时效工艺对AerMet100钢强韧性能的影响*

doi:10.11901/1005.3093.2015.624

材料研究学报

2016, Vol. 30

Issue (11): 819-824 DOI: 10.11901/1005.3093.2015.624

论文

本期目录 | 过刊浏览

时效工艺对AerMet100钢强韧性能的影响*

王鑫,董洪波(

),袁大庆,邹忠波,王明主

南昌航空大学南昌 330063

Effect of Aging Process on Strength and Toughness of AerMet100 Steel

Xin WANG,Hongbo DONG(

),Daqing YUAN,Zongbo ZOU,Mingzhu WANG

Nanchang Hangkong University, Nanchang 330063, China

引用本文:

王鑫, 董洪波, 袁大庆, 邹忠波, 王明主. 时效工艺对AerMet100钢强韧性能的影响*[J]. 材料研究学报, 2016, 30(11): 819-824.
Xin WANG, Hongbo DONG, Daqing YUAN, Zongbo ZOU, Mingzhu WANG. Effect of Aging Process on Strength and Toughness of AerMet100 Steel[J]. Chinese Journal of Materials Research, 2016, 30(11): 819-824.

全文: PDF(4499 KB) HTML

摘要:

采用正常时效、预时效+正常时效、双时效等多种时效工艺对热锻后的AerMet100钢进行热处理, 研究时效工艺对AerMet100钢回火组织及力学性能的影响。结果表明: 正常时效处理后AerMet100钢的抗拉强度较高(1978 MPa), 但是冲击韧性较低(冲击功74J); 双时效处理后冲击韧性较高(冲击功102J), 但是抗拉强度较低(1662 MPa); 经过预时效+正常时效(510℃×30 min, +482℃×5 h)处理得到优良的强韧性能, 其抗拉强度为1946 MPa, 冲击功为104 J。强韧性提高的原因是: 510℃预时效促进了C原子扩散, 提高了膜状逆转奥氏体含量及其稳定性, 有利于韧性的改善; 同时, 预时效保温时间短(≤30 min), 析出相M₂C未与基体脱离共格关系, 析出的强化作用提高了强度。

关键词 ：金属材料, 二次硬化钢, 预时效, 力学性能, 逆转变奥氏体, 析出强化

Abstract：

The effect of aging processes on the tempered microstructure and mechanical properties of the forged AerMet100 steel was investigated, while the named processes include normal aging, pre-aging + normal aging and double aging etc. The results show that high tensile strength (1978 MPa) with low impact toughness (A_K=74 J) can be obtained by the normal aging process; higher impact toughness (impact energy 102 J) can be obtained by double aging process, but tensile strength is lower (1662 MPa); however, excellent strength and toughness (σ_b=1946 MPa; A_K=104 J) can be obtained by pre aging + normal aging (510℃×30 min, OQ+482℃×5 h, AC) process. The improvment of strength and toughness can be attribute to that the 510℃ pre aging could promote the C atom diffusion, therewith increased the amount and the stability of the flim-like reversed austenite; besides enable the M₂C precipitate to maintain a good lattice relationship with the matrix induced by the short time (≤30 min) pre aging, therefore the precipitation strengthening effect was enhanced.

Key words： metallic materials secondary hardening steel pre aging mechanical property reversed austenite precipitation strengthening

收稿日期: 2015-12-03

基金资助:* 国家自然科学基金项目51164029、航空科学基金2015ZE56011和江西省科学计划项目20151BBE50042资助

	服务

	把本文推荐给朋友
	加入引用管理器
	E-mail Alert
	RSS
	作者相关文章
	王鑫
	董洪波
	袁大庆
	邹忠波
	王明主
44.8K

链接本文:

https://www.cjmr.org/CN/10.11901/1005.3093.2015.624 或 https://www.cjmr.org/CN/Y2016/V30/I11/819

表1 AerMet100钢的化学成分

表2 AerMet100钢热处理方案(OQ, 油淬; AC, 空冷)

表3 不同时效工艺处理后AerMet100钢的力学性能

图1 不同时效工艺AerMet100钢冲击断口的宏观和微观形貌

图2 不同时效工艺AerMet100钢的XRD图谱

图3 AerMet100钢在200-600℃的平衡相热力学计算结果(a) 平衡相体积分数与温度的关系 (b) 奥氏体中元素含量与温度的关系

图4 时效后逆转变奥氏体的TEM明场像

图5 预时效+正常时效后析出相M2C的明场像

1	WAN Ru, Aermet100 ultrahigh-strength steel with the unique combination of properties, Journal of Beijing University of Aeronautics and Astronautics, 22(6), 639(1996)
1	(万如, AerMet100—极好综合性能的超高强度钢, 北京航空航天大学学报, 22(6), 639(1996))
2	Koji Sato, Improving the toughness of ultrahigh strength steel, PhD Thesis, (USA, Berkeley, University of California, 2002)
3	R Ayer, P M Machmeier, Transmission of electron microscopy examination of hardening and toughening phenomena in Aermet100, Metallurgical Transactions A, 24, 1943(1993)
4	R Ayer, P. M. Machmeier, On the characteristics of M2C carbides in the peak hardening regime of aerMet 100 steel, Metallurgical Transactions A, 29A(3), 903(1998)
5	PENG Wenwen, ZENG Weidong, YAN Wenqiao, KANG Chao, WANG Tengfei, Effect of tempering process on microstructure and toughness of AerMet100 ultrahigh strength steel, Transactions of Materials and Heat Treatment, 34(6), 58(2013)
5	(彭雯雯, 曾卫东, 闫文巧, 康超, 王腾飞, 回火工艺对Aermet100 超高强度钢组织与韧性的影响, 材料热处理学报, 34(6), 58(2013))
6	LI Jie, GU Lixin, LI Zhi, WANG Junli, GUO Feng, Tempering temperature sensitivity of mechanical properties for AerMet100 steel, Heat Treatment of Metals, 35(3), 33(2010)
6	(李杰, 古立新, 李志, 王俊丽, 郭峰, AerMet100钢力学性能的回火温度敏感性研究, 金属热处理, 35(3), 33(2010))
7	Wang L D, Jiang L Z, Zhu M, Combining strength and toughness in ultrahigh strength steel, Journal of Physics D: Applied Physics, 37, 2151(2004)
8	LIANG Jinkui, WANG Liuding, LI Zhi, WANG Baimin, DING Fucai, Refinement of effective grain and enhancement of reverted austenite stability for AerMet100 steel, Transactions of Materials and Heat Treatment, 31(5), 57(2010)
8	(梁锦奎, 王六定, 李志, 王佰民, 丁富才, AerMet100有效晶粒细化与逆转变奥氏体稳定性的提高, 材料热处理学报, 31(5), 57(2010))
9	Z. F. Hu, X. F. Wu, High resolution electron microscopy of precipitates in high Co-Ni alloy steel, Micron, 34, 19(2003)
10	GAO Kuan, WANG Liuding, ZHU Ming, Improving the grain refinement and toughness of low alloy ultra high strength bainitic steel, Acta Metallurgica Sinica, 43, 315(2007)
10	(高宽, 王六定, 朱明, 低合金超高强度贝氏体钢的晶粒细化与韧性提高, 金属学报, 43, 315(2007))
11	XU Zhuyao, Martensitic transformation and martensite (Beijing Science Press, 1999)
11	(徐祖耀, 马氏体相变与马氏体(北京, 科学出版社, 1999))
12	LING Bin, ZHONG Ping, ZHONG Bingwen, ZHAO Zhenye, On the strengthening mechanism of high Co-Ni Ultrahigh strength steel, Acta Aeronautica Et Astronautica Sinica, 18(1), 44(1997)
12	(凌斌, 钟平, 钟炳文, 赵振业, 新型二次硬化高Co-N i超高强度钢强韧化机制的研究, 航空学报, 18(1), 44(1997))
13	CHEN Ding, CHEN Jihua, YAN Hongge, HUANG Peiyun, Mechanism & industrial applications of cryogenic treatment, Ordnance Material Science and Engineering, 26(3), 68(2003)
13	(陈鼎, 陈吉华, 严红革, 黄培云, 深冷处理原理及其在工业上的应用, 兵器材料科学与工程, 26(3), 68(2003))
14	ZHAO Zhenye, Studing status on the secondary hardening phenomenon in ultra-high strength steels , Journal of Aeronautical Materials, 22(4), 46(2002))
14	(赵振业, 超高强度钢中二次硬化现象研究, 航空材料学报, 22(4), 46(2002))
15	LI Jie, LI Chunzhi, GUO Feng, LI Zhi, YAN Ningao, HRTEM study of strengthening precipitates of secondary hardening ultra-high strength steel, Journal of Aeronautical Materials, 28(4), 1(2008)
15	(李杰, 李志春, 郭峰, 李志, 颜宁皋, 二次硬化超高强度钢中析出强化相HRTEM研究, 航空材料学报, 28(4), 1(2008))
16	LI Jie, SUN Feng, LI Chunzhi, GUO Feng, LI Zhi, YAN Ningao, Analysis of strengthening precipitates of high Co-Ni ultra-high strength steel,Journal of Material engineering, (7), 1(2009)
16	(李杰, 孙枫, 李春志, 郭峰, 李志, 颜宁皋, 高Co-Ni 超高强度钢强化析出相的微观分析, 材料工程, (7), 1(2009))
17	HU Zhengfei, WU Xingfang, WANG Chunxu, Coarsening kinetics of multi-component M2C precipitates in secondary hardening alloy steels, Acta Metallurgica Sinica, 39(6), 585(2003)
17	(胡正飞, 吴杏芳, 王春旭, 二次硬化合金钢中多组元强化相屿碳化物的粗化动力学研究, 金属学报, 39(6), 585(2003))

[1]	毛建军, 富童, 潘虎成, 滕常青, 张伟, 谢东升, 吴璐. AlNbMoZrB系难熔高熵合金的Kr离子辐照损伤行为[J]. 材料研究学报, 2023, 37(9): 641-648.
[2]	宋莉芳, 闫佳豪, 张佃康, 薛程, 夏慧芸, 牛艳辉. 碱金属掺杂MIL125的CO₂ 吸附性能[J]. 材料研究学报, 2023, 37(9): 649-654.
[3]	赵政翔, 廖露海, 徐芳泓, 张威, 李静媛. 超级奥氏体不锈钢24Cr-22Ni-7Mo-0.4N的热变形行为及其组织演变[J]. 材料研究学报, 2023, 37(9): 655-667.
[4]	邵鸿媚, 崔勇, 徐文迪, 张伟, 申晓毅, 翟玉春. 空心球形AlOOH的无模板水热制备和吸附性能[J]. 材料研究学报, 2023, 37(9): 675-684.
[5]	幸定琴, 涂坚, 罗森, 周志明. C含量对VCoNi中熵合金微观组织和性能的影响[J]. 材料研究学报, 2023, 37(9): 685-696.
[6]	欧阳康昕, 周达, 杨宇帆, 张磊. 含LPSO相Mg-Y-Er-Ni合金的组织和拉伸性能[J]. 材料研究学报, 2023, 37(9): 697-705.
[7]	潘新元, 蒋津, 任云飞, 刘莉, 李景辉, 张明亚. 热挤压钛/钢复合管的微观组织和性能[J]. 材料研究学报, 2023, 37(9): 713-720.
[8]	徐利君, 郑策, 冯小辉, 黄秋燕, 李应举, 杨院生. 定向再结晶对热轧态Cu71Al18Mn11合金的组织和超弹性性能的影响[J]. 材料研究学报, 2023, 37(8): 571-580.
[9]	熊诗琪, 刘恩泽, 谭政, 宁礼奎, 佟健, 郑志, 李海英. 固溶处理对一种低偏析高温合金组织的影响[J]. 材料研究学报, 2023, 37(8): 603-613.
[10]	刘继浩, 迟宏宵, 武会宾, 马党参, 周健, 徐辉霞. 喷射成形M3高速钢热处理过程中组织的演变和硬度偏低问题[J]. 材料研究学报, 2023, 37(8): 625-632.
[11]	陈晶晶, 占慧敏, 吴昊, 朱乔粼, 周丹, 李柯. 纳米晶CoNiCrFeMn高熵合金的拉伸力学性能[J]. 材料研究学报, 2023, 37(8): 614-624.
[12]	由宝栋, 朱明伟, 杨鹏举, 何杰. 合金相分离制备多孔金属材料的研究进展[J]. 材料研究学报, 2023, 37(8): 561-570.
[13]	任富彦, 欧阳二明. g-C₃N₄ 改性Bi₂O₃ 对盐酸四环素的光催化降解[J]. 材料研究学报, 2023, 37(8): 633-640.
[14]	王昊, 崔君军, 赵明久. 镍基高温合金GH3536带箔材的再结晶与晶粒长大行为[J]. 材料研究学报, 2023, 37(7): 535-542.
[15]	刘明珠, 樊娆, 张萧宇, 马泽元, 梁城洋, 曹颖, 耿仕通, 李玲. SnO₂ 作散射层的光阳极膜厚对量子点染料敏化太阳能电池光电性能的影响[J]. 材料研究学报, 2023, 37(7): 554-560.

Viewed

Full text

Abstract

Cited

Shared

Discussed