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材料研究学报  2016, Vol. 30 Issue (7): 509-516    DOI: 10.11901/1005.3093.2015.185
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铸辗成形环坯热压缩过程中晶粒的取向和织构演变*
秦芳诚, 李永堂()
太原科技大学材料科学与工程学院 太原 030024
Evolution of Grain Orientation and Texture of Ring Shaped Blank Induced by Hot Compression During Casting-rolling Process
QIN Fangcheng, LI Yongtang**()
School of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan 030024, China
引用本文:

秦芳诚, 李永堂. 铸辗成形环坯热压缩过程中晶粒的取向和织构演变*[J]. 材料研究学报, 2016, 30(7): 509-516.
Fangcheng QIN, Yongtang LI. Evolution of Grain Orientation and Texture of Ring Shaped Blank Induced by Hot Compression During Casting-rolling Process[J]. Chinese Journal of Materials Research, 2016, 30(7): 509-516.

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摘要: 

在不同变形温度和应变速率为0.1 s-1条件下研究了砂型铸造和离心铸造Q235B环坯的热压缩变形行为, 并使用电子背散射衍射(EBSD)技术分析其晶粒取向和织构的演化特点。结果表明: Q235B环坯的晶粒在1000℃尺寸较小, 有少量仍保持铸造状态的晶粒, 组织演变的机理为动态回复和大应变几何动态再结晶; 离心铸造环坯中有22%集中在20°-50°的大角度晶界。在1100℃再结晶充分, 晶粒趋于等轴状; 晶界取向差分布仍呈现典型的双峰特征, 大角度晶界的比例为60%-75%。在1000℃砂型铸造Q235B的织构组态, 为少量沿着<001>//ND取向线分布的{001}<100>立方织构和{001}<110>织构; 在1100℃主要是高斯织构{110}<001>和沿着<110>//ND向{110}<001>方向移动并聚集的旋转立方织构{110}<110>。在1000℃离心铸造环坯的织构组态为旋转立方织构{110}<110>和铜型织构{112}<111>, Copper织构沿着ε-取向线分布; 在1100℃主要为{001}<110>织构和沿着γ 取向线由黄铜R{111}<112>向{111}<110>转变的织构, 再结晶的程度高, 取向密度大。

关键词 金属材料铸态Q235B环坯EBSD晶粒取向织构再结晶    
Abstract

The characteristics for the evolution of grain orientation and texture of ring shaped blanks of sand- and centrifugal-casting Q235B respectively were investigated by electron backscatter diffraction (EBSD) technique, while the blanks have been subjected to hot compression with a strain rate of 0.1 s-1 at different temperatures. The results show that the grain size of the blanks after hot compression at 1000℃ becomes smaller in the deformed microstructure, but a few grains maintains as in cast state. The mechanisms of the microstructure evolution may be ascribed to dynamic recovery and large strain geometric dynamic recrystallization. For centrifugal cast ones, the percentage of high-angle boundary in 20°-50° is 22%, but after hot compression at 1100℃ it shows a homogenous microstructure with equiaxed grains because of sufficient recrystallization, while the mis-orientation distribution of grain boundaries still presents a typical characteristic of double-peaks and the proportion of the high-angle boundaries reaches to 60%-75%. The textures of sand casting Q235B are a small amount cube texture {001}<100> and {001}<110> along <001>//ND at 1000℃, while the main textures are Goss texture {110}<001> and r-cube texture {110}<001> at 1100℃. For centrifugal casting ones at 1000℃, {110}<110> and Cu texture {112}<111> distributes along ε orientation; at 1100℃ the types of texture including {001}<110> and {111}<110> transformed from {111}<112> along γ orientation. The orientation density is higher due to the high extent of recrystallization.

Key wordsmetallic materials    as-cast Q235B ring blank    EBSD    grain orientation    texture    recrystallization
收稿日期: 2015-08-07     
基金资助:* 国家自然科学基金51135007、51174140、51205270, 高校博士项目20111415130001和山西省回国留学人员2011-084资助
作者简介: null

本文联系人: 李永堂

图1  Q235B环坯热压缩真应力-应变曲线
图2  砂型铸造环坯EBSD晶界重构图(红线>15°晶界, 绿线<15°晶界)
图3  离心铸造环坯EBSD晶界重构图(红线>15°晶界, 绿线<15°晶界)
图4  砂型铸造Q235B晶界取向差分布图
图5  离心铸造Q235B晶界取向差分布图
图6  砂型铸造Q235B环坯的ODF恒?2=45o截面图
图7  离心铸造Q235B环坯的ODF恒?2=45o截面图
图8  在不同变形条件下砂型铸造环坯的极图
图9  在不同变形条件下离心铸造环坯极图
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