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Chinese Journal of Materials Research  2016, Vol. 30 Issue (10): 767-772    DOI: 10.11901/1005.3093.2015.325
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Strain Aging Behavior of X70 Pipeline Steel
Yongwen JIANG1,**(),Tao NIU1,Chenggang AN1,Xinlang WU2,Caixia ZHANG2,Xiaoli DAI1
1. Shougang Research Institute of Technology, Beijing 100043, China
2. Shougang Qian’an Iron &Steel Co.Ltd, Qian’an 064404, China;
Cite this article: 

Yongwen JIANG,Tao NIU,Chenggang AN,Xinlang WU,Caixia ZHANG,Xiaoli DAI. Strain Aging Behavior of X70 Pipeline Steel. Chinese Journal of Materials Research, 2016, 30(10): 767-772.

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Abstract  

Effect of pre-strain and aging temperature on mechanical property and microstructure of X70 pipeline steel was investigated by means of scanning electron microscope ( SEM ) and transmission electron microscope ( TEM ). The results indicate that the X70 steel shows a microstructure compopsed of granular bainite, acicular ferrite and M/A. The aging temperatures below 300℃, exhibit nearly no effect on the microstructure and the tensile strength of the steel. With the rising of aging temperature, the quantity of activated interstitial atoms, therewith, the pinning effect on dislocations increases, which leads to the gradual increase of the yield strength; However, when the temperature raises to above 200℃, the recovery of pinning effect occurs resulting in the decline of the yield strength. With the rising of aging temperature, the hardening of material induced by the increased cottrell atmosphere and precipitations leads to the decline of the impact toughness. With the increase of the pre-strain, the increment of dislocations may lead to the increase of yield strength, and the stress concentration will increase at boundries of the hard brittle phase M/A, therewith increase the probability of the formation micro-cracks, as a result, the impact toughness delines.

Key words:  metal materials      X70 pipeline steel      strain aging      mechanical properties      microstructure     
Received:  12 October 2015     

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2015.325     OR     https://www.cjmr.org/EN/Y2016/V30/I10/767

Element C Si Mn Nb+V+Ti Mo Others
Content ≤0.07 0.10~0.30 1.50~1.80 ≤0.10 0.10~0.30 Cr、Cu、Ni
Table 1  Chemical composition of experimental steel (%, mass fraction)
No. Pre-strain/% Aging temperature/℃ Holding time/min Cooling mode
1-1 3 RT / /
1-2 3 150 10 AC
1-3 3 200 10 AC
1-4 3 250 10 AC
1-5 3 300 10 AC
Table 2  Test scheme of different aging temperature
No. Pre-strain/% Aging temperature/℃ Holding time/min Cooling mode
2-1 Rolled / / /
2-2 0 200 10 AC
2-3 1 200 10 AC
2-4 2 200 10 AC
2-5 3 200 10 AC
Table 3  Test scheme of different re-strain
Fig.1  Mechanical properties variation with different aging temperatures (a) strength; (b) Y/T; (c) elongation; (d) impact absorbing energy
Fig.2  Mechanical properties variation with different pre-strain (a) strength; (b) Y/T; (c) elongation; (d) impact absorbing energy
Fig.3  Partial enlarged detail of tensile curve with different pre-strain
Fig.4  Microstructure comparison at different aging temperatures (SEM) (a) Rolled; (b) 150℃; (c) 250℃; (d) 300℃
Fig.5  Impact fracture with different pre-strain (a) Rolled; (b) 3%/300℃
Fig.6  Dislocation of X70 with different aging temperature (a) Room temperature; (b) 300℃
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