液相沉淀法工艺条件对羟基磷灰石粉体的影响

材料研究学报

2012, Vol. 26

Issue (2): 187-190

研究论文

本期目录 | 过刊浏览

液相沉淀法工艺条件对羟基磷灰石粉体的影响

黄红燕^1,2, 杨梅², 张春紫³, 邵忠财²

1.沈阳市口腔医院沈阳 100002
2.沈阳理工大学环境与化学工程学院沈阳 110159
3.沈阳于洪张春紫口腔诊所沈阳 110142

Effects of Technological Parameters in the Process of HA Preparation

HUANG Hongyan^1,2, YANG Mei², ZHANG Chunzi³, SHAO Zhongcai²

1.Stomatology Hospitalof Shenyang, Shenyang 110002
2. School of Environment and Chemical Engineering, Shenyang Ligong University, Shenyang 110159
3. Shenyang Yuhong Zhang Chunzi Dental Clinic 110142

引用本文:

黄红燕杨梅张春紫邵忠财. 液相沉淀法工艺条件对羟基磷灰石粉体的影响[J]. 材料研究学报, 2012, 26(2): 187-190.
. Effects of Technological Parameters in the Process of HA Preparation[J]. Chin J Mater Res, 2012, 26(2): 187-190.

全文: PDF(837 KB)

摘要: 采用液相沉淀法成功制备纳米羟基磷灰石陶瓷粉体, 使用X--射线衍射、扫描电子显微镜等检测手段分析了粉体的组织结构, 研究了反应温度、pH值、陈化时间对粉末粒径和物相组成等的影响。结果表明, 反应温度为90℃、溶液pH值为10、陈化12 h, 在700℃煅烧2 h可制备出高纯度、晶体完整的球形羟基磷灰石粉体, 平均尺寸为60 nm。

关键词 ：无机非金属材料, 羟基磷灰石, 液相沉淀法, 纳米粉体

Abstract：Nano-sized hydroxyapatite(HA) powder was prepared by means of liquid precipitation method and its crystal structure and the characteristic were analyzed using X-ray diffraction and SEM. The effects of reaction temperature, pH value and aging time on the Powder particle size and phase composition were investigated. The results show on condition that value the reaction temperature is 90^oC, pH value is 10 and the aging time is 12 h, the pure and integrate HA crystals with average diameter of 70 nm can be gained.

收稿日期: 2011-05-31

ZTFLH:

TB321

基金资助:

沈阳市科学计划1081251--1--00资助项目。

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