Recrystallization and Grain Growth Behavior for Strip and Foil of Ni-based Superalloy GH3536

doi:10.11901/1005.3093.2022.417

Chinese Journal of Materials Research

2023, Vol. 37

Issue (7): 535-542 DOI: 10.11901/1005.3093.2022.417

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Recrystallization and Grain Growth Behavior for Strip and Foil of Ni-based Superalloy GH3536

WANG Hao¹^,², CUI Junjun¹^,², ZHAO Mingjiu¹^,²(

)

^1.CAS Key Laboratory of Nuclear Materials and Safety Assessment, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
^2.School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China

Cite this article:

WANG Hao, CUI Junjun, ZHAO Mingjiu. Recrystallization and Grain Growth Behavior for Strip and Foil of Ni-based Superalloy GH3536. Chinese Journal of Materials Research, 2023, 37(7): 535-542.

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Abstract

The microstructure and crystallographic structure characteristics of as cold-rolled strip and foil with different thicknesses of GH3536 alloy after annealing was investigated by optical microscope (OM), scanning electron microscope (SEM), transmission electron microscope (TEM) and X-ray diffractometer (XRD) to get an insight into the recrystallization and grain growth behavior. The results show that the cold rolled strip and foil of GH3536 alloy show a microstructure composed of elongated grains along the rolling directions, and its main phase was γ. The grain growth equations of the strip and foil with thicknesses of 200,100 and 50 μm annealed at 1050~1150℃ for 10~60 min were established respectively, and the relevant activation energies were acquired as follows: Q_{200 μm}=800.34 kJ/mol, Q_{100 μm}=609.50 kJ/mol and Q_{50 μm}=314.79 kJ/mol. The activation energy of the thinner strip and foil was smaller, and the grain growth was more prone to occur. The main factors affecting the grain growth were related to deformation degree and precipitated particles.

Key words: metallic materials Ni-base superalloy strip and foil recrystallization grain growth behaviors

Received: 28 July 2022

ZTFLH:

TG132.32

Fund: National Natural Science Foundation of China and China Academy of Engineering Physics(U1730140)

Corresponding Authors: ZHAO Mingjiu, Tel: (024)23975662, E-mail:mjzhao@imr.ac.cn

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https://www.cjmr.org/EN/10.11901/1005.3093.2022.417 OR https://www.cjmr.org/EN/Y2023/V37/I7/535

Table 1 Chemical composition of experimental GH3536 superalloy strip and foil (%, mass fraction)

Fig.1 Surface morphologies of cold-rolled state GH3536 superalloy strip and foil with thicknesses of 200 μm (a), 100 μm (b) and 50 μm (c)

Fig.2 Microstructure (a) and chemical analysis of matrix (b) and precipitation (c) with SEM-EDS of GH3536 superalloy with a thickness of 200 μm

Table 2 EDS analysis of matrix and particles on the GH3536 superalloy with a thickness of 200 μm (%, mass fraction)

Fig.3 XRD patterns of cold-rolled state GH3536 superalloy strip and foil with different thicknesses

Fig.4 Optical microstructures of GH3536 superalloy strip and foil annealing at 1050℃ (200 μm (a), 100 μm (b), 50 μm (c)), 1080℃ (200 μm (d), 100 μm (e), 50 μm (f)), 1100℃ (200 μm (g), 100 μm (h), 50 μm (i)), 1150℃ (200 μm (j), 100 μm (k), 50 μm (l))

Fig.5 XRD patterns of GH3536 superalloy strip and foil annealed at 1150℃ for 20 min with different thicknesses

Fig.6 Logarithmic plots of lnt-lnD of GH3536 superalloy strip and foil with thicknesses of 200 μm (a), 100 μm (b) and 50 μm (c)

Table 3 Grain growth equation of GH3536 superalloy strip and foil

Fig.7 Logarithmic plots of 1000/T-lnK of GH3536 superalloy strip and foil with thicknesses of 200 μm (a), 100 μm (b) and 50 μm (c) annealed at 1050~1150℃ and with a thickness of 200 μm (d) annealed at 1080~1150℃

Fig.8 BSE images of GH3536 superalloy with thick-nesses of 200 μm (a), 100 μm (b) and 50 μm (c) annealed at 1050℃

Fig.9 TEM morphologies and the electron diffraction patterns of the precipitates of GH3536 superalloy with a thickness of 100 μm annealed at 1100℃ (a) and 1150℃ (b)

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