Preparation and Characterization of Totally Encapsulated Microcapsules of Jasmine Fragrance

doi:10.11901/1005.3093.2015.484

Chinese Journal of Materials Research

2017, Vol. 31

Issue (1): 27-31 DOI: 10.11901/1005.3093.2015.484

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Preparation and Characterization of Totally Encapsulated Microcapsules of Jasmine Fragrance

Xiaoqiu SONG(

),Yuping DUAN

(School of Perfume and Aroma Technology, Shanghai Institute of Technology, Shanghai, 201418, China)

Cite this article:

Xiaoqiu SONG,Yuping DUAN. Preparation and Characterization of Totally Encapsulated Microcapsules of Jasmine Fragrance. Chinese Journal of Materials Research, 2017, 31(1): 27-31.

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Abstract

Totally encapsulated microcapsules of jasmine fragrance were prepared by in situ polymerization with melamine resin as wall material and inorganic nanometer silicon dioxide as surface modifier. The morphology, chemical composition, structure and embedding rate of the prepared microcapsules were characterized by scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) spectrometric test, thermo gravimetric analysis (TG-DTG). Results show that the totally encapsulated microcapsules of jasmine fragrance present a core-shell structure with the capsule shell of good tightness and an embedding rate of 18%.

Key words: inorganic non-metallic materials Jasmine fragrance nano silica melamine resin in situ polymerization totally encapsulated microcapsules

Received: 18 December 2015

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https://www.cjmr.org/EN/10.11901/1005.3093.2015.484 OR https://www.cjmr.org/EN/Y2017/V31/I1/27

Fig.1 FT-IR of fragrance microcapsules、melamine resin-SiO₂、fragrance

Fig.2 SEM images of totally encapsulated jasmine fragrance microcapsules

Fig.3 TGA diagrams (a) Melamine resin, (b) fragrance microcapsules

Fig.4 Alcoholic solution of jasmine fragrance UV absorbance spectrum

Fig.5 Curve of absorbance and fragrance concentration relation

Fig.6 Curve of soak time-absorbance of fragrance microcapsules soak with ethyl alcohol

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