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Chinese Journal of Materials Research  2021, Vol. 35 Issue (5): 381-393    DOI: 10.11901/1005.3093.2020.249
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Microstructure and Recrystallization Behavior of 18.5%Cr High-Mn Low-Ni Type Duplex Stainless Steel during Hot Compression with Large Deformation
PAN Xiaoyu, YANG Yinhui(), NI Ke, CAO Jianchun, QIAN Hao
School of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, China
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PAN Xiaoyu, YANG Yinhui, NI Ke, CAO Jianchun, QIAN Hao. Microstructure and Recrystallization Behavior of 18.5%Cr High-Mn Low-Ni Type Duplex Stainless Steel during Hot Compression with Large Deformation. Chinese Journal of Materials Research, 2021, 35(5): 381-393.

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Abstract  

The 18.5% Cr low nickel type duplex stainless steel with high manganese content was compressed by using thermal simulation test machine with large deformation of 70% under deformation conditions of 1123~1423 K/0.01~0.1 s-1, while the microbstructure characteristics and softening mechanism of two phases during thermal deformation were investigated. The results show that the thermal compression softening in the range of 0.01~0.1 s-1/1123~1223 K was dominated by recrystallization of ferrite phase, while in the range of 0.1 s-1/1323~1423 K and 10 s-1/1223 K was dominated by recrystallization of austinite phase. When deformed at 1223 K and 0.01~10 s-1, the dislocation tangles in the ferrite phase evolved into dislocation cells and the dislocation lines appeared with the increase of strain rate, and the substructure of austenite phase transformed into fine recrystallized grains. When deformed at 0.1 s-1 and 1123~1323 K the substructure of the dislocation cells gradually formed due to the increase of dislocation density in ferrite phase with increasing deformation temperature, but the deformation microstructure in austenite phase changed from DRV to DRX with the decrease of dislocation density. The deformation apparent activation energy Q and the apparent stress exponent n were calculated as 514.29 kJ/mol and 7.13 respectively based on thermal deformation equation, and the constitutive equation with Z parameter was established. Meanwhile, the critical conditions of DRX have been obtained by the relationship between work hardening rate and flow stress, and the relationships between Z parameter and the critical conditions were also determined. The hot working map analysis shows that the instability zone gradually decreases with increasing deformation strain, and the optimal processing zones are within the range of 1348~1432 K/1~10 s-1, and corresponding values of power dissipation coefficient are above 0.4.

Key words:  metallic materials      duplex stainless steel      recrystallization      critical strain      large deformation      hot working map     
Received:  23 June 2020     
ZTFLH:  TG142.1  
Fund: National Natural Science Foundation of China(51461024)
About author:  YANG Yinhui, Tel: 13518726308, E-mail: yyhyanr@sina.com

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2020.249     OR     https://www.cjmr.org/EN/Y2021/V35/I5/381

Fig.1  Experimental process flow chart
Fig.2  True stress-true strain curves under the condiyion of same strain rate and different deformation temperatures (a) 0.01 s-1; (b) 0.1 s-1; (c) 1 s-1; (d) 10 s-1
Fig.3  Typical microstructures of specimen under the condition of different temperatures (T) and different strain rates (ε?) (a) 0.01 s-1/1223 K; (b) 0.1 s-1/1223 K; (c) 1 s-1/1223 K; (d) 10 s-1/1223 K; (e) 0.1 s-1/1323 K; (f) 0.1 s-1/1423 K
Fig.4  TEM images of specimens deformed at temperature of 1123K and different strain rates (a, b) 0.01 s-1; (c, d) 1 s-1; (e, f) 10 s-1
Fig.5  TEM images of specimens deformed at strain rate of 0.1 s-1 and different deformation temperatures (a, b, c) 1123 K; (d, e, f) 1223 K; (g, h, i) 1323 K
Fig.6  Relationship between ?2θ and σ at the same strain rate and different deformation temperatures (a) 0.01 s-1, (b) 0.1 s-1, (c) 1 s-1 and (d) 10 s-1
Fig.7  Effect of deformation temperatures and strain rates on the critical strain of the specimen
Fig.8  Relationship between critical stress σc and peak stress σp and critical strain εc and peak strain εp of specimen (a) σc-σp , (b) εc-εp
Fig.9  Relationship between thermal deformation peak stress and strain rate and deformation temperature (a) lnσp-lnε˙, (b) σp-lnε˙,(c) ln[sinh(ασp)]-lnε˙,(d) ln[sinh(ασp)]-10000/T
Fig.10  Relationship between lnZ and ln[sinh(ασp)]
Fig.11  Fitting of the characteristic parameters and Z parameters (a) lnσc-lnZ (b) lnσp-lnZ (c) lnεc-lnZ (d) lnεp-lnZ
Fig.12  Processing maps of specimen for different true strain (ε˙) (The shadow regions represent the rheological instability zones and the contours represent power dissipation coefficients) (a) ε˙=0.2 (b)?ε˙=0.3 (c)?ε˙=0.4 (d)?ε˙=0.6 (e)?ε˙=0.8 (f)?ε˙=1.0 (g)?ε˙=1.2
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