Effect of Surface Modification of Carbon Fiber on Friction Properties of Carbon Fiber/Phenolic Resin Matrix Composite

doi:10.11901/1005.3093.2014.356

Chinese Journal of Materials Research

2015, Vol. 29

Issue (2): 101-107 DOI: 10.11901/1005.3093.2014.356

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Effect of Surface Modification of Carbon Fiber on Friction Properties of Carbon Fiber/Phenolic Resin Matrix Composite

Xiaolong MA¹,Yuhui AO^1,^3,^**(

),Linghan XIAO^1,³,Jinglong DONG¹,Huixuan ZHANG^1,²

1. Changchun University of Technology, college of chemistry and life science, Changchun 130012, China
2. Changchun Institute of Applied Chemistry, Chinese Academy of Science, Changchun 130022, China
3. Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun 130012, China

Cite this article:

Xiaolong MA,Yuhui AO,Linghan XIAO,Jinglong DONG,Huixuan ZHANG. Effect of Surface Modification of Carbon Fiber on Friction Properties of Carbon Fiber/Phenolic Resin Matrix Composite. Chinese Journal of Materials Research, 2015, 29(2): 101-107.

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Abstract

Polyacrylonitrile (PAN)-based carbon fiber was surface modified with HNO₃ (65-68%) and silane coupling agent (hk550) and of which the structural and surface characteristics of were investigated by SEM, FT-IR, and X-ray photoelectron spectroscopy (XPS). Then the surface modified carbon fiber reinforced phenolic matrix composites were prepared. The tensile strength and the friction performance of the composites were examined by tensile testing machine and integrated micro-nano-mechanical test system (UNMT-1) respectively. The results showed that the surface modification with HNO₃ and hk550 could enhance the surface chemical activity and roughness of the fibers, resulting in better interfacial adhesion between carbon fibers and phenolic resin matrix, therefore, improved the tensile strength and reduced the wear rate of the composites.

Key words: composite coupling agent surface modified carbon fiber wear rate

Received: 15 July 2014

Fund: *Supported by the Program of Jilin Province for "Ten Keys" Problems in Transformation of Technology No. ZDZH11003.

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	Xiaolong MA
	Yuhui AO
	Linghan XIAO
	Jinglong DONG
	Huixuan ZHANG

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https://www.cjmr.org/EN/10.11901/1005.3093.2014.356 OR https://www.cjmr.org/EN/Y2015/V29/I2/101

Fig.1 Surface morphologies of carbon fibers before and after treatment (a) CF, (b) CF-0.5 h, (c) CF-3 h, (d) CF-A-0.5 h, (e) CF-A-1.5 h, (f) CF-A-3 h

Fig.2 FTIR spectra of carbon fibe

Table 1 Element analysis on the surface of carbon fibers with different treatment

Fig.3 XPS wide scan spectra of different samples

Fig.4 C1s XPS narrow-scan spectra of different samples (a) CF, (b) CF-0.5 h, (c) CF-1.5 h, (d) CF-3 h

Table 2 Surface functional components obtained from the deconvolution of C1s peaks

Fig.5 hk550 hydrolysis structure and reaction with CF diagram

Fig.6 SEM fractographs of different sample (a) CFRP-0.5 h, (b) CFRP-1.5 h, (c) CFRP-3 h, (d) CFRP-A-0.5 h, (e) CFRP-A-3 h

Fig.7 Tensile strength of the composites

Fig.8 Schematic wear process of composites

Fig.9 SEM pictures of the worn surfaces of the composites

Fig.10 Dynamic friction coefficient of different sample

Fig.11 Friction coefficient and wear rate of composites

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