Effect of Lattice-interface Synergy of NiFe-layered Double Hydroxide /Co, La-doped CeO2 on Efficient Oxygen Evolution Reaction

doi:10.11901/1005.3093.2026.110

Chinese Journal of Materials Research

2026, Vol. 40

Issue (7): 507-518 DOI: 10.11901/1005.3093.2026.110

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Effect of Lattice-interface Synergy of NiFe-layered Double Hydroxide /Co, La-doped CeO₂ on Efficient Oxygen Evolution Reaction

WANG Jun¹, LIU Wen¹(

), JI Weihua²(

), MIAO Yang²^,³(

), WANG Yijie⁴(

), ZONG Zhenhao¹, MA Haoming¹, ZHOU Lingling⁵

^1.College of Chemical Engineering and Technology, Taiyuan University of Science and Technology, Taiyuan 030024, China
^2.College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
^3.Shanxi Innovation Technology Center for Coal-Based Solid Waste Resource Utilization, Taiyuan 030021, China
^4.Beijing Advanced Innovation Center for Materials Genome Engineering, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China
^5.State Key Laboratory of Nonlinear Mechanics, Institute of Mechanics, Chinese Academy of Sciences, Beijing 100190, China

Cite this article:

WANG Jun, LIU Wen, JI Weihua, MIAO Yang, WANG Yijie, ZONG Zhenhao, MA Haoming, ZHOU Lingling. Effect of Lattice-interface Synergy of NiFe-layered Double Hydroxide /Co, La-doped CeO₂ on Efficient Oxygen Evolution Reaction. Chinese Journal of Materials Research, 2026, 40(7): 507-518.

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Abstract

A novel heterojunction electrocatalyst of NiFe-layered double hydroxide/Co, La doped CeO₂ was prepared by electrodepositing ultrathin NiFe-LDH nanosheets onto a Co, La co-doped CeO₂ (Co, La-CeO₂) support on copper foam (CF) according to the "lattice-interface synergistic regulation" strategy of our group. The support of Co, La co-doped CeO₂ on CF was first synthesized via a one-pot hydrothermal method, while the controllable lattice strain and abundant oxygen vacancies (Oᵥ) were introduced, which may significantly enhance the intrinsic electronic conductivity and structural stability of the support. Furthermore, the strong interfacial coupling between NiFe-LDH and Co, La co-doped CeO₂ may facilitate the charge transfer and optimize the adsorption of oxygen-containing intermediates. As a result, the NiFe-LDH/Co, La co-doped CeO₂/CF composite exhibits superior performance of oxygen evolution reaction in 1.0 mol/L KOH, requiring an overpotential of only 230 mV to reach 50 mA·cm^-2 with a Tafel slope of 74.65 mV·dec^-1. It also retains 97.14% of its initial current density after 50 h of continuous operation. This study highlights the importance of lattice doping and interfacial synergy, providing a generalizable design framework for high-efficiency non-noble metal electrocatalysts for oxygen evolution reaction.

Key words: composite heterojunction lattice strain oxygen vacancies oxygen evolution reaction cerium-based catalysts

Received: 26 January 2026

ZTFLH:

O646.54

Fund: National Natural Science Foundation of China(52472075);Natural Science Foundation for Young Scientists of Shanxi Province(202403021212037)

Corresponding Authors: LIU Wen, Tel: 13700509372, E-mail: 13700509372@163.com;
JI Weihua, Tel: 18800185926, E-mail: jiweihua@tyut.edu.cn;
MIAO Yang, Tel: 18636918826, E-mail: miaoyang198781@163.com;
WANG Yijie, Tel: 18811398701, E-mail: wangyijie_2016@126.com

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	WANG Jun
	LIU Wen
	JI Weihua
	MIAO Yang
	WANG Yijie
	ZONG Zhenhao
	MA Haoming
	ZHOU Lingling

URL:

https://www.cjmr.org/EN/10.11901/1005.3093.2026.110 OR https://www.cjmr.org/EN/Y2026/V40/I7/507

Fig.1 Schematic illustration of the preparation process for the NiFe-LDH/Co, La-CeO₂/CF composite

Fig.2 SEM images of the synthesized CeO₂/CF (a) and Co-CeO₂/CF (b)

Fig.3 SEM images of as-synthesized Co, La-CeO₂/CF (a-c), NiFe-LDH/ Co, La-CeO₂/CF (d-f), EDS elemental mapping of NiFe-LDH/Co, La-CeO₂/CF (g), XRD patterns of NiFe-LDH/Co, La-CeO₂ (h)

Fig.4 TEM (a, b, d, e) and HRTEM (c, f) images of Co, La-CeO₂ (a-c) and NiFe-LDH/Co, La-CeO₂ (d-f)

Fig.5 Raman spectra of NiFe-LDH/Co, La-CeO₂, Co,La-CeO₂ and CeO₂

Fig.6 XPS survey spectrum of NiFe-LDH-Co, La-CeO₂/CF (a) and XPS spectrum of C 1s in NiFe-LDH/Co, La-CeO₂/CF (b)

Fig.7 XPS of NiFe-LDH/Co, La-CeO₂/CF, Co, La-CeO₂/CF and CeO₂/CF (a) Ce 3d, (b) O 1s, (c) Co 2p, (d) La 3d, (e) Ni 2p, (f) Fe 2p

Fig.8 OER LSV curves of samples (a), overpotential histograms of various samples at 10 mA·cm^-2, 50 mA·cm^-2, and 100 mA·cm^-2 current densities (b), associated tafel plots (c), C_dl plots for the relevant (d), EIS Nyquist plots (e) and stability test of NiFe-LDH/Co, La-CeO₂/CF at 100 mA·cm^-2 (f)

Table 1 Comparison of OER performance of NiFe-LDH/Co, La-CeO₂/CF with reported electrocatalysts

Table 2 Resistance values of the equivalent circuits for various catalysts during OER tests

Fig.9 Gibbs free energy diagram for the four steps of OER (a) on NiFe-LDH and NiFe-LDH/Co, La-CeO₂, total density of states (b) and density of states (DOS) (c, d) for NiFe-LDH and NiFe-LDH/Co, La-CeO₂

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