缺口取向及温度对第三代单晶高温合金<strong>DD33</strong>热疲劳行为的影响

doi:10.11901/1005.3093.2023.178

材料研究学报

2024, Vol. 38

Issue (2): 111-120 DOI: 10.11901/1005.3093.2023.178

研究论文

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缺口取向及温度对第三代单晶高温合金DD33热疲劳行为的影响

郑明瑞¹^,², 李亚微¹^,², 刘静¹^,², 王莉¹(

), 郑伟¹, 董加胜¹(

), 张健¹, 楼琅洪¹

^1.中国科学院金属研究所沈阳 110016
^2.中国科学技术大学材料科学与工程学院沈阳 110016

Effect of Notch Orientation and Temperature on Thermal Fatigue Behavior of a Third-Generation Single Crystal Superalloy DD33

ZHENG Mingrui¹^,², LI Yawei¹^,², LIU Jing¹^,², WANG Li¹(

), ZHENG Wei¹, DONG Jiasheng¹(

), ZHANG Jian¹, LOU Langhong¹

^1.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
^2.School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China

引用本文:

郑明瑞, 李亚微, 刘静, 王莉, 郑伟, 董加胜, 张健, 楼琅洪. 缺口取向及温度对第三代单晶高温合金DD33热疲劳行为的影响[J]. 材料研究学报, 2024, 38(2): 111-120.
Mingrui ZHENG, Yawei LI, Jing LIU, Li WANG, Wei ZHENG, Jiasheng DONG, Jian ZHANG, Langhong LOU. Effect of Notch Orientation and Temperature on Thermal Fatigue Behavior of a Third-Generation Single Crystal Superalloy DD33[J]. Chinese Journal of Materials Research, 2024, 38(2): 111-120.

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摘要:

使用OM、SEM和EDS等手段，研究了第三代镍基单晶高温合金DD33不同V型缺口取向([100]、[210]和[110])片状试样从室温到不同上限温度(1000℃、1100℃和1200℃)的热疲劳过程中裂纹的萌生和扩展行为。结果表明，在三种上限温度，DD33合金的热疲劳性能均出现明显的各向异性。在三个上限温度[100]取向试样均表现出最好的热疲劳性能；上限温度为1000℃和1200℃[110]取向试样的热疲劳性能最差，上限温度为1100℃[210]取向试样的热疲劳性能最差。不同取向试样的热疲劳裂纹的萌生和扩展行为，均呈现出一定的晶体学取向规律。热应力、氧化以及滑移系的开动，导致不同取向试样裂纹的扩展速率不同。

关键词 ：金属材料, 单晶高温合金, 缺口取向, 热疲劳, 各向异性, 氧化

Abstract：

The crack initiation and propagation behavior of a third-generation single crystal superalloy DD33 with V-notches of different orientations ([100], [210] and [110]) during thermal fatigue tests: samples were hold at different high-temperatures (1000^oC, 1100^oC and 1200^oC respectively) for 60 s and then quick quenching into water as one cycle, was investigated by OM, SEM and EDS. The results show that the thermal fatigue properties of DD33 show obvious anisotropy tested at different high-temperatures. The initiation and propagation behavior of thermal fatigue cracks in samples with different notch orientations show the dependence of crystallographic orientation. At 1000^oC/1100^oC/1200^oC, the [100] orientated specimens exhibit the best thermal fatigue performance. The thermal fatigue performance of the [210] oriented sample is the worst at 1100^oC, while the thermal fatigue performance of the [110] oriented sample is the worst at 1000^oC and 1200^oC. The thermal stress, oxidation, and the operation of slip systems result in the difference in crack growth rate of samples with different notch orientations.

Key words： metallic materials single crystal superalloy notch orientation thermal fatigue anisotropy oxidation

收稿日期: 2023-03-15

ZTFLH:

TG132.32

基金资助:航空发动机及燃气轮机基础科学中心项目(P2021-AB-IV-001-002);国家科技重大专项(2017-VI-0019-0091)

通讯作者: 王莉，研究员，wangli@imr.ac.cn，研究方向为单晶高温合金组织及性能;
董加胜，研究员，djs@imr.ac.cn，研究方向为先进高温合金及叶片制备技术

Corresponding author: WANG Li, Tel: (024)23971276, E-mail: wangli@imr.ac.cn;
DONG Jiasheng, Tel: (024)23748882, E-mail: djs@imr.ac.cn

作者简介: 郑明瑞，男，1997年生，硕士生

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https://www.cjmr.org/CN/10.11901/1005.3093.2023.178 或 https://www.cjmr.org/CN/Y2024/V38/I2/111

表1 实验用高温合金的名义成分

图1 不同缺口取向热疲劳样品的示意图

图2 热疲劳试样的几何形状和尺寸

图3 不同取向试样缺口的形态、表面宏观形貌和显微组织形貌

图4 不同取向试样在不同温度下的裂纹扩展动力学曲线

图5 不同取向试样的热疲劳裂纹萌生所需的循环周次

图6 三种取向试样的热疲劳裂纹萌生情况

图7 在1000℃下[100]取向试样裂纹尖端元素的分布

图8 在1000℃下[210]取向试样裂纹尖端元素的分布

图9 在1000℃下[110]取向试样裂纹尖端元素的分布

图10 上限温度为1100℃时不同取向试样裂纹的宏观和微观形貌

图11 上限温度为1200℃时不同取向试样的裂纹形貌

1	Reed R C. The Superalloys Fundamentals and Application [M]. New York: Cambridge University Press, 2006
2	Zhang J, Wang L, Wang D, et al. Recent progress in research and development of nickel-based single crystal superalloys [J]. Acta Metall. Sin., 2019, 55(09): 1077
2	张健, 王莉, 王栋等. 镍基单晶高温合金的研发进展 [J]. 金属学报, 2019, 55(09): 1077
3	Halford G R. Low-cycle thermal fatigue [J]. Therm. Fatigue, 1986, 22(2): 285
4	Zhang J, Zhao Z, Kong Y, et al. Crack initiation and propagation mechanisms during thermal fatigue in directionally solidified superalloy DZ125 [J]. Int. J. Fatigue, 2019, 119: 355 doi: 10.1016/j.ijfatigue.2018.09.001
5	Xia P C, Yu J J, Sun X F, et al. Influence of holding time and notched radius on thermal fatigue property of DZ951 alloy [J]. Trans. Mater. Heat Treat., 2010, 33(02): 40
5	夏鹏成, 于金江, 孙晓峰等. 保温时间和缺口半径对DZ951合金热疲劳性能的影响 [J]. 材料热处理学报, 2010, 31(02): 40
6	Xiao X, Xu H, Qin X Z, et al. Microstructural evolution of two cast nickel-base superalloys in thermal fatigue process [J]. J. Iron Steel Res., 2011, 23(S2): 393 doi: 10.1016/S1006-706X(16)30062-0
6	肖旋, 许辉, 秦学智等. 两种铸造高温合金热疲劳过程中微观组织演化 [J]. 钢铁研究学报, 2011, 23(S2): 393
7	Ning K L, Zheng Z, An F Q, et al. Thermal fatigue behavior of K125L superalloy [J]. Rare Met., 2016, 35(02): 172 doi: 10.1007/s12598-014-0254-y
8	Zhou T J, Ding H S, Ma X P, et al. A comparison study of the thermal fatigue properties of three ni-based cast superalloys cycled from 20 to 1100^oC [J]. Adv. Eng. Mater., 2019, 21(7): 190054
9	Gui W M, Zhang H Y, Yang M, et al. The intrinsic relationship between microstructure evolution and thermal fatigue behavior of a single-crystal cobalt-base superalloy [J]. Acta Metall. Sin. (Engl. Lett.), 2017, 30(12): 1192 doi: 10.1007/s40195-017-0646-8
10	Chen J, Shi D Q, Miao G L, et al. Thermal fatigue behavior of nickel based superalloy GH536 [J]. J. Aero. Power, 2017, 32(6): 1381
10	陈静, 石多奇, 苗国磊等. 镍基高温合金GH536的热疲劳行为 [J]. 航空动力学报, 2017, 32(6): 1381
11	Zhou Z, Yu D, Wang L, et al. Effect of skew angle of holes on the thermal fatigue behavior of a Ni-based single crystal superalloy [J]. Acta Metall. Sin. (Engl. Lett.), 2017, 30(2): 185 doi: 10.1007/s40195-016-0514-y
12	Wang L, Zhou Z J, Jiang W G, et al. Effect of secondary orientation on thermal fatigue behavior of a nickel-base single crystal superalloy DD33 [J]. Chin. J. Mater. Res., 2014, 28(09): 663
12	王莉, 周忠娇, 姜卫国等. 第二取向对镍基单晶高温合金DD33热疲劳性能的影响 [J]. 材料研究学报, 2014, 28(09): 663
13	Lv J J, Wang A D, Chen C F, et al. Thermal fatigue behavior of a nickel-base single crystal superalloy DD5 with secondary orientation [J]. Mater. Res. Express, 2018, 5(10): 106516 doi: 10.1088/2053-1591/aadac7
14	Xiao X, Xu H, Qin X Z, et al. Thermal fatigue behavior of three cast nickel base superalloys [J]. Acta Metall. Sin., 2011, 47(09): 1129
14	肖旋, 许辉, 秦学智等. 3种铸造镍基高温合金热疲劳行为研究 [J]. 金属学报, 2011, 47(09): 1129
15	Xia P C, Yang L, Yu J J, et al. Influence of direction of notch on thermal fatigue property of a directionally solidified nickel base superalloy [J]. Rare Met., 2011, 30: 472 doi: 10.1007/s12598-011-0327-0
16	Zhang Z H, Yu J J, Shi F, et al. Influence of thin wall on the tensile properties of DD499 single crystal superalloy [J]. Foundry, 2014, 63(08): 781
16	张泽海, 于金江, 石峰等. DD499单晶合金拉伸性能薄壁效应 [J]. 铸造, 2014, 63(08): 781
17	Hu Y, Zhang L, Cao T, et al. The effect of thickness on the creep properties of a single-crystal nickel-based superalloy [J]. Mater. Sci. Eng. A, 2018, 728: 124 doi: 10.1016/j.msea.2018.04.114
18	Li Q, Xie J, Yu J, et al. Effect of casting thickness on microstructure and mechanical properties of the high-W superalloy K416B [J]. Mater. Today Commun., 2021, 29: 102916
19	Zhao J Q, Shi Z X. Wall-thinned effects on tensile property in single crystal superalloys and influence of anisotropy [J]. Vacuum, 2018, 55(03): 41
19	赵金乾, 史振学. 单晶高温合金拉伸性能薄壁效应及各向异性的影响 [J]. 真空, 2018, 55(03): 41
20	Hu G X. Fundamentals of Materials Science (3rd Edition) [M]. Shanghai: Shanghai Jiao Tong University Press, 2017
20	胡庚祥. 材料科学基础(第三版) [M]. 上海: 上海交通大学出版社, 2017
21	Siebörger D, Knake H, Glatzel U. Temperature dependence of the elastic moduli of the nickel-base superalloy CMSX-4 and its isolated phases [J]. Mater. Sci. Eng. A, 2001, 298(1): 26 doi: 10.1016/S0921-5093(00)01318-6
22	Liu J L, Ye L H, Zhou Y Z, et al. Anisotropy of elasticity of a Ni base single crystal superalloy [J]. Acta Metall. Sin., 2020, 56(06):855
22	刘金来, 叶荔华, 周亦胄等. 一种单晶高温合金的弹性性能的各向异性 [J]. 金属学报, 2020, 56(06): 855
23	Suresh S. Fatigue of materials [M]. 3nd Ed., New York: Cambridge University Press, 1998
24	Wu C H, Jiang R, Zhang L C, et al. Oxidation accelerated dwell fatigue crack growth mechanisms of a coarse grained PM Ni-based superalloy at elevated temperatures [J]. Corros. Sci., 2022, 209: 110702 doi: 10.1016/j.corsci.2022.110702
25	Li T F. High Temperature Oxidation and Hot Corrosion of Metals [M]. Beijing: Chemical Industry Press, 2003
25	李铁藩. 金属高温氧化及热腐蚀 [M]. 北京: 化学工业出版社, 2003
26	Qiu W, He Z, Fan Y, et al. Effects of secondary orientation on crack closure behavior of nickel-based single crystal superalloys [J]. Int. J. Fatigue, 2016, 83: 335 doi: 10.1016/j.ijfatigue.2015.11.004
27	Zhao Z, Li Q, Zhang F, et al. Transition from internal to surface crack initiation of a single-crystal superalloy in the very-high-cycle fatigue regime at 1100^oC [J]. Int. J. Fatigue, 2021, 150: 106343 doi: 10.1016/j.ijfatigue.2021.106343
28	Wang L, He Y F, Shen J, et al. Effect of secondary orientation on oxidation anisotropy around the holes of single crystal superalloy during thermal fatigue tests [J]. Acta Metall. Sin., 2019, 55(11): 1417 doi: 10.11900/0412.1961.2019.00109
28	王莉, 何禹锋, 申健等. 第二取向对第三代单晶高温合金热疲劳过程中冷却孔孔周氧化行为的影响研究 [J]. 金属学报, 2019, 55(11): 1417
29	Wang L, Liu X G, Zhang J, et al. High temperature oxidation of a single crystal nickel-base superalloy [J]. J. Iron Steel Res., 2011, 23(S2): 353
29	王莉, 刘心刚, 张健等. 第三代单晶高温合金DD33的高温氧化行为 [J]. 钢铁研究学报, 2011, 23(S2): 353

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