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材料研究学报  2017, Vol. 31 Issue (10): 796-800    DOI: 10.11901/1005.3093.2016.606
  研究论文 本期目录 | 过刊浏览 |
Ti-6246中α相转变织构的形成机制
赵子博1(), 王国强1,2, 杨晓龙3, 刘建荣1, 李玉兰1, 杨锐1
1 中国科学院金属研究所 沈阳 110016
2 中国科学技术大学材料科学与工程学院 合肥 230026
3 宝钛集团有限公司 宝鸡 721014
Mechanism of α Texture Formation of Ti-6246 Alloy Induced by β Forging Process
Zibo ZHAO1(), Guoqiang WANG1,2, Xiaolong YANG3, Jianrong LIU1, Yulan LI1, Rui YANG1
1 Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2 School of Materials Science and Engineering, University of Science and Technology of China, Hefei 230026, China
3 Baoji Titanium Industry Co., Ltd., Baoji 721014, China
引用本文:

赵子博, 王国强, 杨晓龙, 刘建荣, 李玉兰, 杨锐. Ti-6246中α相转变织构的形成机制[J]. 材料研究学报, 2017, 31(10): 796-800.
Zibo ZHAO, Guoqiang WANG, Xiaolong YANG, Jianrong LIU, Yulan LI, Rui YANG. Mechanism of α Texture Formation of Ti-6246 Alloy Induced by β Forging Process[J]. Chinese Journal of Materials Research, 2017, 31(10): 796-800.

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摘要: 

利用EBSD研究了β单相区锻造Ti-6246饼坯的显微组织和晶体取向。结果表明,β锻造的Ti-6246合金有网篮组织,原始β晶粒沿着金属的流动方向拉长。β相呈现<100>β与饼坯压缩方向平行的强丝织构。次生α相的织构类型与β相符合Burgers取向关系。当相邻原始β晶粒具有相近<110>方向时,在该β/β晶界两侧析出的次生α相的晶体c轴将沿着这一共同的<110>方向,即发生变体选择,导致α相在{0001}极图上的最大织构密度明显高于β相在(110)极图上的最大织构密度。

关键词 金属材料Ti6246织构变体选择    
Abstract

The microstructure and texture of β forged Ti-6246 biscuit were studied using optical microscope (OM) and electron backscattered diffraction (EBSD). It is found that a mesh-basket like microstructure with elongated β-phase grains along the metal flow direction was formed after forging the Ti-6246 biscuit in β-phase state. The β-phase presented a strong <100> fiber texture parallel to the deformation direction. The texture components of transformed α-phase are controlled by the parent β-phase, but the intensity of the transformed α-phase is influenced by variant selection. The variant selection, the α-phase colonies with a common c-axis often situated at the prior β-phase boundary when the neighboring β-phase grains share a common {110} plane, is one of the important reasons for the strengthened α-phase texture intensity.

Key wordsmetallic materials    Ti6246    texture    variant selection
收稿日期: 2016-10-24     
ZTFLH:  TG146  
作者简介:

作者简介 赵子博,男,1986年生,博士生

图1  Ti6246饼坯的显微组织
图2  Ti6246合金饼坯的菊池线衬度图以及α相和β相的取向图
图3  EBSD测得图2a标记区域内同一原始β晶粒内α相和β相的极图
图4  Ti6246饼坯β相和α相的极图
图5  Ti6246合金中的变体选择
图6  计算所得无变体选择时α相的织构
[1] Whittaker M T, Evans W J, Hurley P J, et al., Prediction of notched specimen behaviour at ambient and high temperatures in Ti6246[J]. Int. J. Fatigue, 2007, 29(9-11): 1716
[2] Qiu J, Feng X, Ma Y, et al., Fatigue crack growth behavior of beta-annealed Ti-6Al-2Sn-4Zr-xMo (x=2, 4 and 6) alloys: Influence of microstructure and stress ratio[J]. Int. J. Fatigue 83, Part 2(2016): 150
[3] Pederson R, Niklasson F, Skystedt F, et al., Microstructure and mechanical properties of friction- and electron-beam welded Ti-6Al-4V and Ti-6Al-2Sn-4Zr-6Mo[J]. Mater Sci. Eng. A, 2012, 552: 555
[4] Qiu J, Ma Y, Lei J, et al., A comparative study on dwell fatigue of Ti-6Al-2Sn-4Zr-xMo(x=2 to 6) alloys on a microstructure-normalized basis[J]. Metallurgical and Materials Transactions A, 2014, 45(13): 6075
[5] Corre S L, Forestier R, Brisset F, et al., Influence of β-forging on texture development in Ti 6246 alloy[A]. Proceedings of the 13th World Conference on Titanium[C]. John Wiley & Sons, Inc. 2016, pp. 757
[6] Gerland M, Lefranc P, Doquet V, et al., Deformation and damage mechanisms in an α/β 6242 Ti alloy in fatigue, dwell-fatigue and creep at room temperature. Influence of internal hydrogen[J]. Mater Sci. Eng. A, 2009, 507(1-2): 132
[7] Hagiwara M, Emura S, Blended elemental P/M synthesis and property evaluation of Ti-1100 alloy[J]. Mater Sci. Eng. A, 2003, 352(1-2): 85
[8] L. Mendia, Estensoro F J, Mary C, et al., ffect of combined cycle fatigue on Ti6242 fatigue strength, Procedia Engineering, 2011, 10: 1809
[9] Yang W G, Wang Q J, Zhang C B, et al.Evaluation of tensile strength of BT25Y titanium alloy in terms of equivalents[J]. Acta Metall, 2004, 40(2): 155(杨卫国,王青江,张彩碚等BT25Y钛合金拉伸强度的当量计算[J]. 金属学报, 2004, 40(2): 155-158)
[10] Zhao Z B, Wang Q J, Hu Q M, et al., Effect of β (110) texture intensity on α-variant selection and microstructure morphology during β→α phase transformation in near α titanium alloy[J]. Acta Mater., 2017, 126: 372
[11] Zhao Z B, Wang Q J, Liu J R, et al., Texture of Ti60 alloy precision bars and its tensile properties[J]. Acta Metall., 2015, 51(5): 561
[12] Wang Y N, Huang J C, Texture analysis in hexagonal materials[J]. Mater. Chem. Phys., 2003, 81(1): 11
[13] Birosca S, Buffiere J Y, Karadge M, et al., 3-D observations of short fatigue crack interaction with la2mellar and duplex microstructures in a two-phase titanium alloy[J]. Acta Mater., 2011, 59(4): 1510
[14] Germain L, Gey N, Humbert M, et al., Analysis of sharp microtexture heterogeneities in a bimodal IMI 834 billet[J]. Acta Mater., 2005, 53(13): 3535
[15] Roy S, Suwas S, Tamirisakandala S, et al., Development of solidification microstructure in boron-modified alloy Ti-6Al-4V-0.1B[J]. Acta Mater., 2011, 59(14): 5494
[16] Bhattacharyya D, Viswanathan G B, Denkenberger R, et al., The role of crystallographic and geometrical relationships between α and β phases in an α/β titanium alloy[J]. Acta Mater., 2003, 51(16): 4679
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