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Chinese Journal of Materials Research  2023, Vol. 37 Issue (10): 731-738    DOI: 10.11901/1005.3093.2022.574
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Effect of Reinforced Particle Size on the Microstructure and Tensile Properties of B4C/Al-Zn-Mg-Cu Composites
XIE Donghang1,3, PAN Ran2, ZHU Shize3, WANG Dong3(), LIU Zhenyu3, ZAN Yuning3, XIAO Bolv3, MA Zongyi3
1.School of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, China
2.AVIC Manufacturing Technology Institute, Beijing 100024, China
3.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
Cite this article: 

XIE Donghang, PAN Ran, ZHU Shize, WANG Dong, LIU Zhenyu, ZAN Yuning, XIAO Bolv, MA Zongyi. Effect of Reinforced Particle Size on the Microstructure and Tensile Properties of B4C/Al-Zn-Mg-Cu Composites. Chinese Journal of Materials Research, 2023, 37(10): 731-738.

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Abstract  

Composites 15%B4C/Al-6.5Zn-2.8Mg-1.7Cu with various size (7 μm, 14 μm, 20 μm) of reinforced paricales B4C were prepared by powder metallurgy vacuum hot pressing method. B4C particles can be uniformly distributed in the three composite materials, and the B4C-Al interface reaction is relatively slight, and no obvious interfacial reaction products are observed. In the matrix of the three composites, the size of the precipitates is basically the same, all of which are about 5.5 nm. When the B4C particle size is 7 μm, the composite has the best performance, i.e., yield strength of 648 MPa, tensile strength of 713 MPa and elongation of 3.3%. With the increase of particle size, the strength and elongation of the composites decreased. The strengthening mechanism and fracture mechanism of the three composites were analyzed, and the results showed that the composite reinforced with smaller B4C particles had higher strength. The particles are not easy to break during deformation, so they have better plasticity.

Key words:  composites      Al alloy matrix      powder metallurgy      interface reaction      particle size      mechanical properties     
Received:  31 October 2022     
ZTFLH:  TB333  
Fund: National Key Research and Development Program of China(2021YFA1600704);Beijing Municipal Natural Science Foundation(3214053);Liaoning Province Xingliao Talent Program Project(XLYC2007009)
Corresponding Authors:  WANG Dong, Tel: (024)23971752, E-mail: dongwang@imr.ac.cn

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2022.574     OR     https://www.cjmr.org/EN/Y2023/V37/I10/731

Fig.1  OM images of 15 %B4C/Al-6.5Zn-2.8Mg-1.7Cu composites with various particle sizes (a) 7 μm, (b) 14 μm, (c) 20 μm
Fig.2  SEM micrographs of 15 %B4C/Al-6.5Zn-2.8Mg-1.7Cu composites with various particle sizes (a) 7 μm, (b) 14 μm, (c) 20 μm, (d,e,f) EDS analysis of particles pointed out by white arrows in (a,b,c)
Fig.3  XRD patterns of B4Cp/Al-Zn-Mg-Cu composites with varying particle sizes in artificial aging state (a) 7 μm, (b) 14 μm, (c) 20 μm
Fig.4  Bright-field TEM images of artificially aged composites taken along [110]Al zone axis (a, d) 7 μm, (b, e) 14 μm, (c, f) 20 μm

Particle

size

/ μm

Tensile strength

/ MPa

Yield strength

/ MPa

Elongation

/%

7714±12648±113.3±0.9
14681±3622±82.0±0.1
20637±1610±91.0±0.1
Table 1  Tensile properties of 15%B4C/Al-6.5Zn-2.8Mg-1.7Cu composites with various particle sizes
Fig.5  Fractographs of 15%B4C/Al-6.5Zn-2.8Mg-1.7Cu composites with various particle sizes (a) 7 μm, (b) 14 μm, (c) 20 μm
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