<strong>NiFe-LDH/Co, La-CeO<sub>2</sub></strong> 催化剂的制备及其性能

doi:10.11901/1005.3093.2026.110

材料研究学报

2026, Vol. 40

Issue (7): 507-518 DOI: 10.11901/1005.3093.2026.110

研究论文

本期目录 | 过刊浏览

NiFe-LDH/Co, La-CeO₂ 催化剂的制备及其性能

王俊¹, 刘雯¹(

), 籍伟花²(

), 苗洋²^,³(

), 王一杰⁴(

), 宗振昊¹, 马浩铭¹, 周玲玲⁵

^1.太原科技大学化学工程与技术学院太原 030024
^2.太原理工大学材料科学与工程学院太原 030024
^3.山西省煤基固废资源化利用创新技术中心太原 030021
^4.北京科技大学北京材料基因工程高精尖创新中心新金属材料国家重点实验室北京 100083
^5.中国科学院力学研究所非线性力学国家重点实验室北京 100190

Effect of Lattice-interface Synergy of NiFe-layered Double Hydroxide /Co, La-doped CeO₂ on Efficient Oxygen Evolution Reaction

WANG Jun¹, LIU Wen¹(

), JI Weihua²(

), MIAO Yang²^,³(

), WANG Yijie⁴(

), ZONG Zhenhao¹, MA Haoming¹, ZHOU Lingling⁵

^1.College of Chemical Engineering and Technology, Taiyuan University of Science and Technology, Taiyuan 030024, China
^2.College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
^3.Shanxi Innovation Technology Center for Coal-Based Solid Waste Resource Utilization, Taiyuan 030021, China
^4.Beijing Advanced Innovation Center for Materials Genome Engineering, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China
^5.State Key Laboratory of Nonlinear Mechanics, Institute of Mechanics, Chinese Academy of Sciences, Beijing 100190, China

引用本文:

王俊, 刘雯, 籍伟花, 苗洋, 王一杰, 宗振昊, 马浩铭, 周玲玲. NiFe-LDH/Co, La-CeO₂ 催化剂的制备及其性能[J]. 材料研究学报, 2026, 40(7): 507-518.
Jun WANG, Wen LIU, Weihua JI, Yang MIAO, Yijie WANG, Zhenhao ZONG, Haoming MA, Lingling ZHOU. Effect of Lattice-interface Synergy of NiFe-layered Double Hydroxide /Co, La-doped CeO₂ on Efficient Oxygen Evolution Reaction[J]. Chinese Journal of Materials Research, 2026, 40(7): 507-518.

全文: PDF(15891 KB) HTML

摘要:

用一锅水热法合成Co,La-CeO₂基底，引入了可控的晶格应变和丰富的氧空位(Ov)，使电子传导能力和结构稳定性显著提高。NiFe-LDH与Co, La-CeO₂之间形成的强界面耦合，提高了电荷传递效率和优化了含氧中间体的吸附行为。这种NiFe-LDH/Co, La-CeO₂/CF复合电极在1.0 mol/L KOH溶液中的OER催化性能优异，电流密度为50 mA·cm^-2所需过电位仅为230 mV，Tafel斜率则为74.65 mV·dec^-1，连续运行50 h其初始电流密度仍保持在97.14%。表明在电催化材料中晶格掺杂改性与界面的协同效应起了关键作用。

关键词 ：复合材料, 异质结, 晶格应变, 氧空位, 析氧反应, 铈基催化剂

Abstract：

A novel heterojunction electrocatalyst of NiFe-layered double hydroxide/Co, La doped CeO₂ was prepared by electrodepositing ultrathin NiFe-LDH nanosheets onto a Co, La co-doped CeO₂ (Co, La-CeO₂) support on copper foam (CF) according to the "lattice-interface synergistic regulation" strategy of our group. The support of Co, La co-doped CeO₂ on CF was first synthesized via a one-pot hydrothermal method, while the controllable lattice strain and abundant oxygen vacancies (Oᵥ) were introduced, which may significantly enhance the intrinsic electronic conductivity and structural stability of the support. Furthermore, the strong interfacial coupling between NiFe-LDH and Co, La co-doped CeO₂ may facilitate the charge transfer and optimize the adsorption of oxygen-containing intermediates. As a result, the NiFe-LDH/Co, La co-doped CeO₂/CF composite exhibits superior performance of oxygen evolution reaction in 1.0 mol/L KOH, requiring an overpotential of only 230 mV to reach 50 mA·cm^-2 with a Tafel slope of 74.65 mV·dec^-1. It also retains 97.14% of its initial current density after 50 h of continuous operation. This study highlights the importance of lattice doping and interfacial synergy, providing a generalizable design framework for high-efficiency non-noble metal electrocatalysts for oxygen evolution reaction.

Key words： composite heterojunction lattice strain oxygen vacancies oxygen evolution reaction cerium-based catalysts

收稿日期: 2026-01-26

ZTFLH:

O646.54

基金资助:国家自然科学基金(52472075);山西省青年科学基金(202403021212037)

通讯作者: 刘雯，教授，13700509372@163.com，研究方向为纳米碳材料的制备及微观界面结构;
籍伟花，讲师，jiweihua@tyut.edu.cn，研究方向为电催化析氧反应;
苗洋，教授，miaoyang198781@163.com，研究方向为无机非金属;
王一杰，博士，wangyijie_2016@126.com，研究方向为电化学模拟

Corresponding author: LIU Wen, Tel: 13700509372, E-mail: 13700509372@163.com;
JI Weihua, Tel: 18800185926, E-mail: jiweihua@tyut.edu.cn;
MIAO Yang, Tel: 18636918826, E-mail: miaoyang198781@163.com;
WANG Yijie, Tel: 18811398701, E-mail: wangyijie_2016@126.com

作者简介: 王俊，男，1999年生，硕士生

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https://www.cjmr.org/CN/10.11901/1005.3093.2026.110 或 https://www.cjmr.org/CN/Y2026/V40/I7/507

图1 NiFe-LDH/Co, La-CeO2/CF制备过程的示意图

图2 CeO2/CF和Co-CeO2/CF的SEM照片

图3 Co, La-CeO2/CF和NiFe-LDH/Co, La-CeO2/CF的SEM照片、NiFe-LDH/Co, La-CeO2/CF的EDS元素分布以及NiFe-LDH/Co, La-CeO2的XRD谱

图4 Co, La-CeO2和NiFe-LDH/Co, La-CeO2的TEM和HRTEM图像

图5 NiFe-LDH/Co, La-CeO2、Co, La-CeO2和CeO2的Raman光谱

图6 NiFe-LDH-Co, La-CeO2/CF的XPS全谱和NiFe-LDH/Co, La-CeO2/CF中C 1s的XPS谱

图7 NiFe-LDH/Co, La-CeO2/CF、Co, La-CeO2/CF和CeO2/CF的XPS谱

图8 催化剂的OER电化学测试

表1 NiFe-LDH/Co, La-CeO2/CF与已报道电催化剂的OER性能对比

表2 OER测试中各催化剂等效电路的电阻值

图9 NiFe-LDH与NiFe-LDH/Co, La-CeO2上OER四步反应的Gibbs自由能、NiFe-LDH与NiFe-LDH/Co, La-CeO2的总态密度和态密度

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