Effect of Polypyrrole Modified Carbon Fiber on Interfacial Property of Composite PPy-carbon Fiber/epoxy

doi:10.11901/1005.3093.2017.422

Chinese Journal of Materials Research

2018, Vol. 32

Issue (3): 209-215 DOI: 10.11901/1005.3093.2017.422

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Effect of Polypyrrole Modified Carbon Fiber on Interfacial Property of Composite PPy-carbon Fiber/epoxy

Wenyu WANG¹, Yamin LIU¹, Xin JIN¹(

), Changfa XIAO¹, Zhengtao ZHU^1,², Tong LIN^1,²

1 School of Materials Science and Engineering, State Key Laboratory of Membrane Separation and Membrane Processing, Tianjin University of Technology, Tianjin 300387, China
2 South Dakota Mining Institute, Rapid City SD57702, United States;

Cite this article:

Wenyu WANG, Yamin LIU, Xin JIN, Changfa XIAO, Zhengtao ZHU, Tong LIN. Effect of Polypyrrole Modified Carbon Fiber on Interfacial Property of Composite PPy-carbon Fiber/epoxy. Chinese Journal of Materials Research, 2018, 32(3): 209-215.

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Abstract

In order to improve the interfacial property of carbon fiber composites, the carbon fiber was pretreated by plasma technique and then coated with polypyrrole (PPy) by chemical oxidation polymerization of pyrrole. The surface modified carbon fiber and composite were characterized by SEM, AFM, XPS, FT-IR and IFSS. Results show that the interfacial shear strength of the modified single fiber increased by 259.3%, which may be ascribed to that the plasma pretreatment can increase the amount of polar groups on the surface of the carbon fiber, and facilitate the formation of hydrogen bonds between the carbon fiber and PPy, thus enhancing the interfacial property of the composite PPy-carbon fiber/epoxy.

Key words: composite polypyrrole plasma hydrogen bond interface shear strength

Received: 12 July 2017

ZTFLH:

TB332

Fund: Supported by National Natural Science Foundation of China (Nos. 51573136 ＆ 51103101), Natural Science Foundation of Tianjin (Nos. 12JCYBJC17800 & 16JCTPJC45100), and the Science and Technology Plan of Tianjin (Nos. 15PTSYJC00230, 15PTSYJC00240 ＆ 15PTSYJC00250)

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	Wenyu WANG
	Yamin LIU
	Xin JIN
	Changfa XIAO
	Zhengtao ZHU
	Tong LIN

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https://www.cjmr.org/EN/10.11901/1005.3093.2017.422 OR https://www.cjmr.org/EN/Y2018/V32/I3/209

Fig.1 Interfacial shear strength (IFSS) of single fiber composites

Fig.2 SEM images of the fracture surface of carbon fiber composite (a) CF, (b) p-CF, (c) PPy-CF, (d) PPy-p-CF

Fig.3 SEM images of the morphologies of the carbon fiber (a) CF, (b) p-CF, (c) PPy-CF, (d) PPy-p-CF

Fig.4 AFM images of different CF surfaces (a) CF, (b) p-CF, (c) PPy-CF, (d) PPy-p-CF

Fig.5 Wide-scan XPS spectra (a) CF, (b) p-CF, (c) PPy-CF, (d) PPy-p-CF

Fig.6 C1s high-resolution XPS element spectra of CF (a), p-CF(b), PPy-CF (c) and PPy-p-CF (d)

Table1 XPS surface element analysis of CF, p-CF, PPy-CF and PPy-p-CF (%, element or group fraction)

Fig.7 Infrared spectra of different samples (a) CF, (b) PPy-CF, (c) PPy-p-CF, (d) PPy

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