Effect of Long-term Thermal Exposure on Microstructure Evolution of a Platinum Modified Aluminide Coated Single Crystal Superalloy DD413

doi:10.11901/1005.3093.2022.600

Chinese Journal of Materials Research

2023, Vol. 37

Issue (12): 889-899 DOI: 10.11901/1005.3093.2022.600

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Effect of Long-term Thermal Exposure on Microstructure Evolution of a Platinum Modified Aluminide Coated Single Crystal Superalloy DD413

ZHANG Yingjian¹, ZHANG Siqian¹(

), WANG Dong², ZHANG Haoyu¹, ZHOU Ge¹, CHEN Lijia¹

^1.School of Material Science and Engineering, Shenyang University of Technology, Shenyang 110870, China
^2.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Cite this article:

ZHANG Yingjian, ZHANG Siqian, WANG Dong, ZHANG Haoyu, ZHOU Ge, CHEN Lijia. Effect of Long-term Thermal Exposure on Microstructure Evolution of a Platinum Modified Aluminide Coated Single Crystal Superalloy DD413. Chinese Journal of Materials Research, 2023, 37(12): 889-899.

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Abstract

A nickel base single crystal superalloy DD413 was coated with platinum modified aluminide (Pt-Al) coating via successively Pt electrodepositing and vapor phase aluminizing, then the degradation behavior of the Pt-Al coating/ DD413 alloy after long-term thermal exposure in air at 850℃ and 1000℃is studied by means of scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The results show that with the extension of thermal exposure time, MC carbide and σ-TCP phase dissolve to varying degrees in the interdiffusion of zone (IDZ), accompanied by M₂₃C₆ carbide precipitation on the interface. At the same time, the size of the secondary reaction of zone (SRZ) and σ-TCP phase increases continuously. In the substrate beneath the coating, cubic γ' precipitates are spheroidized and connected with each other in a raft shape. The higher thermal exposure temperature, the more obvious the above microstructure degradation process. It can be seen from the comparative analysis that the microstructure degradation after long-term thermal exposure is closely related to the diffusion of elements at high temperatures.

Key words: metallic materials Nickel base single crystal superalloy Pt-Al Coating Long-term thermal exposure Interface microstructure degradation

Received: 14 November 2022

ZTFLH:

TG113

Fund: National Natural Science Foundation of China(52071219)

Corresponding Authors: ZHANG Siqian, Tel: 13700022372, E-mail: sqzhang@alum.imr.ac.cn

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	ZHANG Yingjian
	ZHANG Siqian
	WANG Dong
	ZHANG Haoyu
	ZHOU Ge
	CHEN Lijia

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https://www.cjmr.org/EN/10.11901/1005.3093.2022.600 OR https://www.cjmr.org/EN/Y2023/V37/I12/889

Table 1 Nominal composition of DD413 alloy (mass fraction, %)

Fig.1 Diagram of cross section of coating/substrate

Fig.2 XRD diffraction pattern of original Pt-Al coating

Fig.3 (a) Cross section morphology of original Pt-Al coating/Alloy and (b) EDS energy spectrum corresponding to red box in (a)

Fig.4 BSE images and EDS spectrum of Pt-Al coating/alloy section after etched: (a) sectional image of Pt-Al coating; (b, c) enlarged image of coating/substrate interface image of γ/γ'; (d, e) are the corresponding MC and σ-TCP EDS spectra in (a)

Fig.5 TEM image and selected area diffraction pattern (SAD) of Pt-Al coating/alloy (a) TEM image of interdiffusion region of original coating; (A) and (B) selected area diffraction (SAD) corresponding to (a)

Fig.6 BSE images of Pt-Al coating/alloy section after long-term thermal exposure at 850℃ for different time (a) 50 h; (b)600 h; (c) 1800 h; (d) 3600 h

Fig.7 TEM image and selected area diffraction patterns (SAD) of block precipitated in IDZ after heat exposure at 850℃ for 3600 h

Fig.8 BSE images of Pt Al coating/alloy section etched after thermal exposure at 850℃ for different time (a) 50 h; (b) 600 h; (c) 1800 h; (d) 3600 h

Fig.9 (a) TEM image after thermal exposure at 850℃ for 3600 h and selected area diffraction pattern (SAD), (b) EDS energy spectrum corresponding to needle phase in (a)

Fig.10 BSE images of Pt-Al coating/alloy section after long-term thermal exposure at 1000℃ for different time (a) 50 h; (b)600 h; (c)1800 h; (d) 3600 h

Fig.11 Evolution trend of thickness of IDZ (a) and SRZ (b) after 850℃ and 1000℃ thermal exposure

Fig.12 Evolution trend of MC carbide in IDZ after thermal exposure at 850℃ and 1000℃ (a) Average size of MC carbide; (b) Volume fraction of MC carbide

Fig.13 XRD pattern of Pt-Al / DD413 system after long-term thermal exposure (a) 850℃/0-3600 h; (b) 1000℃/0-3600 h

Fig.14 BSE images of Pt-Al coating/alloy section after long-term thermal exposure at 1000℃ for different time (a) 50 h; (b)600 h; (c) 1800 h; (d) 3600 h

Fig.15 (a) 1000℃/3600 h, TEM image and selected area diffraction pattern (SAD) and (b) EDS energy spectrum corresponding to needle phase in (a)

1	Zhu Z, Basoalto H, Warnken N, et al. A model for the creep deformation behaviour of nickel-based single crystal superalloys [J]. Acta Mater., 2012, 60(12): 4888 doi: 10.1016/j.actamat.2012.05.023
2	Zhang J, Wang L, Wang D, et al. Recent progress in research and development of nickel-based single crystal superalloys [J]. Acta. Metall. Sin., 2019, 55(09): 1077
	张健, 王莉, 王栋等. 镍基单晶高温合金的研发进展 [J]. 金属学报, 2019, 55(09): 1077
3	Darolia R. Development of strong, oxidation and corrosion resistant nickel-based superalloys: critical review of challenges, progress and prospects [J]. Int. Mater. Rev., 2019, 64(6): 355 doi: 10.1080/09506608.2018.1516713
4	Pradhan D, Mahobia G S, Chattopadhyay K, et al. Effect of surface roughness on corrosion behavior of the superalloy IN718 in simulated marine environment [J]. J. Alloys Compd., 2018, 740: 250 doi: 10.1016/j.jallcom.2018.01.042
5	Yan G, Yu W, Shengping S. Oxidation protection of enamel coated Ni based superalloys: Microstructure and interfacial reaction [J]. Corros Sci., 2020, 173: 108760 doi: 10.1016/j.corsci.2020.108760
6	Itoh Y, Saitoh M, Ishiwata Y. Influence of high-temperature protective coatings on the mechanical properties of nickel-based superalloys [J]. J Mater Sci., 1999, 34(16): 3957 doi: 10.1023/A:1004643311001
7	Liu H, Xu M M, Li S, et al. Improving cyclic oxidation resistance of Ni₃Al-based single crystal superalloy with low-diffusion platinum-modified aluminide coating [J]. J Mater Sci Technol., 2020, 54: 132 doi: 10.1016/j.jmst.2020.05.007
8	Latief F H, Kakehi K. Influence of thermal exposure on the creep properties of an aluminized Ni-based single crystal superalloy in different surface orientations [J]. Mater. Des., 2014, 56: 816 doi: 10.1016/j.matdes.2013.11.075
9	Qin X Z, Guo J T, Yuan C, et al. Long-term thermal exposure responses of the microstructure and properties of a cast Ni-base superalloy [J]. Mater. Sci. Eng. A., 2012, 543: 121 doi: 10.1016/j.msea.2012.02.059
10	Yang L, Chen M, Wang J, et al. Microstructure and composition evolution of a single-crystal superalloy caused by elements interdiffusion with an overlay NiCrAlY coating on oxidation [J]. J Mater Sci Technol., 2020, 45: 49 doi: 10.1016/j.jmst.2019.11.017
11	Alam M Z, Satyanarayana D V V, Chatterjee D, et al. Creep behavior of Pt-aluminide (PtAl) coated directionally solidified Ni-based superalloy CM-247LC after thermal exposure [J]. Mater. Sci. Eng. A., 2015, 641: 84 doi: 10.1016/j.msea.2015.06.011
12	Zhang J C, Liu L, Huang T W, et al. Coarsening kinetics of γ' precipitates in a Re-containing Ni-based single crystal superalloy during long-term aging [J]. J Mater Sci Technol., 2021, 62(03): 1 doi: 10.1016/j.jmst.2020.05.034
13	Moshtaghin R S, Asgari S. Growth kinetics of γ' precipitates in superalloy IN-738LC during long term aging [J]. Mater. Des., 2003, 24(5): 325 doi: 10.1016/S0261-3069(03)00061-X
14	Chen X, Yao Z, Dong J, et al. The effect of stress on primary MC carbides degeneration of Waspaloy during long term thermal exposure [J]. J. Alloys Compd., 2018, 735: 928 doi: 10.1016/j.jallcom.2017.11.166
15	Tan Z, Yang L, Wang X, et al. Evolution of TCP phase during long term thermal exposure in several Re-Containing single crystal superalloys [J]. Acta. Metall. Sin. (English Letters), 2020, 33(5): 731
16	Dubiel B, Indyka P, Kalemba-Rec I, et al. The influence of high temperature annealing and creep on the microstructure and chemical element distribution in the γ, γ' and TCP phases in single crystal Ni-base superalloy [J]. J. Alloys Compd., 2018, 731: 693 doi: 10.1016/j.jallcom.2017.10.076
17	Yuan K, Eriksson R, Lin P R, et al. Modeling of microstructural evolution and lifetime prediction of MCrAlY coatings on nickel based superalloys during high temperature oxidation [J]. Surf. Coat. Technol., 2013, 232: 204 doi: 10.1016/j.surfcoat.2013.05.008
18	Yang H Z, Zou J P, Shi Q, et al. Comprehensive study on the microstructure evolution and oxidation resistance performance of NiCoCrAlYTa coating during isothermal oxidation at High temperature [J]. Corros Sci., 2020, 175: 108889 doi: 10.1016/j.corsci.2020.108889
19	Angenete J, Stiller K, Bakchinova E. Microstructural and microchemical development of simple and Pt-modified aluminide diffusion coatings during long term oxidation at 1050℃ [J]. Surf. Coat. Technol., 2004, 176(3): 272 doi: 10.1016/S0257-8972(03)00767-9
20	Rahmani K, Nategh S. Influence of aluminide diffusion coating on the tensile properties of the Ni-base superalloy René 80 [J]. Surf. Coat. Technol., 2008, 202(8): 1385 doi: 10.1016/j.surfcoat.2007.06.041
21	Alam M Z, Satyanarayana D V V, Chatterjee D, et al. Effect of prior cyclic oxidation on the creep behavior of directionally solidified (DS) CM-247LC alloy [J]. Mater. Sci. Eng. A., 2012, 536: 14 doi: 10.1016/j.msea.2011.10.016
22	Li S, Qi H, Yang X. Oxidation-induced damage of an uncoated and coated nickel-based superalloy under simulated gas environment [J]. Rare Metals, 2018, 37(3): 204 doi: 10.1007/s12598-017-0931-8
23	Han L, Zheng S, Tao M, et al. Service damage mechanism and interface cracking behavior of Ni-based superalloy turbine blades with aluminized coating [J]. Int J Fatigue., 2021, 153: 106500 doi: 10.1016/j.ijfatigue.2021.106500
24	Han L, Li P, Yu S, et al. Creep/fatigue accelerated failure of Ni-based superalloy turbine blade: Microscopic characteristics and void migration mechanism [J]. Int J Fatigue., 2022, 154: 106558 doi: 10.1016/j.ijfatigue.2021.106558
25	Shi L, Xin L, Wang X, et al. Influences of MCrAlY coatings on oxidation resistance of single crystal superalloy DD98M and their inter-diffusion behaviors [J]. J. Alloys Compd., 2015, 649: 515 doi: 10.1016/j.jallcom.2015.07.095
26	Liu C T, Ma J, Sun X F, et al. Mechanism of the oxidation and degradation of the aluminide coating on the nickel-base single-crystal superalloy DD32M [J]. Surf. Coat. Technol., 2010, 204(21): 3641 doi: 10.1016/j.surfcoat.2010.04.041
27	Leng W, Pillai R, Naumenko D, et al. Effect of substrate alloy composition on the oxidation behaviour and degradation of aluminide coatings on two Ni base superalloys [J]. Corros Sci., 2020, 167: 108494 doi: 10.1016/j.corsci.2020.108494
28	Aghaie-Khafri M, Farahany S. Creep life prediction of thermally exposed rene 80 superalloy [J]. J. Mater. Eng. Perform., 2010, 19(7): 1065 doi: 10.1007/s11665-009-9584-6
29	Yin B, Xie G, Lou L, et al. Effect of Ta on microstructural evolution of NiCrAlYSi coated Ni-base single crystal superalloys [J]. J. Alloys Compd., 2020, 829: 154440 doi: 10.1016/j.jallcom.2020.154440
30	Walston W S, Schaeffer J C, Murphy W H. A new type of microstructural instability in superalloys-SRZ [J]. Superalloys, 1996: 9
31	Chen M, Shen M, Zhu S, et al. Effect of sand blasting and glass matrix composite coating on oxidation resistance of a nickel-based superalloy at 1000℃ [J]. Corros Sci., 2013, 73: 331 doi: 10.1016/j.corsci.2013.04.022
32	Li J, Jing J, He J, et al. Microstructure evolution and elemental diffusion behavior near the interface of Cr₂AlC and single crystal superalloy DD5 at elevated temperatures [J]. Mater. Des., 2020, 193:108776 doi: 10.1016/j.matdes.2020.108776
33	Liu Y, Zou M, Su H, et al. Coating-associated microstructure evolution and elemental interdiffusion behavior at a Mo-rich nickel-based superalloy [J]. Surf. Coat. Technol., 2021, 411: 127005 doi: 10.1016/j.surfcoat.2021.127005
34	Liu L R, Jin T, Zhao N R, et al. Formation of carbides and their effects on stress rupture of a Ni-base single crystal superalloy [J]. Mater. Sci. Eng. A., 2003, 361(1): 191 doi: 10.1016/S0921-5093(03)00517-3
35	Xiang X, Yao Z, Dong J, et al. Dissolution behavior of intragranular M₂₃C₆ carbide in 617B Ni-base superalloy during long-term aging [J]. J. Alloys Compd., 2019, 787: 216 doi: 10.1016/j.jallcom.2019.01.389
36	Zhan X, Wang D, Ge Z, et al. Microstructural evolution of NiCoCrAlY coated directionally solidified superalloy [J]. Surf. Coat. Technol., 2022, 440: 128487 doi: 10.1016/j.surfcoat.2022.128487
37	Campbell C E. Assessment of the diffusion mobilites in the γ' and B2 phases in the Ni-Al-Cr system [J]. Acta Mater., 2008, 56(16): 4277 doi: 10.1016/j.actamat.2008.04.061
38	Suzuki A, Rae C M F. Secondary reaction zone formations in coated Ni-base single crystal superalloys [J]. J Phys Conf Ser., 2009, 165: 12002 doi: 10.1088/1742-6596/165/1/012002
39	Pollock T M, Argon A S. Directional coarsening in nickel-base single crystals with high volume fractions of coherent precipitates [J]. Acta Metall. Mater., 1994, 42(6): 1859 doi: 10.1016/0956-7151(94)90011-6

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