<i>γ' </i>相的形貌对Ni-Co基高温合金Portevin-Le Chatelier效应的影响

doi:10.11901/1005.3093.2017.524

材料研究学报

2018, Vol. 32

Issue (9): 647-654 DOI: 10.11901/1005.3093.2017.524

本期目录 | 过刊浏览

γ' 相的形貌对Ni-Co基高温合金Portevin-Le Chatelier效应的影响

张国梁¹, 王新广¹, 王道红², 李志海², 严红彬², 崔传勇¹(

)

1 中国科学院金属研究所沈阳 110016
2 江苏飞跃机泵集团有限公司泰州 225300

Influence of the γ' -phase Morphology on Portevin-Le Chatelier Effect in a Ni-Co Base Superalloy

Guoliang ZHANG¹, Xinguang WANG¹, Daohong WANG², Zhihai LI², Hongbin YAN², Chuanyong CUI¹(

)

1 Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2 Jiangsu Feiyue Pump Group Co. Ltd, Taizhou 225300, China

引用本文:

张国梁, 王新广, 王道红, 李志海, 严红彬, 崔传勇. γ' 相的形貌对Ni-Co基高温合金Portevin-Le Chatelier效应的影响[J]. 材料研究学报, 2018, 32(9): 647-654.
Guoliang ZHANG, Xinguang WANG, Daohong WANG, Zhihai LI, Hongbin YAN, Chuanyong CUI. Influence of the γ' -phase Morphology on Portevin-Le Chatelier Effect in a Ni-Co Base Superalloy[J]. Chinese Journal of Materials Research, 2018, 32(9): 647-654.

全文: PDF(7036 KB) HTML

摘要:

通过不同的热处理工艺制备含花状、球状、立方状γ'相的Ni-Co基变形高温合金,研究了γ'相的形貌对其PLC效应的影响。结果表明：合金的PLC效应与γ'相的形貌有关。球状形貌的γ'相使合金的应力跌幅较大,花状和立方状形貌的γ'相使合金更快完成从正常PLC到反常PLC的转变。合金在中低温(400℃、500℃)拉伸时位错易塞积在复杂形貌(花状和立方)的γ'相周围,合金的变形机制以形成层错或微孪晶为主;而在球状形貌γ'相的周围位错塞积较少,合金的变形机制则以位错滑移为主。

关键词 ：金属材料, PLC效应, γ'相形貌;, Ni-Co基变形高温合金

Abstract：

A Ni-Co based alloy with γ' -phase of various morphologies was prepared by different heat treatment processes. Then the influence of the γ' -phase on the Portevin-Le Chatelier (PLC) effect was investigated systematically. Results show that the PLC effect is related to the morphology of the γ' -phase. During tensile test the alloy shows large stress drop while the spherical-shaped γ' -phase existed. The γ' -phase with flowery and cubic morphology would accelerate the transformation from normal PLC to inverse PLC. When the alloy was tensile tested in medium-low temperatures (400, 500°C) the dislocations would pile up around the γ' -phase with flowery and cubic morphology, and the deformation mechanism of the alloy may be described mainly to stacking fault or deformation twin. While less dislocation piled up around the spherical-shaped γ' -phase, therefore, the deformation of the alloy is mainly controlled by the dislocation slip.

Key words： metallic materials PLC effect γ' morphology; Ni-Co based superalloys

收稿日期: 2017-09-05

ZTFLH:

TG171

基金资助:中国高新技术研究与发展规划(2014AA041701)和国家自然科学基金(51671189, 51331005, 11332010)

作者简介:

作者简介张国梁,男,1990年生,硕士生

	服务

	把本文推荐给朋友
	加入引用管理器
	E-mail Alert
	RSS
	作者相关文章
	张国梁
	王新广
	王道红
	李志海
	严红彬
	崔传勇
44.8K

链接本文:

https://www.cjmr.org/CN/10.11901/1005.3093.2017.524 或 https://www.cjmr.org/CN/Y2018/V32/I9/647

图1 不同γ’相形貌合金的SEM照片

图2 在不同温度下Ni-Co基合金的拉伸真应力-真应变曲线

图3 γ’相形貌不同的Ni-Co基合金的力学性能随着温度和应变速率的变化

图4 在500℃拉伸时不同γ’相形貌合金的临界应变随着应变速率的变化

图5 γ’相的形貌对PLC效应锯齿类型的影响

图6 γ’相的形貌和温度对合金发生PLC效应应力跌幅的影响

图7 不同γ’相形貌的样品拉伸实验后的TEM照片

图8 立方状γ’相样品在750℃拉伸后的TEM照片

[1]	Gu Y F, Cui C Y, Yuan Y, et al.Progress in a high performance cast&wrought superalloy for turbine disc applications[J]. Acta Metallurgica Sinica, 2015, 51(10): 1191
[2]	Y. F. Gu, C. Y. Cui, H. Harada, et al.Development of Ni-Co-base alloys for high-temperature disk applications[C]. Proceedings of the Eleventh International Symposium on Superalloys, Pennsylvania, 2008, 53
[3]	D. U. Furrer, H. J. Fecht.γ' formation in superalloy U720Li[J]. Scripta Materialia, 1999, 40(11): 1215
[4]	M. Jackson, R. Reed, Heat treatment of Udimet 720Li: The effect of microstructure on properties[J]. Materials Science and Engineering, 1999; 259(1): 85
[5]	Q. Zhang, Z. Jiang, H. Jiang, et al.On the propagation and pulsation of Portevin-Le Chatelier deformation bands: An experimental study with digital speckle pattern metrology[J]. International Journal of Plasticity, 2005, 21(11): 2150
[6]	H. Jiang, Q. Zhang, X. Chen,et al.Three types of Portevin-Le Chatelier effects: Experiment and modelling[J]. Acta Materialia, 55(7), 2219(2007)
[7]	J. Min, L. G. Hector, J. Lin, et al.Spatio-temporal characteristics of propagative plastic instabilities in a rare earth containing magnesium alloy[J]. International Journal of Plasticity, 2014, 57: 52
[8]	H. Halim, D. Wilkinson, M. Niewczas.The Portevin-Le Chatelier (PLC) effect and shear band formation in an AA5754 alloy[J]. Acta Materialia, 2007, 55(12): 4151
[9]	A. Le Chatelier.Influence du temps et de la température sur les essais au choc[J]. Rev Metall, 1909, 6: 914
[10]	A. Portevin, F. Le Chatelier.Sur un phénomène observé lors de l’essai de traction d’alliages en cours de transformation[J]. Comptes Rendus de l'Académie des Sciences Paris, 1923, 176: 507
[11]	A. Portevin, F. Le Chatelier.Heat treatment of aluminum-copper alloys[J]. Transactions of the American Society of Steel Treating, 1924, 5: 457
[12]	C. Y. Cui, Y. F. Gu, Y. Yuan, et al.Dynamic strain aging in a new Ni-Co base superalloy[J].Scripta Materialia, 2011, 64(6): 502
[13]	Y. Brechet, Y. Estrin.On the influence of precipitation on the Portevin-Le Chatelier effect[J]. Acta Metallurgica et Materialia, 1995, 43(3): 955
[14]	Y. L. Cai, C. G. Tian, S. H. Fu,et al.Influence of γ? precipitates on Portevin-Le Chatelier effect of Ni-based superalloys[J]. Materials Science and Engineering, 2015, 638(A): 314
[15]	S. Nalawade, M. Sundararaman, R. Kishore, et al.The influence of aging on the serrated yielding phenomena in a nickel-base superalloy[J]. Scripta Materialia, 2008, 59(9): 991
[16]	S. Kumar, H. McShane.Serrated yielding in Al-Li alloys[J]. Scripta Metallurgica et Materialia, 1993, 28(9): 1149
[17]	S. Fu, T. Cheng, Q. Zhang, et al.Two mechanisms for the normal and inverse behaviors of the critical strain for the Portevin-Le Chatelier effect[J]. Acta Materialia, 2012, 60(19): 6650
[18]	B. Brindley, P. Worthington.Yield-point phenomena in substitutional alloys[J]. Metallurgical Reviews, 1970, 15(1): 101
[19]	K. Chihab, Y. Estrin, L. Kubin, et al.The kinetics of the portevin-le chatelier bands in an Al-5at% Mg alloy[J]. Scripta Metallurgica, 1987, 21(2): 203
[20]	P. McCormick.Dynamic strain ageing[J]. Trans Indian Inst Met, 1986, 39(2): 98
[21]	M. Zaiser, P. H?hner.Oscillatory modes of plastic deformation: Theoretical concepts[J]. Physica Status Solidi, 1997, 199(2): 267
[22]	M. Lebyodkin, Y. Brechet, Y. Estrin, et al.Statistics of the catastrophic slip events in the Portevin-Le Chatelier effect[J]. Physical Review Letters, 1995, 74(23): 4758
[23]	M. Lebyodkin, Y. Brechet, Y. Estrin, et al.Statistical behaviour and strain localization patterns in the Portevin-Le Chatelier effect[J]. Acta Materialia, 1996, 44(11): 4531
[24]	M. Lebyodkin, L. Dunin-Barkowskii, Y. Brechet, et al.Spatio-temporal dynamics of the Portevin-Le Chatelier effect: Experiment and modelling[J]. Acta Materialia, 1992, 48(10): 2529
[25]	C. G. TIAN.Effect of stacking fault energy and γ′ volume fraction on the mechanical properties of Ni-Co based superalloys [D], Institute of Metal Research Chinese Academy of Sciences, 2015
[26]	Y. Wen.Symmetrical sisf in deformed Ni3Al and its formation mechanism[J]. Acta Materialia, 1992, 5(2): 76
[27]	R. Mulford, U. Kocks.New observations on the mechanisms of dynamic strain aging and of jerky flow[J]. ActaMetallurgica, 1979, 27(7): 1125
[28]	J. G. Sevillano.An alternative model for the strain hardening of fcc alloys that twin, validated for twinning-induced plasticity steel[J]. Scripta Materialia, 2009, 60(5): 336

[1]	毛建军, 富童, 潘虎成, 滕常青, 张伟, 谢东升, 吴璐. AlNbMoZrB系难熔高熵合金的Kr离子辐照损伤行为[J]. 材料研究学报, 2023, 37(9): 641-648.
[2]	宋莉芳, 闫佳豪, 张佃康, 薛程, 夏慧芸, 牛艳辉. 碱金属掺杂MIL125的CO₂ 吸附性能[J]. 材料研究学报, 2023, 37(9): 649-654.
[3]	赵政翔, 廖露海, 徐芳泓, 张威, 李静媛. 超级奥氏体不锈钢24Cr-22Ni-7Mo-0.4N的热变形行为及其组织演变[J]. 材料研究学报, 2023, 37(9): 655-667.
[4]	邵鸿媚, 崔勇, 徐文迪, 张伟, 申晓毅, 翟玉春. 空心球形AlOOH的无模板水热制备和吸附性能[J]. 材料研究学报, 2023, 37(9): 675-684.
[5]	幸定琴, 涂坚, 罗森, 周志明. C含量对VCoNi中熵合金微观组织和性能的影响[J]. 材料研究学报, 2023, 37(9): 685-696.
[6]	欧阳康昕, 周达, 杨宇帆, 张磊. 含LPSO相Mg-Y-Er-Ni合金的组织和拉伸性能[J]. 材料研究学报, 2023, 37(9): 697-705.
[7]	徐利君, 郑策, 冯小辉, 黄秋燕, 李应举, 杨院生. 定向再结晶对热轧态Cu71Al18Mn11合金的组织和超弹性性能的影响[J]. 材料研究学报, 2023, 37(8): 571-580.
[8]	熊诗琪, 刘恩泽, 谭政, 宁礼奎, 佟健, 郑志, 李海英. 固溶处理对一种低偏析高温合金组织的影响[J]. 材料研究学报, 2023, 37(8): 603-613.
[9]	刘继浩, 迟宏宵, 武会宾, 马党参, 周健, 徐辉霞. 喷射成形M3高速钢热处理过程中组织的演变和硬度偏低问题[J]. 材料研究学报, 2023, 37(8): 625-632.
[10]	由宝栋, 朱明伟, 杨鹏举, 何杰. 合金相分离制备多孔金属材料的研究进展[J]. 材料研究学报, 2023, 37(8): 561-570.
[11]	任富彦, 欧阳二明. g-C₃N₄ 改性Bi₂O₃ 对盐酸四环素的光催化降解[J]. 材料研究学报, 2023, 37(8): 633-640.
[12]	王昊, 崔君军, 赵明久. 镍基高温合金GH3536带箔材的再结晶与晶粒长大行为[J]. 材料研究学报, 2023, 37(7): 535-542.
[13]	刘明珠, 樊娆, 张萧宇, 马泽元, 梁城洋, 曹颖, 耿仕通, 李玲. SnO₂ 作散射层的光阳极膜厚对量子点染料敏化太阳能电池光电性能的影响[J]. 材料研究学报, 2023, 37(7): 554-560.
[14]	秦鹤勇, 李振团, 赵光普, 张文云, 张晓敏. 固溶温度对GH4742合金力学性能及γ' 相的影响[J]. 材料研究学报, 2023, 37(7): 502-510.
[15]	刘天福, 张滨, 张均锋, 徐强, 宋竹满, 张广平. 缺口应力集中系数对TC4 ELI合金低周疲劳性能的影响[J]. 材料研究学报, 2023, 37(7): 511-522.

Viewed

Full text

Abstract

Cited

Shared

Discussed