材料研究学报  1998, Vol. 12 Issue (3): 239-244

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影响Sol—gel法制SnO_2膜的因素及膜特性

张建成;周跃;沈嘉祺

上海大学;上海市;201800;上海大学;上海大学

FACTORS OF AFFECTING SnO_2 FILMS PREPARED BY SOL-GEL METHOD AND THEIR CHARACTERISTICS

ZHANG Jiancheng; ZHOU Yue; SHEN Jiaqi (Dep.of Inorg.Mater.; Shanghai University; Shanghai 201800)

张建成;周跃;沈嘉祺. 影响Sol—gel法制SnO_2膜的因素及膜特性[J]. 材料研究学报, 1998, 12(3): 239-244.
, , . FACTORS OF AFFECTING SnO_2 FILMS PREPARED BY SOL-GEL METHOD AND THEIR CHARACTERISTICS[J]. Chin J Mater Res, 1998, 12(3): 239-244.

摘要 参考文献 相关文章 Metrics 全文: PDF(1275 KB)   摘要: Sn(OC2H5)4是制SnO2膜的前驱体之一。本文报道控制形成溶胶的Sn(OC2H5)4水解条件,水解产物的pH值(≤3)及粘度等.研究了水解产物的热分解过程及膜的某些特性,包括得到较佳SnO2膜的合宜热处理温度和加温速率、若干掺杂剂、电子束辐照及村底加热温度对膜材的电学参数的影响,测定了涂膜后光纤的弯曲断裂强度与此类膜的气敏特性. 关键词 ： SnO_2膜,  溶胶凝胶方法,  锡醇盐,  气敏材料     Abstract：Sn(OC2H5)4 can be selected as one of the precursors that are used to prepare SnO2films. This paper has reported how to control the hydrozed conditions of Sn(OC2H5)4, pH value (53) and viscosity of the hydrolyzed products in order to form sol solution and Key words： SnO_2 films    sol-gel method    tin(Ⅳ) alkoxide    sensitive materials for gas 收稿日期: 1998-06-25      基金资助:上海市教委重点学科立项资助 服务 把本文推荐给朋友 加入引用管理器 E-mail Alert RSS 作者相关文章 张建成 周跃 沈嘉祺 44.8K 链接本文: https://www.cjmr.org/CN/      或      https://www.cjmr.org/CN/Y1998/V12/I3/239 1傅敏荣,钟仕科应用化学2,83(1985) 2 I.A.Qazi, P.Akhter, A.Mufti, J.Phys. 24, 81(1991) 3 H.H.Afiffy, R.S.Momtax, W.A.Badawy, J.Mater.Sci., Mater.Electron. 2, 40(1991) 4 V.Schmidt, H.Schicht, G.Goermar, Ger. Patent DD 288822(1991) 5 J.C.Zhang, J.Q.Shen, Y.Xia, In Proceedlng of Int. Conf on Electro. Components and Mater (Hangzhou,Int.Acad.publishers, 1992) p.366 6 Pope, EJA, J.D.Mackenzie, J.Non-cryst.Solids. 87, 185(1986) 7 Hirarro S, Kato K., J .Non -cryst.Solids. 100, 538(1986) 8 PDF 卡, edited by Joint Committee on Powder Diffraction Standards, JCPDS-21-1250 9李标荣. 电子元件与材料. 10, 1(1991) 10 T.Yasutaka, W.Yukisa, J.Electeochem.Soc., 137, 267(1990) 11 Gonzalez-Oliver CJR, Kato I, J.Non-cryst.Solids. 82, 400(1986) 12 康昌鹤, 唐省吾. 气湿敏感器件及其应用. (北京, 科技出版社, 1988) P.16,6413 J.C.Giuntini, W.Graniar, J.V.Zanchetta, A.Taha, J.Mater.Sci.Letters. 9, 1383(1990) No related articles found! Viewed Full text Abstract Cited   Shared      Discussed