Chinese Journal of Materials Research
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ISSN 1005-3093
CN 21-1328/TG
Started in 1987
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Current Issue
, Volume 12 Issue 3
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DYNAMIC RHEOLOGICAL BEHMIOR AND PHASE-SEMRATION OF MULTICOMPONENT/MULTIPHASE POLYMERS
ZHENG Qiang; ZHAO Tiejun(Department of Polymer Science and Engineering; Zhejiang University; Hangzhou 310027)
Chinese Journal of Materials Research, 1998,
12
(3): 225-232.
Abstract
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(652KB) (
1378
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This paper briefly reviewed the dynamic rheological behavior of multiphase / multicomponent polymers. Breakdown of the time-temperature superposition principle in the long time range (terminal range) for those polymers Was discussed. The importance of usi
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THE PROGRESS OF SiC SINGLE CRYSTAL GROWTH AND ITS DEVICES
WANG Yinshu; LI Jinmin; LIN Lanying (Institute of Semiconductors; The Chincse Academy of Sciences; Beijing 100083)
Chinese Journal of Materials Research, 1998,
12
(3): 233-238.
Abstract
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(645KB) (
907
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SiC is a material with large band gap, high thermal conductivity, high electron saturation velocity, high breakdown voltage and low dielectric constant. Its promising properties make it a attractive material for high-frequency, high-power, high-temperatur
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FACTORS OF AFFECTING SnO_2 FILMS PREPARED BY SOL-GEL METHOD AND THEIR CHARACTERISTICS
ZHANG Jiancheng; ZHOU Yue; SHEN Jiaqi (Dep.of Inorg.Mater.; Shanghai University; Shanghai 201800)
Chinese Journal of Materials Research, 1998,
12
(3): 239-244.
Abstract
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(1275KB) (
900
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Sn(OC2H5)4 can be selected as one of the precursors that are used to prepare SnO2films. This paper has reported how to control the hydrozed conditions of Sn(OC2H5)4, pH value (53) and viscosity of the hydrolyzed products in order to form sol solution and
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THREE-DIMENSIONAL AND CROSS-SECTIONAL CHARACTERISTICS OF NORMAL GRAIN GROWTH BASED ON COMPUTER SIMULATION
SONG Xiaoyan; LIU Guoquan (School of Materials Science Engineering; University of Science Technology Beijing;Beijing 100083; Hebei University of Technology)
Chinese Journal of Materials Research, 1998,
12
(3): 245-250.
Abstract
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(607KB) (
815
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An appropriate Monte Carlo method was developed to simulate the three-dimensional normal grain growth more completely comparative investigation on the three-dimensional characteristics and the cross-sectional expressions of normal grain growth indicated t
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ON OPTIMIZATION OF LASER SURFACE MELTING TECHNOLOGY FOR 1Cr18Ni9Ti STEEL BASED UPON ARTIFICIAL NEURAL NETWORK-GENETIC ALGORITHM
PAN Qingyue; SONG Renguo; ZHANG Qizhi; HUANG Weidong; ZHOU Yaohe ( State Key Lab of Solidification Processing; Northwestern Polytechnical University;Xi'an 710072 Beijing Institute of Mechanical Industry)
Chinese Journal of Materials Research, 1998,
12
(3): 251-256.
Abstract
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(423KB) (
878
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Laser su rface remelting was conducted to improve the corrosion resistance of 1Cr18Ni9Ti austenitic stainless steeI. Experimental relationship betWeen laser treatment pararneters and corrosion resistance was investigated. Particularly, an artificial neura
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DYNAMIC MECHANICAL BEHMIOR AND STRUCTURE STABILITY OF PMMA/α-MSAN BLENDS
ZHENG Qiang (Department of Polymer Science and Engineering; Zhejiang University; Hangzhou 310027)ARAKI Osamu; MASUDA Toshiro(Department of Material Chemistrp; Kyoto University; Japan)
Chinese Journal of Materials Research, 1998,
12
(3): 257-261.
Abstract
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(493KB) (
976
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Blends of poly (methyl methacrylate) (PMMA) and poly (α-methylstyrene-co acrylonitrile) (α-MSAN). exhibiting an LCST behavior, were prepared by solution casting using methyl ethyl ketone (MEK) as solvent. The dynamic mechanical behavior of the single-phas
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FAST CALCULATION OF THERMAL ACTION OF ACTUAL BEAM DURING THE LASER HEAT TREATMENT
LI Junchang; LI Xingyi;CHEN Qinghua;FAN Zebin;CHEN Jinbo (Kunming University of Science and Technology; Kunming 650093)
Chinese Journal of Materials Research, 1998,
12
(3): 262-266.
Abstract
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(1370KB) (
818
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This paper describes concisely the fast calculation method and the experimental test of the temperature field of an arbitrarily given beam during the laser infusible heat treatment, and discusses theoreticaIIy necessity for detecting laser power density.
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MICROSTRUCTURAL EVOLUTION IN MECHANICAL ALLOYED Mo-67%Si ELEMENTAL POWDERS MIXTURE
MA Qin; YU Ning; KANG Mokuang; YANG Yanqing(College of Materials Science and Engineering; Northwestern Polytechnical University;Xi'an 710072 Department of Materials Engineering; Gansu University of Technology;Lanzhou 730050)
Chinese Journal of Materials Research, 1998,
12
(3): 267-271.
Abstract
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(462KB) (
870
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The microstructural evolution of mechanical alloyed Mo-67%Si powders using the planetary ball mill has been studied by X ray diffractometer (XRD) and differential thermal analyzer (DTA). The result shows that the hexagonal (h) MoSi2 and tetragonal (t) MoS
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PHASE MORPHOLOGY CONTROL OF POLYSULFONE-MODIFIED EPOXY RESIN
SUN Jianing;XIE Xuming; HUANG Pengcheng (Tsinghua University; Beijing 100084) (Beijing University of Aeronautics and Astronautics)
Chinese Journal of Materials Research, 1998,
12
(3): 272-276.
Abstract
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(2768KB) (
1012
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Phase separation during the curing reaction in a blend of diglycidyI ether of bisphenol A (E51, E39, epoxy). polysulfone (PSF) and diamindiphenylsulfone (DDS, curing agent) was studied.ln the first stage, the mixture was a single-phase system. Phase contr
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MICROSTRUCTURE OF BN/SIALON MULTIPHASE CERAMICS AND UNCERTAINTY OF Z FOR SIALON GRAINS
SUI Wanmei(Colloege of Building Engineering ;Zhengzhou University;Zhengzhou 450052)HUANG Yong(Tsinghua University)
Chinese Journal of Materials Research, 1998,
12
(3): 277-281.
Abstract
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(2267KB) (
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BN(P)/Sialon multiphase ceramics were developed by hot-pressing sintering processing to abtain a composite with excellent thermal shock resistance and high reliability without obvious anisotropy of properties. Microstructure and phase intedece features of
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THE TENSILE STRENGTH AND FRACTURE MODE OF δ-ALUMINA SHORT FIBRE REINFORCED ALUMINIUM ALLOYS
ZHANG Jini;YANG Chuan; LIU Shikai; ZHANG Xiyan; KANG Guozheng (Materials Department; Southwest Jiaotong University; Chengdu 610031)
Chinese Journal of Materials Research, 1998,
12
(3): 282-286.
Abstract
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(1873KB) (
901
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The metal matrix composites based on a series of aluminium alloys and " Saffil" short fibre preforms were manufactured with the squeeze casting technique. The volume fraction of fibres in preforms was in the range from 8% to 20%. optical microscopy analys
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DETERMINATION OF SUPERFICIAL STRESS-STRAIN RELATIONSHIP WITH X-RAY DIFFRACTION TECHNIQUE
LI Jiabao (State Key Labomtory for Fatigue and focture of Materials; Institute of Metal Researeh;The Chinese Academy of Sciences; Shenyang 110015)
Chinese Journal of Materials Research, 1998,
12
(3): 287-290.
Abstract
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(356KB) (
1124
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Based on the incremental theory of plasticity and Mises criterion for yielding, a method for determining-the stress-strain relationship aed yield strength of a metallic material sudece with Xray difFraction technique has been established in this article.
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PREPARATION AND MICROSTRUCTURE OF POLYMER UNIFORM DISPERSIONS OF NANO-TiO_2/METHYLMETHACRYLATE
ZHANG Ye; ZHOU Guien; LI Lei; ZHANG Yuheng (Centre of Stuctural Analysis; University of Science and Technology of China;Hoti 230026)
Chinese Journal of Materials Research, 1998,
12
(3): 291-294.
Abstract
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(1145KB) (
1027
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A stable nano-Tio2 colloidal solution was prepared by using oleic acid with unsaturated double bonds and methylmethacrylate(MMA) as a suffoctant and an acetic solvent, respectivelythis dispersion of oleic acid coated nanoparticles of TiO2 within the polym
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THE WETTABILITY AND INTERFACE BONDING OF Co-Ti, Ti-Zr-Cu HIGH TEMPERATURE FILLERS ON Si_3N_4 CERAMIC
LU Shanping; DONG Xiuzhong; WU Qing; GUO Yi (Institute of Metal Researeh; The Chinese Academy of Sciences; Shenyang 110015)
Chinese Journal of Materials Research, 1998,
12
(3): 295-298.
Abstract
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(1782KB) (
1007
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In this paper, the wettability experiments of Co-Ti, Ti-Zr-Cu high temperature fillers on Si3N4 ceramic were carried out. The interface between brazing alloys and ceramic was analysed by X-Ray diffraction. The brazing alloy does not wet the Si3N4 ceramic
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DEPENDENCE OF STRUCTURE OF BURIED SiC LMERS ON C~+ IMPLANTATION DOSE
YAN Hui; CHEN Guanghua (Dep. of Applied Physics; Beijing Polytechnic University; Beijing 100022)
Chinese Journal of Materials Research, 1998,
12
(3): 299-302.
Abstract
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(294KB) (
780
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Buried SiC layers of different implantation doses were formed by using a metal vapor vacuum arc (MEVVA) ion source, with C+ ions implanted into Si substrates. In the present study the beam energy was 50keV and the ion dose was varied from 3.0×1017cm-2 to
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EFFECT OF TiO_2 AND ZrO_2 ON THE CRYSTALLIZATION OF B_2O_3-MgO-SiO_2 SLAG
ZHANG Peixin; SUI Zhitong; ZHAO Jianhua ( Depadrient of Chemical Engineering; Guangxi University; Nanning 530004; Northeastern University)
Chinese Journal of Materials Research, 1998,
12
(3): 303-306.
Abstract
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(916KB) (
885
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The crystallization behaviors of the boron component bearing B2O3-MgO-SiO2 slag with TiO2 and ZrO2 as nucleation agents ulere investigated by Xray diffraction (XRD), differential thermal analysis (DTA), scanning electron microscopy (SEM) and infrared ray(
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MICROYIELD DEFORMATION CHARACTERISTIC OF PARTICLE WITH SUBMICRON SCALE REINFORCED 6061 Al MATRIX COMPOSITE
WU Gaohui; MA Senlin; ZHAO Yongchun; YANG Dezhuang (School of Materials & Engineering; Harbin Institute of Technology; Harbin 150001)
Chinese Journal of Materials Research, 1998,
12
(3): 307-310.
Abstract
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(1034KB) (
929
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In the present paper, microyield characteristic of a Al2O3p /6061 composite was investigated and its microstructure was observed by TEM and HREM. It indicated that the Al2O3p/6061 composite had high microyield stress and good microstructure stability comp
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AMORPHIZATION IN THE IMMISCIBLE SYSTEMS BY SOLID STATE REACTION
PAN Feng; LIU Baixin (Department of Materials Science and Engineering; Tsinghua University; Beijing 100084)
Chinese Journal of Materials Research, 1998,
12
(3): 311-313.
Abstract
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(999KB) (
1600
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The possibility of amorphous phase formation by solid state reaction (SSR) in the immiscible Cu-Ta and Cu-Nb nano-multilayers was studied by means of selected area electron diffraction and X-ray diffraction. The experimental results revealed that, when th
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THE NEGATIVE ELECTROPLASTICITY IN THE Zn-5Al ALLOY
LI Shichun (Department of Machinery; University of Petroleum; Dongying 257062)
Chinese Journal of Materials Research, 1998,
12
(3): 314-316.
Abstract
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(1476KB) (
873
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The Zn-5Al eutectic alloy is superplastically deformed in an electric field of 0.3MV.m-1,and displays the negative electroplasticity The effect of electric field on the strain rate is relative to the effect of the surface charges on the voids on the sudec
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ON IN SITU PREMRATION OF (Ti, Zr)C SOLID-SOLUTION POWDER BY WET-CHEMICAL METHOD
KONG Xiangyang; LI Jianbao; HUANG Yong (Dept.of Mater.Sci.& Eng; Tsinghua University; Beijing 100084)
Chinese Journal of Materials Research, 1998,
12
(3): 317-319.
Abstract
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(1001KB) (
885
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This paper described a kind of technology on in situ preparation of (Ti, Zr)C solid-solution powder with homogenous phase by wet-chemical method. The analysis instrument for particle size and SEM showed the size distribution and morphology of as received
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AMORPHIZATION OF Cu-Ti-Fe-Nb SYSTEMS BY MECHANICAL ALLOYING
LOU Taiping; LI Fushan HONG Jun; CHEN WanjinDING Bingzhe; HU Zhuangqi( National Key Lab for RSA; Institute of Metal Researeh; The Chinese Academy of Sciences;Shenyang 110015 Siping Normal College)
Chinese Journal of Materials Research, 1998,
12
(3): 320-322.
Abstract
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(732KB) (
883
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Mechanical alloying (MA) of elemental powder mixtrues of 38.4Cu/25.6Ti/18Fe/18Nb and amorphous Cu60Ti40 - Fe50Nb50 powder mixtures of (Cu60Ti40)64(Fe50Nb50)36 are pedermed using a high energy ball mill. In the MA processing, the systems for the elemental
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NANO-CRYSTALLINE DIAMOND PREMRATION BY INDUCING REACTION AT LIQUID-SOLID INTERFACE
WANG Jinbin; LIU Qidriang;YANG Guowi;HU Guobin;YOU Jianqiang (Institute of Modern Physics; Xangtan University; Xangtan 411105)
Chinese Journal of Materials Research, 1998,
12
(3): 323-325.
Abstract
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(733KB) (
896
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A novel pulsed laser ablation technique has been used for the synthesis of nano crystalline diamond from a solid graphite target in the reactive liquid. Electron diffraction and high resolution electron micrograph indicate that particles are of hexagonal
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SOLID-PHASE SYNTHESIS GRAPHITE FLUORIDE
XIA Jintong; XU Shengming; ZHENG Maoping; ZHOU Shengmai; CHEN Zongzhang (Institute of Chemical Engineering; Hunan University; Changsha 410082)
Chinese Journal of Materials Research, 1998,
12
(3): 326-328.
Abstract
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(196KB) (
883
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Under nitrogen atmospheric pressure 0.5MPa. the graphite fluoride was prepared through the synthesis reaction between the graphite powder (grain <40μm, carbon content>99.7%)and the polytetrafluoroethylene at 450℃. The real density of the graphite fluoride
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THE MAIN INFLUENTIAL FACTORS ON SEEBECK EFFECT OF CFRC
SUN Mingqing; LI Zhuoqiu; MAO Qizhao; SHEN Darong (Dep. of Engineering Mechanics; Wuhan University of Technology; Wuhan 430070)
Chinese Journal of Materials Research, 1998,
12
(3): 329-331.
Abstract
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(183KB) (
920
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The influence of the content of carbon fiber, cement matrix and curing period on Seebeck effect of carbon fiber reinforced cement (CFRC) is discussed in this paper. The results show that the thermoelectric power (TEP) reaches its maximum when carbon fiber
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ULTRASONIC CHARACTERISTIC OF THE Al_2O_(3f)/Al COMPOSITES
ZHU Changfei; LUO Xisheng (Laboratory of Internel Inction & Defect in Solids; University of Science and Technology of China; Hefei 230026) LI Xiuchen; WANG Qing (Shanghai Jiaotong University)
Chinese Journal of Materials Research, 1998,
12
(3): 332-334.
Abstract
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(257KB) (
880
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The velocities of Iongitudinal and shear waves and the mean densities of three kinds of short fibre alumina (Al2O3) reinforced aluminum composites (Vf=5.4, 9.1 and 13.6%) were measured, from which the elastic moduli and the shear moduli were computed. The
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GROWTH AND MICROSTRUCTURE OF SILICON CARBIDE NANORODS
HAN Weiqiang; FAN Shoushan;LI Qunqing;GU Binglin (Dept. of Physics; Tsinghua University; Beijing 100084)
Chinese Journal of Materials Research, 1998,
12
(3): 335-336.
Abstract
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(892KB) (
851
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A method of two step reactions for Synthesis SiC nanorods has been reported. First,Sio vapour was generated via the silicon reduction of silica. Second, the generated SiO vapour reacted with carbon nanotubes, which resulted in the growth of the single cry
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