Mater., 2016, 108: 26
7	Xu J H, Schulz F, Peng R L, et al. Effect of heat treatment on the microstructure characteristics and microhardness of a novel γ′ nickel-based superalloy by laser powder bed fusion [J]. Results Mater., 2021(12): 100232
8	Xu L, Guo R P, Wu J, et al. Progress in hot isostatic pressing technology of titanium alloy powder. [J]. Acta Metall. Sin., 2018, 54(11): 1537
	徐磊, 郭瑞鹏, 吴杰等. 钛合金粉末热等静压近净成形研究进展 [J]. 金属学报, 2018, 54(11): 1537
9	Tian X S, Wu Jie, Lu Z G, et al. Effects of cooling rate on the microstructure and tensile properties of powder metallurgy Ti₂AlNb alloy [J]. JOM, 2022, 74(8): 2964
10	Raisson G. Evolution of PM nickel base superalloy processes and products [J]. Powder Metall., 2008, 51: 10
11	Bampton C, Goodin W, Vandaam T, et al. Net-shape HIP powder metallurgy components for rocket engines [A]. International Conference on Hot Isostatic Pressing 2005, Net-Shape HIP Powder Metallurgy Components for Rocket Engines [C]. Paris, France, 2005
12	Bassini E, Basile G, Marchese G, et al. Assessment of the reinforcing system and carbides evolution in hot isostatically pressed astroloy after prolonged exposure at 820^oC [J]. Mater. Sci. Eng. A, 2020, 773: 138879
13	Tian X S. Densification mechanism of Inconel 718 pre-alloyed powders consolidated by hot isostatic pressing [D]. Shenyang: University of Science and Technology of China, 2023
	田晓生. Inconel 718粉末合金的热等静压致密化机理研究 [D]. 沈阳: 中国科学技术大学, 2023
14	Hans F, David F. Processing of nickel-base superalloys for turbine engine disc applications [J]. Adv. Powder Technol., 2000, 2: 777
15	Liu Q M, Wu J, Chen Y L, et al. Effect of temperature and powder particle size on mechanical properties and microstructure of PM Ti₂AlNb alloy prepared via hot isostatic pressing [J]. Chin. J. Mater. Res., 2019, 33(3): 161
	刘巧沐, 吴杰, 陈玉龙等. 热等静压温度和粉末粒度对Ti₂AlNb合金组织与性能的影响 [J]. 材料研究学报, 2019, 33(3): 161 doi: 10.11901/1005.3093.2018.509
16	Chang L T. Preparation and hot isostatic press compaction of superalloy powder with less ceramic inclusions [D]. Shenyang: University of Chinese Academy of Sciences, 2014
	常立涛. 洁净高温合金粉末的制备及其热等静压工艺研究 [D]. 沈阳: 中国科学院大学, 2014
17	Wang H L. Study on improving mechanical properties of GH99 alloy plate [J]. Sichuan Metall., 2006, 26(1): 30
	王怀柳. 改善GH99合金板材力学性能的研究 [J]. 四川冶金, 2006, 26(1): 30
18	Wu J, Xu L, Cui X X, et al. Hot isostatic pressing of large thin-wall cylindrical structure of Inconel 718 ring [J]. Aerosp. Sci. Technol., 2020, 63(16): 59
	吴杰, 徐磊, 崔潇潇等. 大尺寸薄壁Inconel 718环件粉末热等静压近净成形 [J]. 航空制造技术, 2020, 63(16): 59
19	Lu Z G, Wu J, Guo R P, et al. Hot deformation mechanism and ring rolling behavior of powder metallurgy Ti₂AlNb intermetallics [J]. Acta Metall. Sin. (Engl. Lett.), 2017, 30(7): 621
20	Chang L T, Sun W R, Cui Y Y, et al. Preparation of hot-isostatic-pressed powder metallurgy superalloy Inconel 718 free of prior particle boundaries [J]. Mater. Sci. Eng. A, 2017, 682: 341
21	Xu L, Guo R P, Chen Z Y, et al. Mechanical property of powder compact and forming of large thin-wall cylindrical structure of Ti55 alloys [J]. Chin. J. Mater. Res., 2016, 30(1): 23 doi: 10.11901/1005.3093.2015.284
	徐磊, 郭瑞鹏, 陈志勇等. Ti55合金的拉伸性能和薄壁筒体结构的成形 [J]. 材料研究学报, 2016, 30(1): 23
22	Zhang Y W, Liu J T, Han S B, et al. Discussion on the mechanism of micro-element Hf eliminating PPBS in powder metallurgy superalloy FGH96 [J]. Powder Metall. Ind., 2014, 24(5): 1
	张义文, 刘建涛, 韩寿波等. 微量元素Hf消除FGH96合金中原始粉末颗粒边界组织机制的探讨 [J]. 粉末冶金工业, 2014, 24(5): 1
23	Xu L, Tian X S, Wu J, et al. Hot isostatic microstructure and mechanical properties of Inconel 718 powder alloy prepared by hot isostatic pressing [J]. Acta Metall. Sin., 2023, 59(5): 693 doi: 10.11900/0412.1961.2021.00586
	徐磊, 田晓生, 吴杰等. 热等静压成形Inconel 718粉末合金的显微组织和力学性能 [J]. 金属学报, 2023, 59(5): 693
24	Tan L M. Effect of Co, W, Mo and C on microstructure and mechanical properties of FGH4097PM superalloy [D]. Beijing: Central Iron & Steel Research Institute, 2015
	谭黎明. Co, W, Mo和C元素对粉末高温合金FGH4097组织和性能的影响 [D]. 北京: 钢铁研究总院, 2015
25	Tian X S, Wu J, Lu Z G, et al. Effect of powder size segregation on the mechanical properties of hot isostatic pressing Inconel 718 alloys [J]. J. Mater. Res. Technol., 2022, 21: 84
26	Wu J, Guo R P, Xu L, et al. Effect of hot isostatic pressing loading route on microstructure and mechanical properties of powder metallurgy Ti₂AlNb alloys [J]. J. Mater. Sci. Technol., 2017, 33(2): 172
27	Yu C, Wu S C, Hu Y N, et al. Three-dimensional imaging of gas pores in fusion welded Al alloys by synchrotron radiation X-ray microtomography [J]. Acta Metall. Sin., 2015, 51(2): 159 doi: 10.11900/0412.1961.2014.00334
	喻程, 吴圣川, 胡雅楠等. 铝合金熔焊微气孔的三维同步辐射X射线成像 [J]. 金属学报, 2015, 51(2): 159
28	Guo R P, Xu L, Zong Y P, et al. Characterization of prealloyed Ti-6AI-4V powders from EIGA and PREP process and mechanical properties of HIPed powder compacts [J]. Acta Metall. Sin. (Engl. Lett.), 2017, 8: 735
29	Tvergaard V. On localization in ductile materials containing spherical voids [J]. Int. J. Fract., 1982, 18(4): 237
30	Aravas N. On the numerical integration of a class of pressure-dependent plasticity models [J]. Int. J. Numer. Meth. Eng., 1987, 24(7): 1395
31	Wu J. Preparation and mechanical properties optimization of powder metallurgy TiAlNb.5Mo alloys [D]. Beijing: University of Chinese Academmy of Sciences, 2016
	吴杰. 粉末冶金Ti-22Al-24Nb-0.5Mo合金的制备和性能调控 [D]. 北京: 中国科学院大学, 2016

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