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材料研究学报  2026, Vol. 40 Issue (8): 561-571    DOI: 10.11901/1005.3093.2025.315
  钛合金专题 本期目录 | 过刊浏览 |
拉拔变形量对超高强钛合金棒材强塑性的影响
胡明, 王啟睿, 邱建科(), 雷晓飞, 张金虎, 董利民, 杨锐
中国科学院金属研究所 沈阳 110016
Effect of Drawing Reduction on Strength-ductility of Ultra-high Strength Ti-alloy Bar
HU Ming, WANG Qirui, QIU Jianke(), LEI Xiaofei, ZHANG Jinhu, DONG Limin, YANG Rui
Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
引用本文:

胡明, 王啟睿, 邱建科, 雷晓飞, 张金虎, 董利民, 杨锐. 拉拔变形量对超高强钛合金棒材强塑性的影响[J]. 材料研究学报, 2026, 40(8): 561-571.
Ming HU, Qirui WANG, Jianke QIU, Xiaofei LEI, Jinhu ZHANG, Limin DONG, Rui YANG. Effect of Drawing Reduction on Strength-ductility of Ultra-high Strength Ti-alloy Bar[J]. Chinese Journal of Materials Research, 2026, 40(8): 561-571.

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摘要: 

对直径为16.4 mm的超高强TC10合金棒材进行不同变形量的拉拔后进行退火和固溶时效处理,使用FEI Inspect F50扫描电子显微镜、电子背散射衍射(EBSD)和HKL-Channel5软件表征其组织和性能,研究了拉拔变形量对其显微组织、织构和力学性能的影响。结果表明:随着拉拔变形量的提高合金中的α晶粒沿拉拔方向拉长并形成<101¯0>丝织构,晶粒细化和加工硬化使合金的强度提高但其塑性降低。退火后发生回复再结晶使合金中的<101¯0>织构先增强后减弱,合金的强度比拉拔态略降但是塑性提高。固溶时效使合金中析出细小的针状次生α相,使合金的强度进一步提高但是塑性降低。拉拔变形量为59.0%的固溶时效态合金的综合性能较高:抗拉强度为1402 MPa,延伸率为11.0%。研究结果为选择用TC10合金棒材制造紧固件的拉拔工艺参数提供了依据。

关键词 金属材料超高强钛合金显微组织织构力学性能    
Abstract

The effect of drawing deformation on the microstructure, texture and mechanical properties of ultra-high strength TC10 Ti-alloy bars were investigated. TC10 alloy bars with a diameter of 16.4 mm were warm-drawn to various reductions, followed by annealing and solution-aging treatments, after which microstructure and mechanical properties were characterized. The results indicate that with the increasing drawing deformation, α-grains elongate along the drawing direction and develop a strong <101¯0> fiber texture. Grain refinement plus work-hardening collectively raise strength but reduce plasticity of the Ti-alloy bar. After annealing, recovery and recrystallization occur, leading to an initial strengthening and subsequent weakening of the <101¯0> texture. The strength of the annealed alloy slightly decreases compared to the as-drawn state, while the ductility improves. Solution-aging treatment leads to the precipitation of fine, acicular secondary α-phases, further increasing the strength but reducing the plasticity of Ti-alloy. At a drawing deformation of 59%, the solution-aged alloy exhibits optimal comprehensive properties, achieving a tensile strength of 1402 MPa and an elongation of 11.0%. These findings provide a meaningful reference for determining the drawing process parameters of TC10 alloy bars used in fastener manufacturing.

Key wordsmetallic materials    ultra-high strength Ti-alloy    microstructure    texture    mechanical property
收稿日期: 2025-10-27     
ZTFLH:  TG146.2  
基金资助:国家重点研发计划(2022YFB3708300);中国科学院青年创新促进会项目(2022188)
通讯作者: 邱建科,研究员,jkqiu@imr.ac.cn,研究方向为钛合金
Corresponding author: QIU Jianke, Tel: (024)23971958, E-mail: jkqiu@imr.ac.cn
作者简介: 胡 明,男,1991年生,博士
Pass0123456791112
Reduction04.810.721.827.141.950.859.069.979.184.3
表1  TC10合金棒材拉拔道次变形量
图1  不同变形量拉拔态TC10合金试样的SEM照片
图2  不同变形量拉拔态TC10合金中α晶粒取向成像图
图3  不同变形量拉拔态TC10合金中α相的反极图
图4  不同变形量拉拔态TC10合金试样的力学性能
图5  不同拉拔变形量TC10合金退火后的SEM照片
图6  不同拉拔变形量TC10合金退火后α晶粒的取向成像
图7  不同拉拔变形量TC10合金退火后α相的反极图
图8  不同拉拔变形量TC10合金退火后的力学性能
图9  不同拉拔变形量TC10合金固溶时效后的SEM照片
图10  不同拉拔变形量TC10合金固溶时效后α晶粒的取向成像
图11  不同拉拔变形量TC10合金固溶时效后α相的反极图
图12  不同拉拔变形量TC10合金固溶时效后的力学性能
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