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Chinese Journal of Materials Research  2017, Vol. 31 Issue (10): 728-736    DOI: 10.11901/1005.3093.2016.055
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Crack Propagation Behavior during DWTT for X80 Pipeline Steel Processed via Ultra-fast Cooling Technique
Jinhua ZHAO1, Xueqiang WANG1,2, Jian KANG1, Guo YUAN1(), Hongshuang DI1
1 State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, China
2 Shougang Qian'an Iron&Steel Co., Ltd, Qian'an 064404, China
Cite this article: 

Jinhua ZHAO, Xueqiang WANG, Jian KANG, Guo YUAN, Hongshuang DI. Crack Propagation Behavior during DWTT for X80 Pipeline Steel Processed via Ultra-fast Cooling Technique. Chinese Journal of Materials Research, 2017, 31(10): 728-736.

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Abstract  

The microstructure and crystallographic features of X80 pipeline steel of 18.4 mm in thickness, which was prepared by ultra-fast cooling (UFC) technique, were characterized by means of optical microscope, electron scanning microscopy, and EBSD technique. The performance of the steel by drop weight tear test (DWTT) was investigated in terms of the crack propagation and the morphology of fractured surfaces, while the mechanism related with the crack arresting ability of the steel resulted from UFC treatment was revealed . The results show that the microstructure of the steel is primarily composed of AF, CB, and M/A island, and the area fractions of AF and CB are ~83%, and ~17%, respectively. The effective grain size is ~3.5 μm, and the fraction of high-angle boundary is ~40.9%. The steel with higher fractions of AF and small-sized M/A island possesses smaller effective grain size, which is beneficial to the crack arresting ability of the steel. The mechanisms related to the enhancement of the crack arresting property may be ascribed to that the UFC promots the formation of AF, and increases the amount of small-sized M/A island by increasing cooling rate. Additionally, the variant selection during bainite transformation is weakened by UFC. Thus, the effective grain size is decreased, and the density of high-angle boundary is increased.

Key words:  microstructure      structure      defects and properties      ultra-fast cooling      AF transformation      X80 pipeline steel      crack arresting mechanism     
Received:  13 January 2016     
ZTFLH:  TG142  
Fund: Supported by National Science-technology Support Plan Projects of China (No.2012BAF04B01), and National Natural Science Foundation of China (No.51504063)

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https://www.cjmr.org/EN/10.11901/1005.3093.2016.055     OR     https://www.cjmr.org/EN/Y2017/V31/I10/728

Element C Si Mn P S Nb+V+Ti Cr+Mo
Content 0.052 0.204 1.80 0.01 0.001 ≤0.13 ≤0.52
Table 1  Chemical composition of experimental steel (%, mass fraction)
Fig.1  Schematic diagram of DWTT specimen
Fig.2  Schematic diagram of observation section for crack propagation
Fig.3  Microstructural characterization at mid-thickness (a) optical micrograph; (b) morphological micrograph
Fig.4  EBSD analysis data of experimental steel (a) orientation distribution map; (b) distribution of grain boundary; (c) distribution of misorientation between different grains; (d) variation trend of misorientation along Line 1, and Line 2
Fig.5  Crystallization relationship between different AF (a) orientation distribution map and (b) pole figure of {001}
No. Orientation Rotational operation Variants
1 {203}[-4-13] - -
2 {113}[4-2-1] [-122],53.8° V17
3 {013}[-23-1] [-623],44.2° V18
4 {112}[-631] [-2-21],52.5° V10
5 {113}[8-3-2] [-133],52.9° V17
6 {325}[-431] [-3-13],56.3° V17
7 {115}[7-2-1] [-1-6-5],53.9° V9
8 {001}[-410] [-312],42.3° V18
Table 2  Crystallographic orientation relationship of different grains showing in Fig.5a
Tensile testing results 30° charpy impact absorbed energy (-20℃)/J 30° DWTT (-15℃)/%
Rt0.5/MPa Rm/MPa Elongation/%, A50 Yield ratio 1# 2# 3# Average 1# 2# Average
Studied steel 570 694 27.9 0.82 426 336 422 395 100 100 100
ASTM A370 555~690 625~825 ≥18 ≤0.93 Single ≥180,Average ≥240 Single ≥70,Average ≥85
Table 3  Mechanical Properties of experimental steel
Fig.6  DWTT fracture of studied X80 pipeline steel
Fig.7  Fracture of DWTT residual sample of studied X80 hot strip: (a)-(d) corresponds to P1 to P4
Fig.8  Crack propagation path at initiation and transition process
Fig.9  Crack propagation path at stable fracture zone
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