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Chinese Journal of Materials Research  2025, Vol. 39 Issue (11): 801-812    DOI: 10.11901/1005.3093.2024.496
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Effect of Different Heterogeneous Microstructures on Tensile Properties of a High Strength Wind Power Steel Q500MD
CHEN Zihao1,2, GAO Chong2, PANG Jianchao2(), MA Heng3,4, HE Kang3,5, LI Xiaowu1, LI Shouxin2, ZHANG Zhefeng2
1.School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China
2.Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
3.Laiwu Branch Technology Center, Shandong Iron and Steel Co. , Ltd. , Jinan 271104, China
4.School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Beijing 100083, China
5.Collaborative Innovation Center of Steel Technology, University of Science and Technology Beijing, Beijing 100083, China
Cite this article: 

CHEN Zihao, GAO Chong, PANG Jianchao, MA Heng, HE Kang, LI Xiaowu, LI Shouxin, ZHANG Zhefeng. Effect of Different Heterogeneous Microstructures on Tensile Properties of a High Strength Wind Power Steel Q500MD. Chinese Journal of Materials Research, 2025, 39(11): 801-812.

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Abstract  

The effect of different heterogeneous microstructures on the tensile properties of high-strength wind power steel Q500MD, a 500 MPa grade wind power steel was assessed. Hence, the as received steel is subjected to an intercritical annealing combined with quenching or tempering one, namely the following three heterogeneous heat treatments: intercritical annealing, quenching + intercritical annealing and quenching + intercritical annealing + tempering. Then the microstructure and tensile property of the acquired three type steels with different heterogeneous microstructures were examined viauniversal testing machine, scanning electron microscopy and electron backscatter diffraction. The results indicate that the as received steel presents typical thermo-mechanical control process (TMCP) heat treatment microstructure composed of a large amount of acicular ferrite and a small amount of martensite. After heterogeneous heat treatment, their microstructures transform into a heterogeneous microstructure of soft phase intercritical ferrite and hard phase martensite, and the martensite varies with different post heat treatment processes. Specifically, the steel microstructure turns into intercritical ferrite, granular martensite, and fibrous martensite after quenching and intercritical annealing. Due to the existence of heterogeneous nucleation in the intercritical annealing process, new microstructure can be generated and grain refinement can be achieved. The heterogeneous microstructure leads to a low yield ratio and high plasticity of high-strength wind power steels. Compared with the as received steel, the presence of the soft-phase intercritical ferrite alters the initial yield threshold and subsequent work hardening behavior of the steel during tensile deformation, resulting in low yield ratio. Based on the analysis of microstructure evolution and tensile properties of the steels prepared by different heterogeneous heat treatment, it can be concluded that the presence of intercritical ferrite and martensite in the microstructure after intercritical annealing can enhance the strength and plasticity of high-strength wind power steels. Furthermore, incorporating quenching prior to intercritical annealing yields a finer grain structure, thereby further reducing the yield ratio of high-strength wind power steels.

Key words:  metallic materials      high strength wind power steel      intercritical annealing      heterogeneous microstructure      tensile property     
Received:  15 December 2024     
ZTFLH:  TG142.1  
Fund: National Key Research and Development Program of China(2022YFB3708200)
Corresponding Authors:  PANG Jianchao, Tel: (024)83978879, E-mail: jcpang@imr.ac.cn

URL: 

https://www.cjmr.org/EN/10.11901/1005.3093.2024.496     OR     https://www.cjmr.org/EN/Y2025/V39/I11/801

Fig.1  Schematic diagram of heat treatment process of Q500MD steel
Fig.2  Dimensions of the tensile specimen
Fig.3  SEM images showing the microstructures in 500 MPa grade wind power steels with different heat treatment technologies (a) OS, (b) IA, (c) QIA, (d) QIAT
Fig.4  Contrast diagram of the microstructure morphology and boundary distribution in 500 MPa grade wind power steels under different heat treatment technologies (a) OS, (b) IA, (c) QIA, (d) QIAT
Fig.5  KAM diagram of 500 MPa grade wind power steels with different heat treatment technologies (a) OS, (b) IA, (c) QIA, (d) QIAT
SampleYS / MPaUTS / MPaYRZ / %A / %Au / %
OS6227340.8547.2420.126.69
IA5248130.6460.0721.2710.27
QIA4718180.5872.8522.5211.28
QIAT5457220.7574.7923.7512.16
Table 1  Tensile data of 500 MPa grade wind power steels under different heat treatment technologies
Fig.6  Tensile engineering stress-strain curves of 500 MPa grade wind power steels under different heat treatment technologies
Fig.7  SEM images showing the tensile fracture surface morphologies of 500 MPa grade wind power steels with different heat treatment technologies (a, e) OS, (b, f) IA, (c, g) QIA, (d, h) QIAT
Fig.8  Inverse pole figure of 500 MPa grade wind power steels with different heat treatment technologies based on EBSD results (a) OS, (b) IA, (c) QIA, (d) QIAT
Fig.9  Changing process of the microstructures of the steels during heterogeneous heat treatment
Fig.10  Grain size distribution of 500 MPa grade wind power steels with different heat treatment technologies (a) OS, (b) IA, (c) QIA, (d) QIAT
Fig.11  Relationship between average grain size and tensile properties of 500 MPa grade wind power steels under different heat treatment technologies (a) the relationship between average grain size and yield/tensile strengths, (b) the relationship between average grain size and uniform elongation
Fig.12  K-M curves of 500 MPa grade wind power steels with different heat treatment technologies
Fig.13  Changes of tensile properties of 500 MPa grade wind power steels under different heat treatment technologies (a) the relationship between yield strength and tensile strength, (b) the relationship between elongation and tensile strength
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