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Chinese Journal of Materials Research  2020, Vol. 34 Issue (12): 881-891    DOI: 10.11901/1005.3093.2020.199
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Influence of Modification, Refinement and Heat Treatment on Mechanical Properties of A356 Al-alloy Components Prepared by Squeeze Casting
JIANG Jufu1(), WANG Ying2, XIAO Guanfei1, DENG Teng1, LIU Yingze1, ZHANG Ying1
1.School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China
2.School of Mechatronics Engineering, Harbin Institute of Technology, Harbin 150001, China
Cite this article: 

JIANG Jufu, WANG Ying, XIAO Guanfei, DENG Teng, LIU Yingze, ZHANG Ying. Influence of Modification, Refinement and Heat Treatment on Mechanical Properties of A356 Al-alloy Components Prepared by Squeeze Casting. Chinese Journal of Materials Research, 2020, 34(12): 881-891.

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Abstract  

Influence of modification, refinement and heat treatment on the microstructure and mechanical properties of A356 Al-alloy components prepared by squeeze casting was investigated. The results show that with increase of Al-10Sr modification agent, the morphology of eutectic Si changed from lamellar, rod-like shape to granular and wormlike shape, and the grain size of α-Al increased first and then decreased. When 0.3% Al-10Sr modification agent was added, the optimal mechanical properties of squeeze casting components including ultimate tensile strength of 221.3 MPa, yield strength of 104.5 MPa and elongation of 10.3% were achieved. The improvement of mechanical properties can be attributed to the increase of nucleation rate, the decrease of α-Al grain size and the change of eutectic Si morphology by adding 0.3% Al-10Sr modification agent. With the increase of A-5Ti-B refiner, the α-Al grain size first decreased and then increased, but the changing trend of mechanical properties is inverse. When 0.6% Al-5Ti-B refiner was added, the optimal ultimate tensile strength, yield strength and elongation were 215.6 MPa, 106.6 MPa and 9.0%, respectively. T6 heat treatment including solid solution at 540℃ for 4 h and artificial aging at 190℃ for 4 h led to the improvement of yield strength and ultimate tensile strength, but it led to the decrease of elongation. The optimal mechanical properties such as yield strength of 239.3 MPa, ultimate tensile strength of 297.5 MPa and elongation of 8.0% were obtained for the squeeze casting component with T6 treatment and an addition of 0.6% A-5Ti-B refiner. The globularization of eutectic Si, the refinement of eutectic Si, the homogenization of composition for the prepared component and the precipitation of Mg2Si phase in α-Al matrix all lead to the improvement of mechanical properties of squeeze casting component with T6 treatment.

Key words:  synthesizing and processing technics for materials      modification and refinement      microstructure      mechanical properties      A356 aluminum alloy      squeeze casting     
Received:  29 May 2020     
ZTFLH:  TG249.9  
Fund: National Key Research and Development Program(2019YFB2006500);National Natural Science Foundation of China(51875124)

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https://www.cjmr.org/EN/10.11901/1005.3093.2020.199     OR     https://www.cjmr.org/EN/Y2020/V34/I12/881

Sample No.Pouring temperature/℃

Die temperature

/℃

Specific pressure

/MPa

Dwell time/sAdded master alloy

Quantity

/%

Heat treatment status
170025039830No0No T6
270025039830Al-10Sr0.1No T6
370025039830Al-10Sr0.3No T6
470025039830Al-10Sr3No T6
570025039830Al-5Ti-B0.1No T6
670025039830Al-5Ti-B0.6No T6
770025039830Al-5Ti-B3No T6
870025039830No0T6
970025039830Al-10Sr0.3T6
1070025039830Al-5Ti-B0.6T6
Table 1  Experimental plan in this research
Fig.1  Three dimension model of squeeze casting component and locations of samples
Fig.2  Microstructure and average grain size of squeeze casting component with different addition quantity of Al-10Sr modifier (a) 0, (b) 0.1%, (c) 0.3%, (d) 3%, (e) 0 (1000x), (f) 0.3% (1000x), (g) average grain size
Fig.3  Mechanical properties of squeeze casting component with different addition quantity of Al-10Sr modifier
Fig.4  Microstructure and average grain size of squeeze casting component with different addition quantity of Al-5Ti-B refiner (a) 0.1%, (b) 0.6%, (c) 3%, (d) average size of grains
Fig.5  Mechanical properties of squeeze casting component with different quantity of Al-5Ti-B refiner
Fig.6  Engineering stress-strain curve of squeeze casting component before and after T6
Fig.7  Microstructure of squeeze casting component with T6 (a) No.8 sample, (b) No.9 sample, (c) No.10 sample
Fig.8  SEM image and EDS of squeeze casting component with 3% addition of Al-10Sr modifier (a) SEM image with scanning line, (b) line scanning of Sr element
Fig.9  SEM image and point scanning EDS of squeeze casting component with 3% addition of Al-10Sr modifier (a) SEM image, (b) point A scanning EDS
Fig.10  Fracture morphology of squeeze casting component (a) low-resolution sample 9, (b) high-resolution sample 9, (c) low-resolution sample 10, (d) high-resolution sample 10
Fig.11  TEM image (a) and EDS mapping images (b) Al, (c) Si, (d) Mn, (e) Mg, (f) Fe
Fig.12  TEM image and selected area electron diffraction (SAED) (a) TEM dark field image, (b) SAED
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