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Chin J Mater Res  2010, Vol. 24 Issue (3): 322-326    DOI:
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Oxalate-induced Synthesis and Growth Mechanism of PbWO4 Ordered Nanostructures
FANG Yi, ZHOU Yuanlin, XIONG Ying, FANG Gang
State Key Laboratory Cultivation Base for Nonmetal Composite and Functional Materials, Southwest University of Science and Technology, Mianyang 621010
Cite this article: 

FANG Yi ZHOU Yuanlin XIONG Ying FANG Gang. Oxalate-induced Synthesis and Growth Mechanism of PbWO4 Ordered Nanostructures. Chin J Mater Res, 2010, 24(3): 322-326.

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Abstract  

Ordered PbWO4 nanostructures were synthesized by a direct precipitation method, and the oxalate anions with double carboxyl were employed as structure-directing agents in the growth stage of PbWO4 nanocrystals. The PbWO4 nanostructures were characterized by X-ray power diffraction (XRD), scanning electron microscopy (SEM), infra-red spectrum (IR) and transmission electron microscopy (TEM). The control role of the oxalate anions in the growth stage of PbWO4 nanocrystals was investigated and formation mechanism of the ordered PbWO4 nanocrystals was proposed.

Key words:  inorganic non-metallic materials        lead tungstate       oxalate       controlled-synthesis       ordered nanostructures     
Received:  29 October 2009     
ZTFLH: 

O781

 
Fund: 

Supported by project co-funded of Natural Foundation of China-Chinese Academy of Engineering Physics No.10876033.

URL: 

https://www.cjmr.org/EN/     OR     https://www.cjmr.org/EN/Y2010/V24/I3/322

[1] Y.Liu, Y.Chu, Y.J.Zhuo, M.Y.Li, L.L.Li, L.H.Dong, Anion-controlled construction of CuO honeycombs and flowerlike assemblies on copper foils, Crystal Growth & Design, 3, 467(2007)
[2] T.Z.Ramon, E.Jamil, L.C.Claude, B.Chegnui, V.Tobias, M.S.Ivan, B.Juan, Influence of the potassium chloride concentration on the physical properties of electrodeposited ZnO nanowire arrays, J. Phys. Chem. C, 112, 16318(2008)
[3]T.Herricks, J.Y.Chen, Y.N.Xia, Polyol synthesis of platinum nanoparticles: control of morphology with sodium nitrate, Nano Lett., 12, 2367(2004)
[4]B.Wiley, T.Herricks, Y.G.Sun, Y.N.Xia, Polyol synthesis of silver nanoparticles use of chloride and oxygen to promote the formation of single-crystal, truncated cubes and tetrahedrons, Nano Lett., 9, 1733(2004)
[5] C.Z.Wu, P.Yin, X.Zhu, C.Z.OuYang, Y.Xie, Synthesis of hematite (α–Fe2O3) nanorods: diameter-size and shape effects on their applications in magnetism, lithium ion battery, and gas sensors, J. Phys. Chem B, 110, 17806(2006)
[6] A.A.Annenkov, M.V.Korzhik, P.Lecoq, Lead tungstate scinitillation material, Nucl. Instrum. Methods Phys. Res. A, 490, 30(2002)
[7] Y.Zhang, N.A.W.Holzwarth, R.T.Williams, Electronic band structures of the scheelite materials CaMoO4, CaWO4, PbMoO4 and PbWO4, Phys. Rev. B, 57, 12738(1998)
[8] Y.H.Chen, C.S.Shi, G.Q.Hu, Influence of Sb doping on the luminescent properties of PbWO4 single crystals, J. Appl. Phys, 87, 1503(2000)
[9] W.Zhao, X.Y.Song, G.Z.Chen, G.R.Tian, S.X.Sun, Hydrothermal synthesis of PbWO4 uniform hierarchical microspheres, Materials Letters, 63, 285(2009)
[10] B.Liu, S.H.Yu, L.J.Li, Q.Zhang, F.Zhang, K.Jiang, Morphology control of stolzite microcrystals with high hierarchy in solution, Angew Chem., Int. Ed, 43, 4745(2004)
[11] X.Y.He, M.H.Cao, Synthesis and characterization of PbCrO4 and PbWO4 nanorods, Nanotechnology, 17, 3139(2006)
[12] J.Geng, J. J.Zhu, D.J.Lu, H.Y.Chen, Sonochemical Preparation of Luminescent PbWO4 Nanocrystalswith Morphology Evolution, Cryst. Growth Des, 6, 321(2006)
[13] G.J.Zhou, M.K.Lv, B.Y.Su, F.Gu, Z.L.Xiu, S.F.Wang, Preparation and characterization of luminescent PbWO4 nano- and macrostructure, Optical Materials, 28, 1385(2006)
[14] A.W.Burton, K.Ong, T.Rea, I.Y.Chan, On the estimation of average crystallite size of zeolites from the scherrer equation: A critical evaluation of its application to zeolites with one-dimensional pore systems, Microporous and Mesoporous Materials, 117, 75(2009)
[15] S.W.Liu, J.G.Yu, X.F.Zhao, B.Cheng, Effects of polyvinylpyrrolidone and cetyltrimethy lammonium bromide on morphology of lead tungstate particles, Journal of Alloys and Compounds, 433, 73(2007)
[16] Y.Yang, R.Scholz, H.J.Fan, D.Hess, U.Gosele, M.Zacharias, Multitwinned spinel nanowires by assembly of nanobricks via oriented attachment:a case study of Zn2TiO4, ACS Nano, 3, 555(2009)

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