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| Effect of Different Coupling Agents on Interfacial Properties of Hollow Glass Microsphere/Phenolic Syntactic Foams |
WANG Bo, HUANG Chi, HUANG Zhixiong*( ), ZHANG Jingjie |
| (Key Laboratory of Advanced Technology for Special Functional Materials of Ministry of Education, School of Materials Science and Engineering, Wuhan University of Technology, Wuhan 430070, China) |
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Cite this article:
WANG Bo, HUANG Chi, HUANG Zhixiong, ZHANG Jingjie. Effect of Different Coupling Agents on Interfacial Properties of Hollow Glass Microsphere/Phenolic Syntactic Foams. Chinese Journal of Materials Research, 2016, 30(3): 209-219.
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Abstract Hollow glass microspheres (HGM) are modified with different types of coupling agents.Phenolic syntactic foams are prepared by introducing the modified hollow glass microspheres into phenolic matrix. The interaction between HGM and phenolic matrix, as well as the flexural strength, fracture toughness, and dynamic mechanical properties of phenolic syntactic foams were then studied. Results showed that the graft of coupling agent onto the surface of HGM could reduce the agglomeration of HGM in the phenolic matrix, enhance the compatibility of HGM with phenolic matrix and the hydrophobicityof HGM, resulting in a good comprehensive property of phenolic syntactic foams. Among various types of coupling agents of γ-aminopropyltriethoxysilane(APTES), di(dioctylpyrophosphato) ethylene titanate(NDZ-311), and glutaraldehyde(GA), the long chains on the surface of NDZ311grafted HGM may interact with polymer chains of PF matrix through Vander Waals forces and physical entanglement of molecular chains; For the case of APTES-HGM, when the particles are immersed in resol phenolic, a few hydroxymethylgroup could react with amino group to form chemical bonding, the physicalentanglement of molecular chains dominates the linkage between filler and matrix; In syntactic foams containing GA modified HGM, the aldehyde group could react with phenolic resinmonomers and form acetal linkage with resin matrix.
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Received: 01 August 2015
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| About author: *To whom correspondence should be addressed, Tel: 13807180447, E-mail: zhixiongh@whut.edu.cn |
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