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Chinese Journal of Materials Research  2015, Vol. 29 Issue (11): 853-859    DOI: 10.11901/1005.3093.2015.027
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Preparation of Magnesium Doped Hydroxyapatite Coating on Carbon/Carbon Composites
Xinye NI1,2,3,Aijun LI1,Ruicheng BAI1,Xinbo XIONG3,Dong ZHOU2,**()
1. School of Materials Science and Engineering, Shanghai University, Shanghai 200444, China
2. Second People’s Hospital of Changzhou, Nanjing Medical University, Changzhou 213003, China
3. College of Materials Science and Engineering, Shenzhen University, Shenzhen 518060, China
Cite this article: 

Xinye NI,Aijun LI,Ruicheng BAI,Xinbo XIONG,Dong ZHOU. Preparation of Magnesium Doped Hydroxyapatite Coating on Carbon/Carbon Composites. Chinese Journal of Materials Research, 2015, 29(11): 853-859.

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Abstract  

Mg doped hydroxyapatite coatings with 0, 0.28%, 0.32%, 0.49% Mg respectively, as artificial human bones were prepared on carbon / carbon composites by means of electromagnetic induction method. Then they were characterized by SEM, EDS, X-ray diffraction and Fourier transform-infrared spectroscopy etc. The results show that Mg ions entered the hydroxyapatite lattice and these coatings have only a little difference in constituents. Within the range Mg content of human bone, Mg ions can enhance the adhesion, multiplication, and differentiation of external osteoblasts.

Key words:  composites      carbon/carbon composites      magnesium      hydroxyapatite     
Received:  14 January 2015     
Fund: *Supported by Postdoctoral Science Foundation of China No. 2014M560323, the municipal social development project of the Changzhou City No. CJ20130019 and Natural Science Foundation of Jiangsu Province No. BK20151181.

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2015.027     OR     https://www.cjmr.org/EN/Y2015/V29/I11/853

Fig.1  SEM comparison of the coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.2  EDS comparison of the coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.3  XRD comparison of the coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.4  FTIR comparison of the coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.5  Osteoblast (MC3T3-E1) morphologies on the coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.6  Cell quantities of coatings of different magnesium content at different times (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
Fig.7  Fluorescence microscopy map of coatings of different magnesium content (a) Mg0M, (b) Mg0.04M, (c) Mg0.08M, (d) Mg0.16M
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