回火温度对两相区退火海工钢组织和性能的影响

doi:10.11901/1005.3093.2020.070

材料研究学报

2020, Vol. 34

Issue (11): 845-852 DOI: 10.11901/1005.3093.2020.070

研究论文

本期目录 | 过刊浏览

回火温度对两相区退火海工钢组织和性能的影响

张翔云¹, 李激光¹(

), 严玲², 何煦泽¹, 郭菁¹

^1.辽宁科技大学材料与冶金学院鞍山 114051
^2.海洋装备用金属材料及其应用国家重点实验室鞍山 114009

Effect of Tempering Temperature on Microstructure and Properties of Intercritical Annealing Marine Steel

ZHANG Xiangyun¹, LI Jiguang¹(

), YAN Ling², HE Xuze¹, GUO Jing¹

^1.School of Materials and Metallurgy, University of Science and Technology Liaoning, Anshan 114051, China
^2.State Key Laboratory of Metal Materials for Marine Equipment and Applications, Anshan 114009, China

引用本文:

张翔云, 李激光, 严玲, 何煦泽, 郭菁. 回火温度对两相区退火海工钢组织和性能的影响[J]. 材料研究学报, 2020, 34(11): 845-852.
Xiangyun ZHANG, Jiguang LI, Ling YAN, Xuze HE, Jing GUO. Effect of Tempering Temperature on Microstructure and Properties of Intercritical Annealing Marine Steel[J]. Chinese Journal of Materials Research, 2020, 34(11): 845-852.

全文: PDF(6511 KB) HTML

摘要:

对690 MPa级海工钢进行“淬火+两相区退火+回火”三步热处理，研究了回火温度对其组织和性能的影响、分析了力学性能变化与组织演变和残余奥氏体体积分数之间的关系。结果表明：回火后实验钢的显微组织为回火贝氏体/马氏体、临界铁素体和残余奥氏体的混合组织。随着回火温度的提高贝氏体/马氏体和临界铁素体逐渐分解成小尺寸晶粒，而残余奥氏体的体积分数逐渐增加；屈服强度由787 MPa降低到716 MPa，塑性和低温韧性明显增强，断后伸长率由20.30%增至29.24%，-40℃下的冲击功由77 J提升至150 J。残余奥氏体体积分数的增加引起裂纹扩展功增大，是低温韧性提高的主要原因。贝氏体/马氏体的分解和残余奥氏体的生成，引起组织细化、晶粒内低KAM值位错的比例逐渐提高和小角度晶界峰值的频率增大，使材料的塑性和韧性显著提高。

关键词 ：金属材料, 海工钢, 两相区退火, 残余奥氏体, 低温韧性

Abstract：

The influence of tempering temperature on microstructure and mechanical properties of 690 MPa grade marine steel after quenching + intercritical annealing + tempering three-step heat treatment was investigated in terms of the microstructure evolution, the volume fraction of retained austenite and the change in mechanical properties. The results show that the microstructure of the steel after tempering is a mixture of tempered bainite/martensite, intercritical ferrite and retained austenite. With the increasing tempering temperature, bainite/martensite and intercritical ferrite gradually decomposed into small grains, while the volume fraction of retained austenite gradually increased. Yield strength decreased from 787 MPa to 716 MPa. Plasticity and low temperature toughness were significantly enhanced, elongation after fracture increased from 20.30% to 29.24%, and impact energy at -40℃ increased from 77 J to 150 J. The increase of the volume fraction of retained austenite lead to the increase of crack propagation work, which was the main cause responsible to the improvement of low temperature toughness. The decomposition of bainite/martensite and the formation of retained austenite lead to grain refinement, the number of dislocations with low KAM values in the grains increased, and the frequency of low angle grain boundary peaks increased, which may be beneficial to the significant increment of plasticity and toughness of the steel.

Key words： metallic materials offshore steel intercritical annealing retained austenite low temperature toughness

收稿日期: 2020-03-05

ZTFLH:

TG156.5

基金资助:国家自然科学基金(U1860112);海洋装备用金属材料及其应用国家重点实验室和辽宁科技大学联合基金(SKLMEA-USTL-201701)

作者简介: 张翔云，男，1994年生，硕士生

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https://www.cjmr.org/CN/10.11901/1005.3093.2020.070 或 https://www.cjmr.org/CN/Y2020/V34/I11/845

图1 实验钢的热处理工艺示意图

图2 在不同温度回火后实验钢的SEM照片

图3 T640试样中残余奥氏体的TEM照片、在不同温度回火试样的衍射谱和残余奥氏体的体积分数

表1 在不同温度回火后实验钢的力学性能

图4 不同工艺和冲击温度试样的示波冲击位移-载荷和位移-吸收能量曲线

图5 在不同温度回火后实验钢的局部取向差图

图6 在不同温度回火后实验钢的晶界分布

图7 在不同温度回火后实验钢的取向差角分布

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