Synthesis and Performances of Silver Vanadate For Battery of Implantable Medical Devices

doi:10.11901/1005.3093.2017.515

Chinese Journal of Materials Research

2018, Vol. 32

Issue (7): 555-560 DOI: 10.11901/1005.3093.2017.515

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Synthesis and Performances of Silver Vanadate For Battery of Implantable Medical Devices

Jin ZHANG(

), Ning WANG, Chong ZHAO, Jiaxing LI, Tianchi ZHANG

Xijing University, Xi'an 710123, China

Cite this article:

Jin ZHANG, Ning WANG, Chong ZHAO, Jiaxing LI, Tianchi ZHANG. Synthesis and Performances of Silver Vanadate For Battery of Implantable Medical Devices. Chinese Journal of Materials Research, 2018, 32(7): 555-560.

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Abstract

One-dimensional α-AgVO₃ nanostructures were synthesized at ambient temperature via in-situ reaction process using one-dimensional K₂V₆O_16·1.5H₂O as precursor template. Then one-dimensional β-AgVO₃ nanostructures were obtained through heat-treatment of the α-AgVO₃ nanostructures at 300℃ for 3 h. The as-prepared α-AgVO₃ and β-AgVO₃ nanostructures were characterized by means of X-ray diffraction (XRD), field emission scanning electron microscope (FE-SEM), transmission electron microscope (TEM), X-ray photoelectron spectroscopy (XPS). Results of the electrochemical tests show that the β-AgVO₃ nanostructures possess better rate capability and cycling performance, as well as smaller charge transfer and lithium ion transport resistance rather than that of the α-AgVO₃ nanostructures.

Key words: functional materials silver vanadium oxides 1D nanostructure in-situ synthesis electrochemistry

Received: 15 May 2017

ZTFLH:

TB34

Fund: Supported by Science Foundation of Xijing University (No. XJ140232)

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	Jin ZHANG
	Ning WANG
	Chong ZHAO
	Jiaxing LI
	Tianchi ZHANG

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https://www.cjmr.org/EN/10.11901/1005.3093.2017.515 OR https://www.cjmr.org/EN/Y2018/V32/I7/555

Fig.1 XRD patterns of K₂V₆O₁₆1.5H₂O precursor (a), the α-AgVO₃ sample (b), the β-AgVO₃ sample (c)

Fig.2 FE-SEM images of K₂V₆O₁₆1.5H₂O precursor (a), the as-prepared α-AgVO₃ sample (b) and the as-prepared β-AgVO₃ sample (c)

Fig.3 TEM and HRTEM images and SAED pattern ofthe as-prepared α-AgVO₃ sample (a, b) andthe as-prepared β-AgVO₃ sample (c, d)

Fig.4 XPS spectra of the α-AgVO₃ sample (a) XPS survey spectrum of the sample, (b) XPS spectrum of the Ag 3d region, (c) XPS spectra of the V 2p regions

Fig.5 Rate capability (a), Cycling performance at 100 mAg^-1 (b) and Nyquist plots after 50 cycles (c) of as-prepared one-dimensional α-AgVO₃ and β-AgVO₃ nanostructures electrode

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