Effect of Hot Isostatic Pressing on Microstructure of a Third-Generation Single Crystal Superalloy DD33

doi:10.11901/1005.3093.2021.490

Chinese Journal of Materials Research

2022, Vol. 36

Issue (9): 649-659 DOI: 10.11901/1005.3093.2021.490

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Effect of Hot Isostatic Pressing on Microstructure of a Third-Generation Single Crystal Superalloy DD33

HE Yufeng¹^,², WANG Li¹, WANG Dong¹, WANG Shaogang³, LU Yuzhang¹, GU Ashan⁴, SHEN Jian¹(

), ZHANG Jian¹

^1.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
^2.School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
^3.Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
^4.AECC Guizhou Liyang Aviation Power Company Limited, Guiyang 550014, China

Cite this article:

HE Yufeng, WANG Li, WANG Dong, WANG Shaogang, LU Yuzhang, GU Ashan, SHEN Jian, ZHANG Jian. Effect of Hot Isostatic Pressing on Microstructure of a Third-Generation Single Crystal Superalloy DD33. Chinese Journal of Materials Research, 2022, 36(9): 649-659.

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Abstract

The third generation DD33 single crystal superalloy was subjected to standard heat treatment and hot isostatic pressing respectively, and then to different post-solution and -aging treatments. Hereafter, the effect of hot isostatic pressing and heat treatment on the microstructure and durability of the alloy were investigated by means of high-temperature endurance tests at 850℃/650 MPa and 1100℃/170 MPa, as well as metallographic microscope (OM), scanning electron microscope (SEM) and X-ray three-dimensional imaging (XCT). The results show that after proper hot isostatic pressing and subsequent heat treatment, the as-cast DD33 single crystal superalloys present more or less the same microstructure of (γ' phase size, volume fraction and cubic degree) as those subjected to standard heat treatment. Compared with the standard heat treated alloy, the volume fraction and size of the micropores of the alloy decreased significantly after hot isostatic pressing, from 0.0190% to 0.0005%, and the maximum equivalent diameter of the micropores decreased from 36.9 μm to 14.2 μm. The durable life of the alloy subjected to hot isostatic pressing was significantly prolonged when testing by 850℃/650 MPa and 1100℃/170 MPa. These results show that proper hot isostatic pressing and heat treatment can eliminate the micro voids, therewith, improve the durability of the alloy.

Key words: metal materials hot isostatic pressing single crystal superalloy micro-pore stress rupture properties X-ray tomography

Received: 24 August 2021

ZTFLH:

TG132.32

Fund: National Natural Science Foundation of China(51631008);National Natural Science Foundation of China(91860201);National Natural Science Foundation of China(51771204);National Natural Science Foundation of China(51911530154);National Natural Science Foundation of China(U1732131);National Science and Technology Major Project(2017-VII-0008-0101);National Science and Technology Major Project(2017-VI-0003-0073);National Science and Technology Major Project(J2019-Ⅵ-0010);Key Deployment Projects of the Chinese Academy of Sciences(ZDRWCN-2019-01)

About author: SHEN Jian, Tel: 13804984964, E-mail: shenjian@imr.ac.cn

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	Yufeng HE
	Li WANG
	Dong WANG
	Shaogang WANG
	Yuzhang LU
	Ashan GU
	Jian SHEN
	Jian ZHANG

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https://www.cjmr.org/EN/10.11901/1005.3093.2021.490 OR https://www.cjmr.org/EN/Y2022/V36/I9/649

Table 1 Nominal composition of the superalloy used in the experiments (mass fraction, %)

Table 2 HIP parameters and heat treatment processes used in this work

Table 3 Parameters for the XCT conducted on Xradia VersaXRM-500 system

Fig.1 Microstructure of as-cast (AC) DD33 alloy processed by HRS (a, b) OM and (c, d) SEM

Fig.2 Microstructure of standard heat treatment (SHT) DD33 alloy processed by HRS (a) OM, (b) dendrite region, and (c) interdendritic region

Fig.3 Scanning electron micrographs of the HRS DD33 before and after HIP treatment (a, b) AC and (c, d) AH

Fig.4 Microstructures (OM) of DD33 after AHS1 (a, b), AHS2 (c, d), and AHS3 heat treatment (e, f)

Fig.5 Scanning electron micrographs of the DD33 after AHS3HT1 (a, d), AHS3HT2 (b, e) and AHS3HT3 heat treatment (c, f)

Fig.6 EBSD data of the (a, c) AH and (b, d) AHSHT specimens nearby carbide: (a, b) IPF-X maps, (c, d) KAM maps

Fig.7 Ex-situ XCT observation of the evolution of micro-pores in DD33 AC sample before and after HIP heat treatment (a, b, c, d) AC, (e, f, g, h) AH, (i, j, k, l) AHS3HT3

Fig.8 Three dimensional morphologies of micro-pores inside the SHT DD33 sample by different processing. (a, b, c) HRS, (d, e, f) HIP

Table 4 Effect of HIP on the stress rupture properties of the DD33 alloy under different conditions

Fig.9 Fracture morphology of (a, c, e) HRS and (b, d, f) HIP specimens after 1100℃/170 MPa (a, b) the fracture surfaces, (c, d) the longitudinal section OM morphologies, (e, f) the morphology of γ/γʹ microstructure

1	Pollock T M, Tin S. Nickel-based superalloys for advanced turbine engines: chemistry, microstructure and properties [J]. J. Propul. Power., 2006, 22(2): 361 doi: 10.2514/1.18239
2	Zhang J, Wang L, Wang D, et al. Recent progress in research and development of nickel-based single crystal superalloys [J]. Acta Metall. Sin., 2019, 55(9): 1077
	张健, 王莉, 王栋等. 镍基单晶高温合金的研发进展 [J]. 金属学报, 2019, 55(9): 1077
3	Fu H Z, Guo J J, Liu L, et al. Directional Solidification and Processing of Advanced Materials [M]. Beijing: Science Press, 2008:7
	傅恒志, 郭景杰, 刘林等. 先进材料定向凝固 [M]. 北京: 科学出版社, 2008: 7
4	Aveson J W, Tennant P A, Foss B J, et al. On the origin of sliver defects in single crystal investment castings [J]. Acta Mater., 2013, 61(14): 5162 doi: 10.1016/j.actamat.2013.04.071
5	Auburtin P, Wang T, Cockcroft S L, et al. Freckle formation and freckle criterion in superalloy castings [J]. Metall. Mater. Trans B, 2000, 31(4): 801 doi: 10.1007/s11663-000-0117-9
6	Link T, Zabler S, Epishin A, et al. Synchrotron tomography of porosity in single-crystal nickel-base superalloys [J]. Mater. Sci. Eng. A, 2006, 425(1-2): 47 doi: 10.1016/j.msea.2006.03.005
7	le Graverend J B, Adrien J, Cormier J. Ex-situ X-ray tomography characterization of porosity during high-temperature creep in a Ni-based single-crystal superalloy: toward understanding what is damage [J]. Mater. Sci. Eng. A, 2017, 695: 367 doi: 10.1016/j.msea.2017.03.083
8	Ruttert B, Meid C, Roncery L M, et al. Effect of porosity and eutectics on the high-temperature low-cycle fatigue performance of a nickel-base single-crystal superalloy [J]. Scr. Mater., 2018, 155: 139 doi: 10.1016/j.scriptamat.2018.06.036
9	Lamm M, Singer R F. The effect of casting conditions on the high-cycle fatigue properties of the single-crystal nickel-base superalloy PWA 1483 [J]. Metall. Mater. Trans. A, 2007, 38(6): 1177
10	Loh N L, Sia K Y. An overview of hot isostatic pressing [J]. J. Mater. Process. Technol., 1992, 30(1): 45 doi: 10.1016/0924-0136(92)90038-T
11	Guo H M, Zhao Y S, Zheng S, et al. Effect of hot-isostatic pressing on microstructure and mechanical properties of second generation single crystal superalloy DD6 [J]. J. Mater. Eng., 2016, 44(10): 60
	郭会明, 赵云松, 郑帅等. 热等静压对第二代单晶高温合金DD6显微组织和力学性能的影响 [J]. 材料工程, 2016, 44(10): 60
12	He S L, Zhao Y S, Lu F, et al. Effects of hot isostatic pressure on microdefects and stress rupture life of second-generation nickel-based single crystal superalloy in as-cast and as-solid-solution states [J]. Acta Metall. Sin., 2020, 56(9): 1195 doi: 10.11900/0412.1961.2020.00020
	和思亮, 赵云松, 鲁凡等. 热等静压对铸态及固溶态第二代镍基单晶高温合金显微缺陷及持久性能的影响 [J]. 金属学报, 2020, 56(9): 1195 doi: 10.11900/0412.1961.2020.00020
13	Chang J C, Choi C, Kim J C, et al. Development of microstructure and mechanical properties of a Ni-base single-crystal superalloy by hot-isostatic pressing [J]. J. Mater. Eng. Perform., 2003, 12(4): 420 doi: 10.1361/105994903770342953
14	Epishin A, Camin B, Hansen L, et al. Synchrotron 3D μ-Tomography of Porosity during Hot Isostatic Pressing of a Single-Crystal Nickel-Base Superalloy [J]. Mater. Sci. Forum., 2021, 1016: 102 doi: 10.4028/www.scientific.net/MSF.1016.102
15	Mujica Roncery L, Lopez-Galilea I, Ruttert B, et al. On the Effect of Hot Isostatic Pressing on the Creep Life of a Single Crystal Superalloys [J]. Adv. Eng. Mater., 2016, 18(8): 1381 doi: 10.1002/adem.201600071
16	Cervellon A, Cormier J, Mauget F, et al. Very high cycle fatigue of Ni-based single-crystal superalloys at high temperature [J]. Metall. Mater. Trans. A, 2018, 49(9): 3938
17	Reed R C, Cox D C, Rae C M F. Damage accumulation during creep deformation of a single crystal superalloy at 1150 C [J]. Mater. Sci. Eng. A, 2007, 448(1-2): 88 doi: 10.1016/j.msea.2006.11.101
18	Roncery L M, Lopez-Galilea I, Ruttert B, et al. Influence of temperature, pressure, and cooling rate during hot isostatic pressing on the microstructure of an SX Ni-base superalloy [J]. Mater. Des., 2016, 97: 544 doi: 10.1016/j.matdes.2016.02.051
19	Li X W. Effect of carbon on the microstructure and creep property of a third generation single crystal nickle-based superalloy [D]. Shenyang: University of Chinese Academy of Sciences, 2013
	李相伟. 碳对第三代镍基单晶高温合金组织和蠕变持久性能的影响 [D]. 沈阳: 中国科学院大学, 2013
20	Kearsey R M, Beddoes J C, Jones P, et al. Compositional design considerations for microsegregation in single crystal superalloy systems [J]. Intermetallics, 2004, 12(7-9): 903 doi: 10.1016/j.intermet.2004.02.041
21	Jiang R, Bull D J, Evangelou A, et al. Strain accumulation and fatigue crack initiation at pores and carbides in a SX superalloy at room temperature [J]. Int. J. Fatigue, 2018, 114: 22 doi: 10.1016/j.ijfatigue.2018.05.003
22	Huang Y Q, Wang D, Lu Y Z, et al. Fatigue crack initiation behavior at intermediate temperature under high stress amplitude for single crystal superalloy DD413 [J]. Chin. J. Mater. Res., 2021, 35(7): 510 doi: 10.11901/1005.3093.2020.274
	黄亚奇, 王栋, 卢玉章等. 第一代单晶高温合金中温高应力幅下的疲劳裂纹萌生行为 [J]. 材料研究学报, 2021, 35(7): 510 doi: 10.11901/1005.3093.2020.274
23	Wang L, Xie G, Zhang J, et al. On the role of carbides during the recrystallization of a directionally solidified nickel-base superalloy [J]. Scr. Mater., 2006, 55(5): 457 doi: 10.1016/j.scriptamat.2006.05.013
24	Bokstein B S, Epishin A I, Link T, et al. Model for the porosity growth in single-crystal nickel-base superalloys during homogenization [J]. Scr. Mater., 2007, 57(9): 801 doi: 10.1016/j.scriptamat.2007.07.012
25	Han D Y, Jiang W G, Xiao J H, et al. Effect of section size and solution treatment on micropore of a third-generation single crystal superalloy DD33 [J]. Chin. J. Mater. Res., 2018, 32(3): 168 doi: 10.11901/1005.3093.2017.152
	韩东宇, 姜卫国, 肖久寒等. 截面尺寸和固溶制度对单晶高温合金DD33中显微孔洞的影响 [J]. 材料研究学报, 2018, 32(3): 168 doi: 10.11901/1005.3093.2017.152
26	Shi Q Y, Li X H, Zheng Y R, et al. Formation of solidification and homogenisation micropores in two single crystal superalloys produced by HRS and LMC processes [J]. Acta Metall. Sin., 2012, 48(10): 1237 doi: 10.3724/SP.J.1037.2012.00172
	石倩颖, 李相辉, 郑运荣等. HRS和LMC工艺制备的两种镍基单晶高温合金铸态及固溶微孔的形成 [J]. 金属学报, 2012, 48(10): 1237
27	Epishin A, Fedelich B, Link T, et al. Pore annihilation in a single-crystal nickel-base superalloy during hot isostatic pressing: Experiment and modelling [J]. Mater. Sci. Eng. A, 2013, 586: 342 doi: 10.1016/j.msea.2013.08.034
28	Li Y, Wang L, Zhang G, et al. Creep anisotropy of a 3rd generation nickel-base single crystal superalloy at 850℃ [J]. Mater. Sci. Eng. A, 2019, 760: 26 doi: 10.1016/j.msea.2019.05.075
29	Le Graverend J B, Cormier J, Kruch S, et al. Microstructural parameters controlling high-temperature creep life of the nickel-base single-crystal superalloy MC2 [J]. Metall. Mater. Trans. A, 2012, 43(11): 3988
30	Isaac A, Sket F, Reimers W, et al. In situ 3D quantification of the evolution of creep cavity size, shape, and spatial orientation using synchrotron X-ray tomography [J]. Mater. Sci. Eng. A, 2008, 478(1-2): 108 doi: 10.1016/j.msea.2007.05.108
31	Shi Z X, Liu S Z, Xiong J C, et al. Effect of hot isostatic pressing on the microstructure and stress rupture properties of single crystal superalloy [J]. Rare Met. Mater. Eng., 2015, 44(9): 2300
	史振学, 刘世忠, 熊继春. 热等静压对单晶高温合金组织和持久性能的影响 [J]. 稀有金属材料与工程, 2015, 44(9): 2300
32	Fritzemeier L G. The influence of high thermal gradient casting, hot isostatic pressing and alternate heat treatment on the structure and properties of a single crystal nickel base superalloy [A]. Superalloys 1988 [C]. Warrendale, 1988: 265

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