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材料研究学报  2026, Vol. 40 Issue (6): 465-473    DOI: 10.11901/1005.3093.2025.179
  研究论文 本期目录 | 过刊浏览 |
DD10合金钎焊接头的力学性能
赵欣宇1,2, 刘恩泽1(), 张功1, 赵媛3, 宁礼奎1, 信昕1, 贾丹1, 刘伟华1, 谭政1,2
1.中国科学院金属研究所 沈阳 110016
2.中国科学技术大学材料科学与工程学院 沈阳 110016
3.中国船舶工业物资东北有限公司 沈阳 110011
Mechanical Properties of Brazed Joints of Nickel-based Superalloy DD10
ZHAO Xinyu1,2, LIU Enze1(), ZHANG Gong1, ZHAO Yuan3, NING Likui1, XIN Xin1, JIA Dan1, LIU Weihua1, TAN Zheng1,2
1.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2.School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
3.China Shipbuilding Equipment & Materials Northeast Corporation, Shenyang 110011, China
引用本文:

赵欣宇, 刘恩泽, 张功, 赵媛, 宁礼奎, 信昕, 贾丹, 刘伟华, 谭政. DD10合金钎焊接头的力学性能[J]. 材料研究学报, 2026, 40(6): 465-473.
Xinyu ZHAO, Enze LIU, Gong ZHANG, Yuan ZHAO, Likui NING, Xin XIN, Dan JIA, Weihua LIU, Zheng TAN. Mechanical Properties of Brazed Joints of Nickel-based Superalloy DD10[J]. Chinese Journal of Materials Research, 2026, 40(6): 465-473.

全文: PDF(18169 KB)   HTML
摘要: 

用钴基钎料钎焊DD10单晶合金并对接头进行热处理,使用扫描电子显微镜(SEM)、电子探针(EPMA)和透射电子显微镜(TEM)等手段表征钎焊接头的微观组织,研究了接头的力学性能并探讨了相应的机制。结果表明,对接头的热处理使其析出了M5B3M3B2MC和Ni3Ti相,B元素的扩散使扩散影响区出现了熔池组织。热处理后钎焊接头的室温和高温断裂强度分别为母材的80%和70%。

关键词 金属材料DD10合金钎焊微观组织热处理力学性能    
Abstract

The turbine blades of heavy-duty gas turbines require materials with excellent mechanical properties and hot corrosion resistance. DD10, a hot-corrosion-resistant single-crystal superalloy is the candidate material for manufacturing F-class gas turbine blades, which are usually fabricated via precision investment casting and then brazing to seal the core removal process remaining holes on the blade tip. However, there are relatively few studies on the brazing process for DD10 alloy. Herein, it is attempted to conduct brazing on DD10 single-crystal superalloy with a Co-based alloy as brazing filler metal. The microstructure of the brazed joints was analyzed using scanning electron microscopy (SEM), electron probe microanalysis (EPMA), and transmission electron microscopy (TEM). Mechanical properties of the joints were evaluated, and the underlying mechanisms were explored. The results indicate that in conditions of brazing followed by heat treatment, phases such as M5B3, M3B2, MC, and Ni3Ti precipitated in the weld zone. Additionally, boron (B) diffusion led to the formation of a molten pool-like structure in the diffusion-affected zone. After heat treatment, the rupture strength of the brazed joints reached 80% and 70% of the base metal's strength at room temperature and high temperature, respectively.

Key wordsmetallic materials    DD10 superalloy    brazing    microstructure    heat treatment    mechanical properties
收稿日期: 2025-05-21     
ZTFLH:  TG132.3  
基金资助:国家科技重大专项(E110A104)
通讯作者: 刘恩泽,研究员,nzliu@imr.ac.cn,研究方向为高温结构材料
Corresponding author: LIU Enze, Tel: (024)23971143, E-mail: nzliu@imr.ac.cn
作者简介: 赵欣宇,男,1999年生,硕士生
图1  DD10合金的微观组织
图2  BCo45钎料的形貌和DSC曲线
图3  钎焊装配的示意图
图4  DD10合金钎焊接头的微观组织
图5  1220 ℃/15 min DD10合金钎焊接头中元素的分布
图6  钎焊接头的局部组织
PositionNiCoCrTiAlWTaMoCB
A59.2410.7612.616.716.921.321.320.190.920.00
B58.2612.0315.284.726.021.580.990.220.600.00
C64.378.652.8914.214.570.823.390.061.050.00
D2.860.291.9025.570.027.8519.620.2241.310.35
E6.523.4032.593.900.0014.032.052.590.0034.91
F2.921.8656.901.730.101.790.141.030.0033.53
表1  图6中各点的EPMA分析结果
图7  Ni3Ti相的TEM和选区电子衍射图像
图8  热处理后的钎焊接头和基体线扫描元素分布
图9  扩散影响区内的熔池组织及其元素分布
SampleTemperatureRm / MPa
1Room temperature606
2893
3908
4950 oC531
5567
6486
表2  热处理后钎焊接头的断裂强度
图10  钎焊接头断口的形貌
图11  钎焊接头断口的XRD谱
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