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Chinese Journal of Materials Research  2019, Vol. 33 Issue (6): 475-480    DOI: 10.11901/1005.3093.2018.694
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Structure and Electromagnetic Properties of Glass D250 Coated FeSiAl Alloy Flakes
Dali ZHANG,Yujian LIU(),Jun FANG
School of Materials Science and Engineering, East China University of Science and Technology, Shanghai 200237, China
Cite this article: 

Dali ZHANG,Yujian LIU,Jun FANG. Structure and Electromagnetic Properties of Glass D250 Coated FeSiAl Alloy Flakes. Chinese Journal of Materials Research, 2019, 33(6): 475-480.

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Abstract  

FeSiAl alloy flakes were coated with glass powder D250 of low melting point via a two-step process, i.e. FeSiAl alloy flakes and glass powders D250 were firstly blended by ball milling to prepare D250 powders covered FeSiAl alloy flakes and then which was heat treated at proper elevated temperature. The phase composition, surface topography and composition of the coated flakes were characterized by using XRD, SEM, XRF and EDS. The electromagnetic parameter and reflection loss were also assessed in the frequency range of 1~18 GHz by using vector network analyzer. The results show that a dense coating formed on the flakes with uniform appearance, which present a lower real part of their complex permittivity of about 8. The glass D250 coated FeSiAl alloy flakes with optimal performance could be acquired when the heat treatment process was conducted at 700℃, namely the maximum reflection loss depresses to -40.10 dB, and the effective bandwidth reaches to 3.76 GHz, respectively.

Key words:  metallic materials      FeSiAl alloy      melt coating      absorptivity     
Received:  06 December 2018     
ZTFLH:  TM25  

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2018.694     OR     https://www.cjmr.org/EN/Y2019/V33/I6/475

Fig.1  XRD patterns of FeSiAl magnetic powder and coating (a) flattening treatment, (b) mechanical coating with D250, (c) melt coating at 600℃, (d) melt coating at 700℃, (e) melt coating at 800℃
Fig.2  SEM images of FeSiAl magnetic powder and coating (a1, a2) Flattening treatment, (b) Mechanical coating with D250, (c1, c2) Melt coating with D250
Fig.3  EDS of melt coating on FeSiAl magnetic powder
OZnSiNaCaMgAlKBaTiRb
29.7%24.5%15.1%8.4%6.8%5.7%3.2%3.1%2.7%0.4%0.3%
Table 1  Element analysis of D250 glass powder by XRF
Fig.4  Complex permittivity of FeSiAl magnetic powder and coating (A) flattening treatment, (B) mechanical coating with D250, (C) melt coating at 600℃, (D) melt coating at 700℃, (E) melt coating at 800℃
Fig.5  Complex permeability of FeSiAl magnetic powder and coating (A) flattening treatment, (B) mechanical coating with D250, (C) melt coating at 600℃, (D) melt coating at 700℃, (E) melt coating at 800℃
Fig.6  Reflection loss of FeSiAl magnetic powder and coating (A) flattening treatment, (B) mechanical coating with D250, (C) melt coating at 600℃, (D) melt coating at 700℃, (E) melt coating at 800℃
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