Please wait a minute...
材料研究学报  2010, Vol. 24 Issue (1): 1-9    
  研究论文 本期目录 | 过刊浏览 |
等通道挤压AZ80镁合金的析出行为和性能
李萧1; 杨平1; 李继忠2; 丁桦2
1.北京科技大学材料科学与工程学院 北京 100083
2.东北大学冶金与材料学院 沈阳 110004
Precipitation Behavior, Texture and Mechanical Properties of AZ80 Magnesium Alloy Produced by Equal Channel
Angular Extrusion
LI Xiao1; YANG Ping1; LI Jizhong2; DING Hua2
1.School of Materials Science and Engineering; University of Science and Technology Beijing; Beijing 100083
2.School of Materials and Metallurgy; Northeastern University; Shenyang 110004
引用本文:

李萧 杨平 李继忠 丁 桦. 等通道挤压AZ80镁合金的析出行为和性能[J]. 材料研究学报, 2010, 24(1): 1-9.
, . Precipitation Behavior, Texture and Mechanical Properties of AZ80 Magnesium Alloy Produced by Equal Channel
Angular Extrusion[J]. Chin J Mater Res, 2010, 24(1): 1-9.

全文: PDF(1471 KB)  
摘要: 

研究了AZ80镁合金经300℃等通道挤压(ECAP)后的组织、织构与力学性能的演变规律以及第二相析出行为的影响。 结果表明: ECAP显著促进了粒状连续析出, 可有效节省后续热处理时间。A路径多道次挤压最终获得基面织构; Bc路径挤压后形成基面近似平行于剪切面的织构; 第二相析出对ECAP织构特征的形成没有显著影响。 用该工艺可获得较高的延伸率(13%--19%), 但是抗拉强度过低($<$300 MPa), 综合机械性能不理想。 可通过抑制挤压前的未溶粗大粒子的析出、减少挤压道次和降低挤压温度等措施优化AZ80的析出控制。

关键词 金属材料  AZ80镁合金 ECAP 析出 织构 性能    
Abstract

AZ80 magnesium alloy was subjected to ECAP (equal channel angular extrusion) processing at 300. The evolution of microstructure, texture and mechanical properties influenced by the precipitation was investigated. The results show that ECAP processing significantly favored granular–like Mg17Al12 continuous precipitation in accompany with reducing time effectively during subsequent aging treatment; basal texture can be obtained via route A after ECAP with multi passes, whereas typical shear texture with most basal planes parallel to the shear plane of mode in route Bc; however the precipitation has not remarkable effect on the texture development during ECAP. A relative low ultimate tensile strength of 300 MPa and an improved elongation of 19% were obtained in the processed samples due to strong texture and coarse precipitates. Further optimization should be made by means of impeding the precipitation of the coarse particles before ECAP and decreasing the number of pass and pressing temperature.

Key wordsmetallic materials     AZ80 magnesium alloy    ECAP    precipitation    texture    mechanical properties
收稿日期: 2009-07-29     
基金资助:

国家自然科学基金50571009资助项目。

1 S.R.Agnew, J.A.Horbon, T.M.Lillo, D.W.Brown, Enhanced ductility in strongly texture magnesium produced by equal channel angular processing, Scripta Materialia, 50(3), 377(2004) 2 B.Chen, D.L.Lin, L.Jin, X.Q.Zeng, C.Lu, Equal–channel angular pressing of magnesium alloy AZ91 and its effect on microstructure and mechanical properties, Material Science and Engineering, A483–484, 113(2008) 3 M.Eddahbi, J.A.del Valle, M.T.P´erez–Prado, O.A.Ruano, Comparison of the microstructure and thermal stability of an AZ31 alloy processed by ECAP and large strain hot rolling, Material Science and Engineering, A410–411, 308(2005) 4 M.Janecek, M.Popov, M.G.Krieger, R.J.Hellming, Y.Estrin, Mechanical properties and microstructure of a Mg alloy AZ31 prepared by equal–channel angular pressing, Material Science and Engineering, A462, 116(2007) 5 T.Mukai, M.Yamanoi, H.Watanabe, K.Higashi, Ductility enhancement in AZ31 magnesium alloy by controlling its grain structure, Scripta Materialia, 45(1), 89(2001) 6 A.Yamashita, Z.Horita, T.G.Langdon, Improving the mechanical properties of magnesium and a magnesium alloy through severe plastic deformation, Material Science and Engineering, A300, 142(2001) 7 W.J.Kim, C.W.An, Y.S.Kim, S.I.Hong, Mechanical properties and microstructures of an AZ61 Mg Alloy produced by equal channel angular pressing, Scripta Materialia, 47(1), 39(2002) 8 LU Linlin, YANG Ping, WANG Faqi, ZHONG Weizhen, Effects of thermomechanical treatments on  microstructure and mechanical properties of AZ80 magnesium alloy, The Chinese Journal of Nonferrous Metals, 16(6), 1034(2006) (路林林, 杨 平, 王发奇, 钟伟珍, 形变热处理对AZ80镁合金组织及性能的影响, 中国有色金属学报,  16(6), 1034(2006)) 9 Q.G.Xie, P.Yang, F.E.Cui, Influence of deformation on precipitation and recrystallization in an AZ80 magnesium alloy, Materials Science Forum, 546–549, 293(2007) 10 D.Duly, M.Audier, Y.Brechet, On the influence of plastic deformation on discontinuous precipitation in Mg–Al, Scripta Metallurgica et Materialia, 29(12), 1593(1993) 11 S.Suwas, G.Gottstein, R.Kumar, Evolution of crystallographic texture during equal channel angular extrution (ECAE) and its effects on secondary processing of magnesium, Material Science and Engineering, A471, 1(2007) 12 S.Suwas, L.S.T´oth, J.J.Fundenberger, A.Eberhardt, Texture evolution in commercially pure Al during equal channel angular extrusion (ECAE) as a function of processing routes, Solid State Phenomena, 105, 357(2005) 13 S.Suwas, L.S.T´oth, J.J.Fundenberger, A.Eberhardt, W.Skrotzki, Evolution of crystallographic texture during equal channel angular extrusion of silver, Scripta Materialia, 49(12), 1203(2003) 14 CHENG Yongqi, CHEN Zhenhua, Deformation law of equal channel angular rolling for AZ31 magnesium alloy sheets, Journal of Plasticity Engineering, 14(4), 127(2007) (程永奇, 陈振华, AZ31镁合金板材等径角轧制变形规律研究, 塑性工程学报,  14(4), 127(2007)) 15 Y.Yoshida, L.Cisar, S.Kamado, J.I.Koike, Y.Kojima, Texture development of AZ31 magnesium alloy during ECAE processing, Materials Science Forum, 491–422, 533(2003) 16 S.R.Agnew, P.Mehrotra, T.M.Lillo, G.M.Stoica, P.K.Liaw, Crystallographic texture evolution of three wrought magnesium alloys during equal channel angular extrusion, Material Science and Engineering, A408, 72(2005) 17 M.A.Michael, B.Hugh, ASM Speciality Handbook–Magnesium and Magnesium Alloys (Ohio, ASM International, 1999) p.22 18 Y.B.Li, Y.B.Chen, H.Cui, B.Q.Xiong, J.S.Zhang, Microstructure and mechanical properties of spray–formed AZ91 magnesium alloy, Materials Characterization, 60(3), 240(2009)
[1] 潘新元, 蒋津, 任云飞, 刘莉, 李景辉, 张明亚. 热挤压钛/钢复合管的微观组织和性能[J]. 材料研究学报, 2023, 37(9): 713-720.
[2] 毛建军, 富童, 潘虎成, 滕常青, 张伟, 谢东升, 吴璐. AlNbMoZrB系难熔高熵合金的Kr离子辐照损伤行为[J]. 材料研究学报, 2023, 37(9): 641-648.
[3] 宋莉芳, 闫佳豪, 张佃康, 薛程, 夏慧芸, 牛艳辉. 碱金属掺杂MIL125CO2 吸附性能[J]. 材料研究学报, 2023, 37(9): 649-654.
[4] 赵政翔, 廖露海, 徐芳泓, 张威, 李静媛. 超级奥氏体不锈钢24Cr-22Ni-7Mo-0.4N的热变形行为及其组织演变[J]. 材料研究学报, 2023, 37(9): 655-667.
[5] 邵鸿媚, 崔勇, 徐文迪, 张伟, 申晓毅, 翟玉春. 空心球形AlOOH的无模板水热制备和吸附性能[J]. 材料研究学报, 2023, 37(9): 675-684.
[6] 幸定琴, 涂坚, 罗森, 周志明. C含量对VCoNi中熵合金微观组织和性能的影响[J]. 材料研究学报, 2023, 37(9): 685-696.
[7] 欧阳康昕, 周达, 杨宇帆, 张磊. LPSOMg-Y-Er-Ni合金的组织和拉伸性能[J]. 材料研究学报, 2023, 37(9): 697-705.
[8] 徐利君, 郑策, 冯小辉, 黄秋燕, 李应举, 杨院生. 定向再结晶对热轧态Cu71Al18Mn11合金的组织和超弹性性能的影响[J]. 材料研究学报, 2023, 37(8): 571-580.
[9] 熊诗琪, 刘恩泽, 谭政, 宁礼奎, 佟健, 郑志, 李海英. 固溶处理对一种低偏析高温合金组织的影响[J]. 材料研究学报, 2023, 37(8): 603-613.
[10] 刘继浩, 迟宏宵, 武会宾, 马党参, 周健, 徐辉霞. 喷射成形M3高速钢热处理过程中组织的演变和硬度偏低问题[J]. 材料研究学报, 2023, 37(8): 625-632.
[11] 陈晶晶, 占慧敏, 吴昊, 朱乔粼, 周丹, 李柯. 纳米晶CoNiCrFeMn高熵合金的拉伸力学性能[J]. 材料研究学报, 2023, 37(8): 614-624.
[12] 由宝栋, 朱明伟, 杨鹏举, 何杰. 合金相分离制备多孔金属材料的研究进展[J]. 材料研究学报, 2023, 37(8): 561-570.
[13] 任富彦, 欧阳二明. g-C3N4 改性Bi2O3 对盐酸四环素的光催化降解[J]. 材料研究学报, 2023, 37(8): 633-640.
[14] 王昊, 崔君军, 赵明久. 镍基高温合金GH3536带箔材的再结晶与晶粒长大行为[J]. 材料研究学报, 2023, 37(7): 535-542.
[15] 刘明珠, 樊娆, 张萧宇, 马泽元, 梁城洋, 曹颖, 耿仕通, 李玲. SnO2 作散射层的光阳极膜厚对量子点染料敏化太阳能电池光电性能的影响[J]. 材料研究学报, 2023, 37(7): 554-560.