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Effect of Graphitization Degree of Mesophase Pitch-based Carbon Fibers on Carbon Fiber/Al Interface Damage |
ZHANG Peng1, HUANG Dong1,2, ZHANG Fuquan1( ), YE Chong1,2, WU Xiao1,2, WU Huang1 |
1.College of Materials Science and Engineering, Hunan Province Key Laboratory for Advanced Carbon Materials and Applied Technology, Hunan University, Changsha 410082, China 2.Hunan Province Engineering Research Center for High Performance Pitch-based Carbon Materials, Hunan Toyi Carbon Material Technology Co. Ltd., Changsha 410006, China |
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Cite this article:
ZHANG Peng, HUANG Dong, ZHANG Fuquan, YE Chong, WU Xiao, WU Huang. Effect of Graphitization Degree of Mesophase Pitch-based Carbon Fibers on Carbon Fiber/Al Interface Damage. Chinese Journal of Materials Research, 2022, 36(8): 579-590.
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Abstract Composite of carbon fiber (Cf) with Al-film (Cf/Al) was constructed by magnetron sputtering with mesophase pitch-based carbon fibers of different graphitization degrees as matrix and Al-plate as sputtering target. Then, the microstructure evolution of Cf /Al interface of the prepared composites was investigated, and the damage mechanism of Cf /Al interface was revealed in comparison to that prepared with polyacrylonitrile carbon fiber. The results show: With the increase of graphitization temperature, the size, the degree of orientation and graphitization of graphite micro-crystallites in mesophase asphalt based carbon fiber increased, whilst both of the reaction degree of Cf /Al interface and the damage of carbon fiber reduced. The damage of Cf /Al interface of the composites prepared with Cf of different graphitization degrees depends on the number of initial defects and the propagation of subsequent cracks in the carbon fiber. The graphitization treatment at 2400℃ and 2700℃ could facilitate the crack propagation through graphite micro-lamellas located in between mesophase asphalt-based carbon fibers, however after removing the Al-coating, the fiber damage was 5.19% and 3.70% higher than that of polyacrylonitrile carbon fiber respectively. After graphitization at 3000℃, the mesophase bituminous carbon fiber with higher chemical inertia could reduce the number of defects generated by interfacial reaction, whilst, after removing the Al-coating, the damage of the fiber was 1.85% lower than that of polyacrylonitrile carbon fiber.
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Received: 15 March 2021
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Fund: National Natural Science Foundation of China(52002104);Special Fund for Innovative Construction of Hunan Province(2020RC3075);Special Fund for Innovative Construction of Hunan Province(2019RS2058);Special Fund for Innovative Construction of Hunan Province(2019GK2021);Special Fund for Innovative Construction of Hunan Province(2020GK4029);Postdoctoral Science Foundation(2020M672480) |
About author: ZHANG Fuquan, Tel: 13907488966, E-mail: zhangfq@hnu.edu.cn
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