Preparation and Erosion Performance for Co-continuous Phase Composites of Si3N4/1Cr18Ni9Ti

doi:10.11901/1005.3093.2018.296

Chinese Journal of Materials Research

2019, Vol. 33

Issue (1): 34-42 DOI: 10.11901/1005.3093.2018.296

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Preparation and Erosion Performance for Co-continuous Phase Composites of Si₃N₄/1Cr18Ni9Ti

Qi DU^1,²,Yong GAO¹,Zhiheng REN^1,³,Xiaoming CAO¹,Chao WANG¹,Jinsong ZHANG¹(

)

1. Institute of Metal Research, Chinese Academy of Science, Shenyang 110016, China
2. School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
3. Liaoning ZhuoYi New Materials Corporation, Yingkou 115004, China

Cite this article:

Qi DU,Yong GAO,Zhiheng REN,Xiaoming CAO,Chao WANG,Jinsong ZHANG. Preparation and Erosion Performance for Co-continuous Phase Composites of Si₃N₄/1Cr18Ni9Ti. Chinese Journal of Materials Research, 2019, 33(1): 34-42.

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Abstract

Composites with co-continuous structure of Si₃N₄/1Cr18Ni9Ti were prepared via a two-step process, namely gel casting and pressure casting. The phase composition, macro- and micro-structure of the composites were characterized. The erosion rate in flow slurry composed of water and quartz sand, as a function of impingement angle, flow velocity, sand content and erosion time was assessed in comparison with the plain 1Cr18Ni9Ti. Results show that Si₃N₄/1Cr18Ni9Ti composites exhibited a perfect co-continuous phase structure with a good combination between Si₃N₄ and 1Cr18Ni9Ti; the fluctuation of erosion rate as a function of impingement angle of this composites is smaller than that of 1Cr18Ni9Ti; the erosion rate of composites has an exponent relationship with flow velocity (E∝V ^0.67), while there is a linear relationship between the erosion rate and flow velocity for 1Cr18Ni9Ti; the erosion rate of this composites decreases gradually with the increasing erosion time and then stabilizes, while that of 1Cr18Ni9Ti is hardly changed; There is a linear relationship between the erosion rate and sand content in the slurry for the two materials. The composite with co-continuous structure of Si3N4/1Cr18Ni9Ti exhibits superior erosion resistance, in contrast with the plain 1Cr18Ni9Ti steel.

Key words: composite co-continuous phase slurry erosion 1Cr18Ni9Ti foam ceramic

Received: 26 April 2018

ZTFLH:

TB333

Fund: National Key Research and Development Program of China(2017YFB0310405)

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	Qi DU
	Yong GAO
	Zhiheng REN
	Xiaoming CAO
	Chao WANG
	Jinsong ZHANG

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https://www.cjmr.org/EN/10.11901/1005.3093.2018.296 OR https://www.cjmr.org/EN/Y2019/V33/I1/34

Fig.1 Sketch of the slurry erosion equipment (a) rotating disk equipment 1-motor, 2-container, 3-disc, 4-baffle, 5-specimen holder, 6-circulating water pipe, 7-cooling bath, 8-circulating pump, 9-holder, 10-jack (b) spacemen holder in (a) 1-nylon holder, 2- location bolt, 3-specimen, 4-disc, 5-junk ring, 6-specimen holder

Fig.2 XRD pattern of Si₃N₄ foam ceramic

Fig.3 Morphology of Si₃N₄ foam ceramic (a) macro image, (b) skeleton zone, (c) micro image

Fig.4 Morphology of Si₃N₄/1Cr18Ni9Ti co-continuous composites (a) macro image, (b) ceramic skeleton zone, (c) BSD of interface zone

Table 1 Main element compositions in different micro-areas in Fig.3c (%, mass fraction)

Fig.5 Relationship between the erosion rate and impingement angle

Fig.6 Relationship between the erosion rate and flow velocity

Fig.7 SEM and 3D surface images of 1Cr18Ni9Ti and Composites after erosion (a) SEM images of 1Cr18Ni9Ti, (b) SEM images of composites, (c) 3D surface images of 1Cr18Ni9Ti, (d) 3D surface images of composites

Fig.8 Relationship between the erosion rate and sand content

Fig.9 Comparison of slurry erosion resistance between 1Cr18Ni9Ti, Si₃N₄/1Cr18Ni9Ti co-continuous composites and Si₃N₄ ceramic

Fig.10 Height difference of composite before and after erosion (a) Si₃N₄ area, (b) 1Cr18Ni9Ti area

Fig.11 Erosion mechanism of Si₃N₄/1Cr18Ni9Ti co-continuous composites (a) 8 h, (b) 16 h, (c) 24 h, (d) 32 h

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