Properties of TiC Reinforced Ti-Composites Synthesized in Situ by Microwave Sintering

doi:10.11901/1005.3093.2020.166

Chinese Journal of Materials Research

2021, Vol. 35

Issue (4): 277-283 DOI: 10.11901/1005.3093.2020.166

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Properties of TiC Reinforced Ti-Composites Synthesized in Situ by Microwave Sintering

HU Manying¹, OUYANG Delai¹(

), CUI Xia¹, DU Haiming², XU Yong¹

^1.School of Materials Science and Engineering, Nanchang Hangkong University, Jiangxi 330063, China
^2.Jiangxi Normal University, Jiangxi 330022, China

Cite this article:

HU Manying, OUYANG Delai, CUI Xia, DU Haiming, XU Yong. Properties of TiC Reinforced Ti-Composites Synthesized in Situ by Microwave Sintering. Chinese Journal of Materials Research, 2021, 35(4): 277-283.

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Abstract

Novel TiC reinforced Ti-based composites were synthesized via in situ microwave sintering with nanotubes (MWCNTs) and pure Ti as raw materials. The properties of the composites were investigated, and the formation mechanism of TiC reinforced phase of the composites was discussed. The results show that TiC reinforced phase could be generated in-situ in the Ti-matrix during microwave sintering. When the addition amount of MWCNTs <1% (in mass fraction), the formed TiC was granular-like and distributed uniformly in the dense Ti matrix of fine grains. When the addition amount of MWCNTs >1.5%, the formed TiC turns to be of dendritic morphology, while the Ti matrix is coarsened and the composite becomes porous. Sequentially, the wear mechanism of the composites will change from adhesive wear to abrasive wear due to the addition of MWCNTs. With the increasing addition amount of MWCNTs the microhardness of the composite increases firstly and then decreases. When the addition amount of MWCNTs is 1%, the acquired composite presents a higher microhardness of about 527HV and better wear resistance with the friction coefficient of about 0.35, which are 1.2 times more and 0.4 less than the corresponding terms of the pure Ti respectively.

Key words: composites microwave sintering TiC in situ synthesis TiC reinforced titanium composites

Received: 18 May 2020

ZTFLH:

TG146

Fund: National Natural Science Foundation of China(51761029)

About author: OUYANG Delai, Tel: (0791)83863039, E-mail: ouyangdelai@163.com

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	Manying HU
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	Xia CUI
	Haiming DU
	Yong XU

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https://www.cjmr.org/EN/10.11901/1005.3093.2020.166 OR https://www.cjmr.org/EN/Y2021/V35/I4/277

Fig.1 Raw materials for preparing titanium matrix composites (a) purification of multi-walled carbon nanotubes, (b) flake pure titanium powder

Fig.2 Experimental procedure

Fig.3 Effect of additive amount of MWCNTs on microstructure of TiC reinforced titanium composites (a) 0.5%MWCNTs, (b) 1%MWCNTs, (c) 1.5%MWCNTs, (d) 2%MWCNTs

Fig.4 XRD spectrum of TiC reinforced titanium composites with different MWCNTs additive amount

Fig.5 Two types morphology of TiC phase in TiC reinforced titanium composites (a) granular, (b) dendritic, (c) EDS analysis of mark A in Fig.5 (a)

Fig.6 Effect of additive amount of MWCNTs on the relative density of TiC reinforced titanium composites

Fig.7 Effect of additive amount of MWCNTs on the hardness of TiC reinforced titanium composites

Fig.8 Friction factor-time curve of composites with different MWCNTs additive amount

Fig.9 Average friction factor and wear volume of composites with different MWCNTs additive amount

Fig.10 Wear microstructure of pure titanium matrix and composites with different MWCNTs additive amount (a) pure titanium, (b) 1% MWCNTs, (c) EDS analysis of mark A in Fig.10 (b)

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