Preparation and Thermal Stability of Large-sized TiAl/Ti3Al Micro-laminated Thin Sheets

doi:10.11901/1005.3093.2014.042

Chinese Journal of Materials Research

2014, Vol. 28

Issue (4): 314-320 DOI: 10.11901/1005.3093.2014.042

Current Issue | Archive | Adv Search

Preparation and Thermal Stability of Large-sized TiAl/Ti₃Al Micro-laminated Thin Sheets

Zaoyu SHEN,Guanghong HUANG,Limin HE(

),Rende MU,Zhendong CHANG

Beijing Institute of Aeronautical Materials, Beijing 100095

Cite this article:

Zaoyu SHEN,Guanghong HUANG,Limin HE,Rende MU,Zhendong CHANG. Preparation and Thermal Stability of Large-sized TiAl/Ti₃Al Micro-laminated Thin Sheets. Chinese Journal of Materials Research, 2014, 28(4): 314-320.

Download:

HTML

PDF(3957KB)
Export: BibTeX | EndNote (RIS)

Abstract

Large-sized TiAl/Ti₃Al micro-laminated composite thin sheet with thickness of 0.1-10 mm was prepared by high-powerful electron beam physical vapor deposition technology in laboratory. The composition and microstructure of TiAl/Ti₃Al were chacterized by XRD and SEM. The results indicated that the prepared material with visible lamellar structure was alternately composed of α₂-Ti₃Al and γ-TiAl phase and the mean grain size of TiAl was about 1-2 µm. The degradation process was also investigated by high temperature annealing at various temperatures for 3 h.

Key words: composite materials EB-PVD microlaminate microstructure thermal stability

Received: 17 January 2014

	Service

	E-mail this article
	Add to citation manager
	E-mail Alert
	RSS
	（）
	Articles by authors
	Zaoyu SHEN
	Guanghong HUANG
	Limin HE
	Rende MU
	Zhendong CHANG

URL:

https://www.cjmr.org/EN/10.11901/1005.3093.2014.042 OR https://www.cjmr.org/EN/Y2014/V28/I4/314

Fig.1 XRD spectra of (a) TiAl and (b) Ti₃Al single layer sample

Fig.2 XRD spectra of the TiAl/Ti₃Al micolaminated composites

Fig.3 Micrographs of surface and cross-section of TiAl/Ti₃Al microlaminated composites by SEM. (a) sample surface, (b) sample cross-section

Fig.4 EDS analysis of Ti₃Al/TiAl microlaminated sheet

Fig.5 XRD of TiAl/Ti₃Al microlaminates get from different annealing temperature for 3 h

Fig.6 Cross-sectional microstructure of a TiAl/Ti₃Al microlaminate annealed at different temperature for 3 h under vacuum.(a)untreated, (b) 450℃, (c) 575℃ , (d) 700℃, (e) 825℃, (f) 950℃

Fig.7 Schematic diagram of TiAl/Ti₃Al microlaminates in cross section

1	J. T. Dorsey, C. C. Poteet, R. R. Chen,Metallic thermal protection system technology development: concepts, requirements and assessment overview, American Institute of Aeronautics and Astronautics, 0502, 1(2002)
2	CAO Yi,CHENG Haifeng, XIAO Jiayu, LI Yongqing, An introduction to American metallic TPS research work, Aerospace Materials Technology, 33(3), 9(2003)
2	(曹义, 程海峰, 肖加余, 李永清, 美国金属热防护系统研究进展, 宇航材料工艺, 33(3), 9(2003))
3	MA Peiyan,FU Zhengyi, The latest research on the microlaminated structural materials, Journal of Materials Science and Engineering, 20(4), 589(2002)
3	(马培燕, 傅正义, 微叠层结构材料的研究现状, 材料科学与工程, 20(4), 589(2002))
4	J. Heathcote, G. R. Odette, G. E. Lucas, R.G. Rowe, D. W. Skelly,On the micromechanics of low temperature strength and toughness of intermetallic/metallic microlaminate composites, Acta Materialia, 44(11), 4289(1996)
5	B. Ferrari, A. J. Sanchez-Herencia, R. Moreno,Aqueous electrophoretic deposition of Al2O3/ZrO2 layered ceramics, Materials Letters, 35(5-6), 370(1998)
6	G. S. Was, T. Foecke,Deformation and fracture in microlaminates, Thin Solid Films, 286(1-2), 1(1996)
7	J. Lapin,Creep behaviour of a cast TiAl-based alloy for industrial applications, Intermetallics, 14(2), 115(2006)
8	ZHANG Deming,CHEN Guiqing, HAN Jiecai, YAO Zhenzhong, Research on gamma TiAl-based alloy sheet fabricated by EB-PVD, Journal of Aeronautical Materials, 26(4), 35(2006)
8	(章德铭, 陈贵清, 韩杰才, 姚振中, EB-PVD制备γ-TiAl基合金薄板的研究, 航空材料学报, 26(4), 35(2006))
9	H. C. Cao, J. P. A. Lofvander, A. G. Evans, R. G. Rowe, D. W. Skelly,Mechanical properties of an in situ synthesized Nb/Nb3Al layered composite, Materials Science and Engineering: A, 185(1-2), 87(1994)
10	C. M. Word-Close, F. H. Froes,Developments in the synthesis of lightweight metals, JOM, 46(1), 28(1994)
11	Y. W. Kim,Intermetallic alloys based on gamma titanium aluminide, JOM, 41(7), 24(1989)
12	YUE Yunlong,WU Haitao, WANG Zhijie, ZHANG Lianmeng, Development of studies of TiAl intermetallics, Journal of University of Jinan (Science and Technology), 18(1), 31(2004)
12	(岳云龙, 吴海涛, 王志杰, 张联盟, TiAl金属间化合物的研究进展, 济南大学学报(自然科学版), 18(1), 31(2004))
13	P. A. Matage,Deformation of crack-bridging ductile reinforcements in toughened brittle materials, Acta Metallurgica, 37(12), 3349(1989)
14	L. Ma, Y. Sun, X. D. He,Preparation and performance of large-sized Ti/Ti-Al microlaminated composite, Rare Metal Materials and Engineering, 37(2), 325(2008)
15	MU Rende,HE Shimei, HE Limin, XU Zhenhua, EB-PVD thermal barrier coatings with microlaminated structure, Journal of Aeronautical Materials, 29(3), 55(2009)
15	(牟仁德, 贺世美, 何利民, 许振华, 微叠层结构EB-PVD热障涂层, 航空材料学报, 29(3), 55(2009))
16	R. G. Rowe, D. W. Skelly, M. Larsen,Microlaminated high temperature intermetallic composites, Scripta Metallurgica et Materialia, 31(11), 1487(1994)
17	G. R. Odette, B. L. Chao, J. W. Sheckherd,Ductile phase toughening mechanisms in a TiA-TiNb laminate composite, Acta Metallurgica et Materialia, 40(9), 2381(1992)
18	K. H. Ludtke, G. E. Lucas, C. G. Levi,Morphological stability of copper-silver multilayer thin films at elevated temperature, Metallurgical and Materials Transactions A, 34(5), 1043(2003)
19	M. Hillert,On the theory of normal and abnormal grain growth, Acta Metallurgica, 13(3), 227(1965)

[1]	PAN Xinyuan, JIANG Jin, REN Yunfei, LIU Li, LI Jinghui, ZHANG Mingya. Microstructure and Property of Ti / Steel Composite Pipe Prepared by Hot Extrusion[J]. 材料研究学报, 2023, 37(9): 713-720.
[2]	MAO Jianjun, FU Tong, PAN Hucheng, TENG Changqing, ZHANG Wei, XIE Dongsheng, WU Lu. Kr Ions Irradiation Damage Behavior of AlNbMoZrB Refractory High-entropy Alloy[J]. 材料研究学报, 2023, 37(9): 641-648.
[3]	ZHAO Zhengxiang, LIAO Luhai, XU Fanghong, ZHANG Wei, LI Jingyuan. Hot Deformation Behavior and Microstructue Evolution of Super Austenitic Stainless Steel 24Cr-22Ni-7Mo-0.4N[J]. 材料研究学报, 2023, 37(9): 655-667.
[4]	XING Dingqin, TU Jian, LUO Sen, ZHOU Zhiming. Effect of Different C Contents on Microstructure and Properties of VCoNi Medium-entropy Alloys[J]. 材料研究学报, 2023, 37(9): 685-696.
[5]	OUYANG Kangxin, ZHOU Da, YANG Yufan, ZHANG Lei. Microstructure and Tensile Properties of Mg-Y-Er-Ni Alloy with Long Period Stacking Ordered Phases[J]. 材料研究学报, 2023, 37(9): 697-705.
[6]	XIONG Shiqi, LIU Enze, TAN Zheng, NING Likui, TONG Jian, ZHENG Zhi, LI Haiying. Effect of Solution Heat Treatment on Microstructure of DZ125L Superalloy with Low Segregation[J]. 材料研究学报, 2023, 37(8): 603-613.
[7]	SHI Chang, DU Yuhang, LAI Liming, XIAO Siming, GUO Ning, GUO Shengfeng. Mechanical Properties and Oxidation Resistance of a Refractory Medium-entropy Alloy CrTaTi[J]. 材料研究学报, 2023, 37(6): 443-452.
[8]	LEI Zhiguo, WEN Shengping, HUANG Hui, ZHANG Erqing, XIONG Xiangyuan, NIE Zuoren. Influence of Rolling Deformation on Microstructure and Mechanical Properties of Al-2Mg-0.8Cu(-Si) Alloy[J]. 材料研究学报, 2023, 37(6): 463-471.
[9]	XIA Bo, WANG Bin, ZHANG Peng, LI Xiaowu, ZHANG Zhefeng. Effect of Tempering Temperature on Microstructure and Impact Properties of Two High-strength Leaf Spring Steels[J]. 材料研究学报, 2023, 37(5): 341-352.
[10]	JIANG Shuimiao, MING Kaisheng, ZHENG Shijian. A Review on Grain Boundary Segregation, Interfacial Phase and Mechanical Property Adjusting-controlling for Nanocrystalline Materials[J]. 材料研究学报, 2023, 37(5): 321-331.
[11]	ZHANG Shuaijie, WU Qian, CHEN Zhitang, ZHENG Binsong, ZHANG Lei, XU Pian. Effect of Mn on Microstructure and Properties of Mg-Y-Cu Alloy[J]. 材料研究学报, 2023, 37(5): 362-370.
[12]	ZHANG Ruixue, MA Yingjie, JIA Yandi, HUANG Sensen, LEI Jiafeng, QIU Jianke, WANG Ping, YANG Rui. Microstructure Evolution and Element Partitioning Behavior during Heat-treatment in Metastable β Titanium Alloy[J]. 材料研究学报, 2023, 37(3): 161-167.
[13]	LIN Shifeng, XU Dongan, ZHUANG Yanxin, ZHANG Haifeng, ZHU Zhengwang. Preparation and Mechanical Properties of TiZr-based Bulk Metallic Glass/TC21 Titanium Alloy Dual-layered Composites[J]. 材料研究学报, 2023, 37(3): 193-202.
[14]	DONG Yu'ang, YANG Huajie, BEN Dandan, MA Yunrui, ZHOU Xianghai, WANG Bin, ZHANG Peng, ZHANG Zhefeng. Excellent Cryogenic Tensile Properties of Ultra-fine Grained 316L Stainless Steel after Electropulsing Treatment in Liquid Nitrogen[J]. 材料研究学报, 2023, 37(3): 168-174.
[15]	ZHAO Yunmei, ZHAO Hongze, WU Jie, TIAN Xiaosheng, XU Lei. Effect of Heat Treatment on Microstructure and Properties of TIG Welded Joints of Powder Metallurgy Inconel 718 Alloy[J]. 材料研究学报, 2023, 37(3): 184-192.

No Suggested Reading articles found!

Viewed

Full text

Abstract

Cited

Shared

Discussed