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Preparation and Supercapacitance of C-ZIF-8@AC Composites Electrode Material |
Chuanxiang ZHANG1,2,Zhongyi JIANG3,Yuming DAI1,2,Xiancong HE1,2,Yuan CONG1,2,Shuaishuai ZHU1,2 |
1. School of Materials Science and Engineering, Nanjing Institute of Technology, Nanjing 211167, China 2. Jiangsu Key Laboratory of Advanced Structural Materials and Application Technology, Nanjing 211167, China 3. College of Material Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China |
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Cite this article:
Chuanxiang ZHANG,Zhongyi JIANG,Yuming DAI,Xiancong HE,Yuan CONG,Shuaishuai ZHU. Preparation and Supercapacitance of C-ZIF-8@AC Composites Electrode Material. Chinese Journal of Materials Research, 2019, 33(5): 352-360.
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Abstract A lead-carbon battery, which possesses simultaneously advantages of lead-acid battery and supercapacitor, can be obtained by adding a certain amount of carbon into the lead-acid battery. So, it is particularly critical to create a new type of carbon with ideal specific capacitance and stability in acid solutions. We tried to synthesize such a new carbon material namely C-ZIF-8@AC via a two step process i.e. low temperature liquid phase method and high temperature calcination. The materials were characterized by field emission scanning electron microscope (FESEM), high resolution transmission electron microscope (HRTEM), X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectrometer (FTIR) etc. The results show that the prepared C-ZIF-8@AC composed of carbon particles with polyhedral structure (ZIF-8 framework) grown uniformly on the surface of active carbon (AC) particles; After ZIF-8 has further been coupled with AC particles, the size of the formed C-ZIF-8 particles is reduced. Electrochemical results indicate that the elemental N in pyridine nitrogen and pyrropyrrole nitrogen of the C-ZIF-8 framework can enhance the specific capacitance of C-ZIF-8@AC, which is about 181 F/g, much higher than that of the simple AC. The C-ZIF-8@AC shows excellent cycling stability with 99% capacitance retention rate after 6000 cycles at the current density of 5 A/g, which is higher than that of the simple AC.
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Received: 21 September 2018
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Fund: National Natural Science Foundation of China(11575084, 51402150);Natural Science Foundation of Nanjing Institute of Technology(CKJA201502, JCYJ201606) |
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