Please wait a minute...
Chinese Journal of Materials Research  2015, Vol. 29 Issue (6): 439-444    DOI: 10.11901/1005.3093.2014.617
Current Issue | Archive | Adv Search |
Effect of Cold Deformation on Microstructure and Mechanical Behavior of Ni-based High Temperature Alloy GH3535
Jinhui FAN1,Kexin CHEN1,2,3,Jianping LIANG2,3,**(),Zhijun LI2,3,Xiaoke LI2,3
1. College of Mechanical Engineering, Donghua University, Shanghai 201620, China
2. Shanghai Institute of Applied Physics, Chinese Academy of Sciences , Shanghai 201800, China
3. Key Laboratory of Nuclear Radiation and Nuclear Energy Technology, Chinese Academy of Sciences,
Cite this article: 

Jinhui FAN,Kexin CHEN,Jianping LIANG,Zhijun LI,Xiaoke LI. Effect of Cold Deformation on Microstructure and Mechanical Behavior of Ni-based High Temperature Alloy GH3535. Chinese Journal of Materials Research, 2015, 29(6): 439-444.

Download:  HTML  PDF(4110KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

The effect of extensometer induced cold-tesile deformation on microstructure and mechanical properties of Ni-based high temperature alloy GH3535 were investigated by means of OM and TEM as well as measurement of true stress-true stain curves. It was found that GH3535 alloy shows characteristics of strong work hardening; cold deformation can result in significant increase of its strength and hardness, whereas decrease of its ductility. With the increase of deformation degree grains were elongated along the deformation direction and twins became profusely lager. The work hardening kinetics of GH3535 alloy is constant with Ludwigson model, dislocation slipping and twin are the main deformation mechanism. With the increase of deformation degree the slip behavior of dislocations changes from single slip to cross slip. When the deformation degree below 30% the work hardening is mainly caused by the dislocation long-range stress field and twin, conversely, for the deformation degree above 30% work hardening is mainly caused by the dislocation short-range stress field and deformation twin.

Key words:  metallic materials      nickel-based superalloy      cold deformation      microstructure      mechanical property     
Received:  24 October 2014     
Fund: *Supported by the Program of International S&T Cooperation, ANSTO-SINAP No. 2014DFG60230, National Natural Science Foundation of China Nos. 51371188 & 51371189, and Strategic Priority Research Program of the Chinese Academy of Science No. XD02004210.

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2014.617     OR     https://www.cjmr.org/EN/Y2015/V29/I6/439

Fig.1  Microstructures of samples with different cold deformation degree (a) 0%, (b) 4%, (c) 7%, (d) 10%, (e) 20%, (f) 30%, (g) 40%
Fig.2  True stress-true stain curves of samples with different cold deformation degree
Fig.3  Mechanical properties of samples with different cold deformation degree
Fig.4  Hardness of different material with different cold deformation degree
Fig.5  lg-lg scale true stress vs true stain curves of samples with different cold deformation degree
Cold deformation/% K1/MPa n1 K2 -n2 εL
0 2091.7 0.53 5.52 17.4 0.317
4 2029.9 0.45 5.76 22.1 0.260
7 1966.6 0.40 5.81 24.1 0.241
10 1910.0 0.35 5.84 26.9 0.217
20 1675.6 0.19 5.87 43.6 0.13
30 1447.9 0.09 2.43 -0.25 0
40 1432.8 0.04 -22.2 -1.04 0
Table 1  Ludwigson regression results of samples with different cold deformation degree
Fig.6  TEM micrographs of samples with different cold deformation degree (a) 0%, (b) 7%, (c) 20%, (d) 20%, (e) 40%
1 T. Abram, S. Ion,Generation-IV nuclear power: A review of the state of the science, Energy Policy, 36(12), 4323(2008)
2 H. E. McCoy Jr,Status of materials development for molten salt reactors, ORNL/TM-5920, (1978)
3 P. Hosnedl, O. Matal,Development of structural material and equipment for molten salt technology, Pyrochemical separations, 197(2001)
4 YONG Qilong, The Second Phase in Steel Materials (Beijing, Metallurgical Industry Press, 2006)p.30
4 (30)
5 Haynes International Inc,Fabrication of Hastelloy Corrosion-Resistant Alloys, H-2010F, 27(2003)
6 E. Voce,The relationship between stress and strain for homogeneous deformation, J. Inst. Met., 74, 537(1948)
7 H. W. Swift,Plastic instability under plane stress, Journal of the Mechanics and Physics of Solids, 1(1), 1(1952)
8 Ludwigson,Modified stress-strain relation for FCC metals and alloys, Metallurgical Transactions, 2(10), 2825(1971)
9 WANG Songtao,YANG Ke,SHAN Yiyin , LI Laifeng, Effects of cold deformation on microstructure and mechanical behavior of a high nitrogen austenitic stainless steel, Acta Metallurgica Sinica, 43(7), 713(2007)
9 (王松涛, 杨 柯, 单以银, 李来风, 冷变形对高氮奥氏体不锈钢组织与力学行为的影响, 金属学报, 43(7), 713(2007))
10 WANG Congzeng, Properties of Materials (Beijing, Beijing University of Technology Press, 2001)p.21
10 (21)
11 LIU Shuxun,LIU Xianmin, LIU Rui, WANG Chunxu, XING Feng, Work-hardening behavior of 0Cr21Ni6Mn9N austenitic stainless steel, Journal of Iron and Steel Research, 17(4), 40(2006)
11 (刘树勋, 刘宪民, 刘 蕤, 王春旭, 邢峰, 0Cr21Ni6Mn9N奥氏体不锈钢的应变强化行为, 钢铁研究学报, 17(4), 40(2006))
12 LIU Shuxun,LIU Xianmin,WANG Weiming , Effect of cold deformation on mechanical properties of 0Cr21Ni6Mn9N stainless steel, Iron Steel, 40(11), 67(2005)
12 (刘树勋, 刘宪民, 王维明, 不同变形量对0Cr21Ni6Mn9N不锈钢力学性能的影响, 钢铁, 40(11), 67(2005))
13 ZHANG Songchuang,ZHENG Wenjie, SONG Zhigang, FENG Han, SUN Yong, Effect of cold deformation on structure and mechanical behavior of Inconel 690 alloy, Journal of Iron and Steel Research, 21(12), 49(2009)
13 (张松闯, 郑文杰, 宋志刚, 丰 涵, 孙 勇, 冷变形对Inconel 690合金力学行为与组织的影响, 钢铁研究学报, 21(12), 49(2009))
14 S. Mahajan,Critique of mechanisms of formation of deformation, annealing and growth twins: face-centered cubic metals and alloys, Scripta Materialia, 68(2), 95(2013)
15 J. Narayan, Y. T. Zhu,Self-thickening, cross-slip deformation twinning model, Applied Physics Letters, 92(15), 151908(2008)
16 J. A. Venables,The nucleation and propagation of deformation twins, Journal of Physics and Chemistry of Solids, 25(7), 693(1964)
17 Y. Zhang, N. R. Tao, K. Lu,Effect of stacking-fault energy on deformation twin thickness in Cu-Al alloys, Scripta Materialia, 60(4), 211(2009)
18 WANG Songtao,Mechanical behavior and mechanisms of nitrogen effect of high nitrogen austenitic stainless steels, PhD Thesis(Beijing, Graduate School of Chinese Academy of Sciences, 2008)
18 (王松涛, 高氮奥氏体不锈钢的力学行为及氮的作用机理, 博士学位论文(北京, 中国科学院研究生院, 2008))
19 G. Saller, K. Spiradek-Hahn, C. Scheu, H. Clemens,Microstructural evolution of Cr–Mn–N austenitic steels during cold work hardening, Materials Science and Engineering: A, 427(1), 246(2006)
[1] MAO Jianjun, FU Tong, PAN Hucheng, TENG Changqing, ZHANG Wei, XIE Dongsheng, WU Lu. Kr Ions Irradiation Damage Behavior of AlNbMoZrB Refractory High-entropy Alloy[J]. 材料研究学报, 2023, 37(9): 641-648.
[2] SONG Lifang, YAN Jiahao, ZHANG Diankang, XUE Cheng, XIA Huiyun, NIU Yanhui. Carbon Dioxide Adsorption Capacity of Alkali-metal Cation Dopped MIL125[J]. 材料研究学报, 2023, 37(9): 649-654.
[3] ZHAO Zhengxiang, LIAO Luhai, XU Fanghong, ZHANG Wei, LI Jingyuan. Hot Deformation Behavior and Microstructue Evolution of Super Austenitic Stainless Steel 24Cr-22Ni-7Mo-0.4N[J]. 材料研究学报, 2023, 37(9): 655-667.
[4] SHAO Hongmei, CUI Yong, XU Wendi, ZHANG Wei, SHEN Xiaoyi, ZHAI Yuchun. Template-free Hydrothermal Preparation and Adsorption Capacity of Hollow Spherical AlOOH[J]. 材料研究学报, 2023, 37(9): 675-684.
[5] XING Dingqin, TU Jian, LUO Sen, ZHOU Zhiming. Effect of Different C Contents on Microstructure and Properties of VCoNi Medium-entropy Alloys[J]. 材料研究学报, 2023, 37(9): 685-696.
[6] OUYANG Kangxin, ZHOU Da, YANG Yufan, ZHANG Lei. Microstructure and Tensile Properties of Mg-Y-Er-Ni Alloy with Long Period Stacking Ordered Phases[J]. 材料研究学报, 2023, 37(9): 697-705.
[7] PAN Xinyuan, JIANG Jin, REN Yunfei, LIU Li, LI Jinghui, ZHANG Mingya. Microstructure and Property of Ti / Steel Composite Pipe Prepared by Hot Extrusion[J]. 材料研究学报, 2023, 37(9): 713-720.
[8] XU Lijun, ZHENG Ce, FENG Xiaohui, HUANG Qiuyan, LI Yingju, YANG Yuansheng. Effects of Directional Recrystallization on Microstructure and Superelastic Property of Hot-rolled Cu71Al18Mn11 Alloy[J]. 材料研究学报, 2023, 37(8): 571-580.
[9] XIONG Shiqi, LIU Enze, TAN Zheng, NING Likui, TONG Jian, ZHENG Zhi, LI Haiying. Effect of Solution Heat Treatment on Microstructure of DZ125L Superalloy with Low Segregation[J]. 材料研究学报, 2023, 37(8): 603-613.
[10] LIU Jihao, CHI Hongxiao, WU Huibin, MA Dangshen, ZHOU Jian, XU Huixia. Heat Treatment Related Microstructure Evolution and Low Hardness Issue of Spray Forming M3 High Speed Steel[J]. 材料研究学报, 2023, 37(8): 625-632.
[11] YOU Baodong, ZHU Mingwei, YANG Pengju, HE Jie. Research Progress in Preparation of Porous Metal Materials by Alloy Phase Separation[J]. 材料研究学报, 2023, 37(8): 561-570.
[12] REN Fuyan, OUYANG Erming. Photocatalytic Degradation of Tetracycline Hydrochloride by g-C3N4 Modified Bi2O3[J]. 材料研究学报, 2023, 37(8): 633-640.
[13] WANG Hao, CUI Junjun, ZHAO Mingjiu. Recrystallization and Grain Growth Behavior for Strip and Foil of Ni-based Superalloy GH3536[J]. 材料研究学报, 2023, 37(7): 535-542.
[14] LIU Mingzhu, FAN Rao, ZHANG Xiaoyu, MA Zeyuan, LIANG Chengyang, CAO Ying, GENG Shitong, LI Ling. Effect of Photoanode Film Thickness of SnO2 as Scattering Layer on the Photovoltaic Performance of Quantum Dot Dye-sensitized Solar Cells[J]. 材料研究学报, 2023, 37(7): 554-560.
[15] QIN Heyong, LI Zhentuan, ZHAO Guangpu, ZHANG Wenyun, ZHANG Xiaomin. Effect of Solution Temperature on Mechanical Properties and γ' Phase of GH4742 Superalloy[J]. 材料研究学报, 2023, 37(7): 502-510.
No Suggested Reading articles found!