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Chinese Journal of Materials Research  2015, Vol. 29 Issue (1): 45-50    DOI: 10.11901/1005.3093.2014.238
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Preparation of Ag-glass Fiber Composite by Plasma Treatment-continuous Immersion
Ping LU(),Xiao CHEN,Ming YANG
Research Center for Analysis and Measurement, Donghua University, Shanghai 201620, China
Cite this article: 

Ping LU,Xiao CHEN,Ming YANG. Preparation of Ag-glass Fiber Composite by Plasma Treatment-continuous Immersion. Chinese Journal of Materials Research, 2015, 29(1): 45-50.

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Abstract  

A Ag-glass fiber composite was prepared by a two step process i.e. the glass fibers were pre-plasma treated and then dipped in a nano-Ag suspension. Results of SEM, AFM and XRD examinations indicate that Ag coating on the glass fiber has good overall properties with well uniform appearance. In comparison with the conventional electroless plating method, the present approach is novel and facile. After the oxygen plasma treatment of glass fibers, multiple active hydroxyl groups on its surface exhibit strong adsorption capacity to Ag. The coating thickness could be easily adjusted by the dipping time. Moreover, there exist abundant Ag particles with high specific surface energy on the surface of the prepared Ag-glass fibers.

Key words:  composites      glass fiber      Ag coating      plasma      atomic force microscope     
Received:  09 May 2014     
Fund: *Supported by National Nature Science Foundation of China No. 51373030.

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2014.238     OR     https://www.cjmr.org/EN/Y2015/V29/I1/45

Fig.1  The Field-Emission Scanning Electron Microscope (FE-SEM) images of the pristine glass fiber
Fig.2  The Atomic Force Microscope (AFM) images of the pristine glass fiber
Fig.3  The EDS spectrum of the pristine glass fiber (left). The FT-IR spectrum of glass fiber before (a) and after (b) O2 plasma processing (right)
Fig.4  The reaction scheme of the Ag-glass fiber
Fig.5  The FE-SEM images of the Ag-glass fiber after spin coating in the Ag ethanol solution
Fig.6  The FE-SEM images of Ag coated glass fiber with different coating times 15 min (a), 30 min (b) and 45 min (c) respectively
Fig.7  The EDS mapping spectra of the Ag-glass fiber composite
Fig.8  The AFM iamges of the Ag-glass fiber composite
Fig.9  The X-Ray Diffraction (XRD) spectra of pristine glassfiber (a) and Ag-glassfiber composite (b)
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