碳纤维<strong>/</strong>铝复层材料的组织和力学性能

doi:10.11901/1005.3093.2021.421

材料研究学报

2022, Vol. 36

Issue (7): 536-544 DOI: 10.11901/1005.3093.2021.421

研究论文

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碳纤维/铝复层材料的组织和力学性能

王艳坤¹, 王宇¹(

), 纪伟², 王智慧², 彭翔飞¹, 呼宇雄¹, 刘斌¹, 徐宏¹, 白培康¹

^1.中北大学材料科学与工程学院太原 030000
^2.内蒙古金属材料研究所烟台 264000

Microstructure and Mechanical Properties of Carbon Fiber/Aluminum Laminated Composites

WANG Yankun¹, WANG Yu¹(

), JI Wei², WANG Zhihui², PENG Xiangfei¹, HU Yuxiong¹, LIU Bin¹, XU Hong¹, BAI Peikang¹

^1.School of materials science and engineering, North University of China, Taiyuan 030000, China
^2.Inner Mongolia Metal Material Research Institute, Yantai 264000, China

引用本文:

王艳坤, 王宇, 纪伟, 王智慧, 彭翔飞, 呼宇雄, 刘斌, 徐宏, 白培康. 碳纤维/铝复层材料的组织和力学性能[J]. 材料研究学报, 2022, 36(7): 536-544.
Yankun WANG, Yu WANG, Wei JI, Zhihui WANG, Xiangfei PENG, Yuxiong HU, Bin LIU, Hong XU, Peikang BAI. Microstructure and Mechanical Properties of Carbon Fiber/Aluminum Laminated Composites[J]. Chinese Journal of Materials Research, 2022, 36(7): 536-544.

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摘要:

在1060系铝基体表面镀镍碳纤维作为增强体,进行真空热压扩散制备出碳纤维/铝复层材料。研究了制备工艺参数(加热温度、保温时间、压力大小)和碳纤维体积分数对碳纤维/铝复层材料的微观组织、界面结合、性能强度和断口形貌的影响。结果表明：碳纤维与铝基体界面结合良好,镀镍层与铝基体在碳纤维附近反应生成的Al₃Ni阻止了铝基体与碳纤维之间生成脆性相Al₄C。随着碳纤维体积分数的提高,材料的抗弯强度先提高后降低。

关键词 ：复合材料, 碳纤维/铝复层材料, 三点弯曲, 制备工艺, 界面微观结构

Abstract：

Carbon fibre-reinforced aluminium laminates was prepared by vacuum hot pressing diffusion with 1060 series aluminum as matrix and nickel plated carbon fiber as reinforcement in this paper. The effects of preparation parameters (heating temperature, holding time, pressure) and carbon fiber volume fraction on the microstructure, interfacial bonding, mechanical strength and fracture morphology of Carbon fibre-reinforced aluminium laminates were investigated. The results show that the interface between carbon fiber and aluminum matrix is well bonded, and the nickel coating and aluminum matrix react near the carbon fiber to form Al₃Ni, which effectively prevents the formation of brittle phase Al4C between aluminum matrix and carbon fiber. With the increase of carbon fiber volume fraction, the bending strength first increases and then decreases.

Key words： composites carbon fiber/aluminum laminated composites three point bending fabrication process interface microstructure

收稿日期: 2021-07-26

ZTFLH:

TB333

基金资助:山西省面上青年基金(201801D221148);山西省高等学校科技创新项目(2020L0319);国防科工局稳定支持经费专项-兵器五五所开放创新项目(JB11-12);安徽省重点研究与开发计划(202004A05020070);山西省重点研发计划国际科技合作项目(201903D421080)

作者简介: 王艳坤,男,1996年生,硕士

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	王艳坤
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	王智慧
	彭翔飞
	呼宇雄
	刘斌
	徐宏
	白培康
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https://www.cjmr.org/CN/10.11901/1005.3093.2021.421 或 https://www.cjmr.org/CN/Y2022/V36/I7/536

表1 1060铝的成分(质量分数,%)

表2 碳纤维的性能(质量分数,%)

表3 N02201镍的成分

图1 镀镍碳纤维的SEM照片[21]和碳纤维毡

表4 碳纤维增强铝基复合材料的制备工艺参数

图2 碳纤维/铝复层材料试样的宏观照片

图3 碳纤维/铝复层材料试样的微观组织

图4 碳纤维/铝复层材料试样的微观组织

图5 碳纤维/铝复层材料试样的EDS谱

图6 碳纤维/铝复层材料试样的EDS谱

表5 EDS测量成分数据表

表6 EDS测量成分数据表

图7 碳纤维/铝复层材料试样的XRD谱

图8 烧结试样的密度

图9 烧结试样的三点抗弯结果

图10 630℃、100 min、21 MPa下不同纤维含量试样的三点抗弯图

图11 碳纤维/铝复层材料试样的断口形貌图谱(a)、(b) 0.2 mm Al、4层纤维 (c)、(d) 0.1 mm Al、4层纤维

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