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材料研究学报  2016, Vol. 30 Issue (10): 767-772    DOI: 10.11901/1005.3093.2015.325
  研究论文 本期目录 | 过刊浏览 |
X70管线钢的应变时效行为
姜永文1(),牛涛1,安成钢1,吴新朗2,张彩霞2,代晓莉1
1. 首钢技术研究院 北京 100043
2. 首钢股份公司迁安钢铁公司 迁安 064404
Strain Aging Behavior of X70 Pipeline Steel
Yongwen JIANG1,**(),Tao NIU1,Chenggang AN1,Xinlang WU2,Caixia ZHANG2,Xiaoli DAI1
1. Shougang Research Institute of Technology, Beijing 100043, China
2. Shougang Qian’an Iron &Steel Co.Ltd, Qian’an 064404, China;
引用本文:

姜永文,牛涛,安成钢,吴新朗,张彩霞,代晓莉. X70管线钢的应变时效行为[J]. 材料研究学报, 2016, 30(10): 767-772.
Yongwen JIANG, Tao NIU, Chenggang AN, Xinlang WU, Caixia ZHANG, Xiaoli DAI. Strain Aging Behavior of X70 Pipeline Steel[J]. Chinese Journal of Materials Research, 2016, 30(10): 767-772.

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摘要: 

采用扫描电子显微镜(SEM)、透射电子显微镜(TEM)等手段研究了时效温度和预应变量对X70管线钢的显微组织和力学性能的影响。结果表明, 由于时效温度比较低(最高300℃), 时效前后X70钢的组织都由粒状贝氏体+针状铁素体+M/A组成, 没有明显的变化。时效前后抗拉强度的变化也不明显。随着时效温度的提高活化的间隙原子增多, 钉扎的位错数量增加, 屈服强度提高; 当时效温度高于200℃时可供钉扎的位错开始大量回复, 屈服强度逐渐降低。随着时效温度的提高柯氏气团及析出物的数量增加, 使材料硬化, 冲击韧性逐渐下降。随着预应变量的增大可被间隙原子钉扎的位错数量增加, 屈服强度逐渐升高。随着预应变量的增大硬质相M/A边界处产生的应力集中不断增大, 产生微裂纹的概率不断提高, 使冲击韧性逐渐下降。

关键词 金属材料X70管线钢应变时效力学性能微观组织    
Abstract

Effect of pre-strain and aging temperature on mechanical property and microstructure of X70 pipeline steel was investigated by means of scanning electron microscope ( SEM ) and transmission electron microscope ( TEM ). The results indicate that the X70 steel shows a microstructure compopsed of granular bainite, acicular ferrite and M/A. The aging temperatures below 300℃, exhibit nearly no effect on the microstructure and the tensile strength of the steel. With the rising of aging temperature, the quantity of activated interstitial atoms, therewith, the pinning effect on dislocations increases, which leads to the gradual increase of the yield strength; However, when the temperature raises to above 200℃, the recovery of pinning effect occurs resulting in the decline of the yield strength. With the rising of aging temperature, the hardening of material induced by the increased cottrell atmosphere and precipitations leads to the decline of the impact toughness. With the increase of the pre-strain, the increment of dislocations may lead to the increase of yield strength, and the stress concentration will increase at boundries of the hard brittle phase M/A, therewith increase the probability of the formation micro-cracks, as a result, the impact toughness delines.

Key wordsmetal materials    X70 pipeline steel    strain aging    mechanical properties    microstructure
收稿日期: 2015-10-12     
Element C Si Mn Nb+V+Ti Mo Others
Content ≤0.07 0.10~0.30 1.50~1.80 ≤0.10 0.10~0.30 Cr、Cu、Ni
表1  试验用钢的化学成分(质量分数, %)
No. Pre-strain/% Aging temperature/℃ Holding time/min Cooling mode
1-1 3 RT / /
1-2 3 150 10 AC
1-3 3 200 10 AC
1-4 3 250 10 AC
1-5 3 300 10 AC
表2  不同时效温度试验方案
No. Pre-strain/% Aging temperature/℃ Holding time/min Cooling mode
2-1 Rolled / / /
2-2 0 200 10 AC
2-3 1 200 10 AC
2-4 2 200 10 AC
2-5 3 200 10 AC
表3  不同预应变量试验方案
图1  不同时效温度下的力学性能(a)强度; (b)屈强比; (c)伸长率; (d)冲击吸收功
图2  不同预应变下力学性能变化(a)强度; (b)屈强比; (c)伸长率; (d)冲击吸收功
图3  不同预应变下的拉伸曲线局部放大图
图4  不同时效温度下的组织对比(SEM) (a)轧制态; (b)150℃; (c)250℃; (d)300℃
图5  不同预应变量下的冲击断口(SEM) (a) 轧制态; (b) 3%预应变/300℃
图6  不同时效温度下X70位错组态 (a)室温; (b)300℃
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